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Journal of Wuhan University of Technology(Materials Science) 2024年第5期39卷 1294-1302页

作者： XIANG Shuo LU Peng zhang Qinhui XIAO Bowen YANG xin zhang Peili MA Pengfei he Yan LI Xuebin Army Logistics Academy of PLA Chongqing 401311China Naval Aeronautical University Yantai 2640003China Unit 32568 Shaoguan 512131China

Fluorographene(FG)with narrow lateral size and thickness distributions was prepared by a liquid-phase exfoliation method,based on liquid cascade *** Rtec MFT-5000 tribo-meter was used to investigate the lubricating performance of bentonite grease enhanced by the as-prepared *** results showed that the coefficient of friction and the wear volume of bentonite grease with 0.3 wt%FG were decreased by 20.4%and 44.9%,respectively,as compared to those of the base *** main reason is that FG can promote the formation of the tribo-chemical reaction film consisting of complex carbon oxide,Fe_(2)O_(3)and FeF_(3)on the friction surface,which can remarkably improve the performance of friction reduction and prevent the appearance of severe wear.

关键词： fluorographene liquid-phase exfoliation bentonite grease lubrication performance

Exploring Motor Imagery EEG: Enhanced EEG Microstate Analysis with GMD-Driven Density Canopy Method

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Computers, Materials & Continua 2024年第6期79卷 4659-4681页

作者： xin Xiong Jing zhang Sanli Yi Chunwu Wang Ruixiang Liu Jianfeng he Faculty of Information Engineering and Automation Kunming University of Science and TechnologyKunming650500China College of Physics and Electronic Engineering Hanshan Normal UniversityChaozhou521041China Department of Clinical Psychology Second People’s Hospital of YunnanKunming650021China

The analysis of microstates in EEG signals is a crucial technique for understanding the spatiotemporal dynamics of brain electrical *** methods such as Atomic Agglomerative Hierarchical Clustering(AAHC),K-means clustering,Principal Component Analysis(PCA),and Independent Component Analysis(ICA)are limited by a fixed number of microstate maps and insufficient capability in cross-task feature *** these limitations,this study introduces a Global Map Dissimilarity(GMD)-driven density canopy K-means clustering *** innovative approach autonomously determines the optimal number of EEG microstate topographies and employs Gaussian kernel density estimation alongside the GMD index for dynamic modeling of EEG *** this advanced algorithm,the study analyzes the Motor Imagery(MI)dataset from the GigaScience database,*** findings reveal six distinct microstates during actual right-hand movement and five microstates across other task conditions,with microstate C showing superior performance in all task *** imagined movement,microstate A was significantly *** with existing algorithms indicates a significant improvement in clustering performance by the refined method,with an average Calinski-Harabasz Index(CHI)of 35517.29 and a Davis-Bouldin Index(DBI)average of ***,an information-theoretical analysis of the microstate sequences suggests that imagined movement exhibits higher complexity and disorder than actual *** utilizing the extracted microstate sequence parameters as features,the improved algorithm achieved a classification accuracy of 98.41%in EEG signal categorization for motor imagery.A performance of 78.183%accuracy was achieved in a four-class motor imagery task on the BCI-IV-2a *** results demonstrate the potential of the advanced algorithm in microstate analysis,offering a more effective tool for a deeper understanding of the spatiotemporal features of EE

关键词： EEG microstate motor imagery K-means clustering algorithm gaus sian kernel function shannon entropy Lempel-Ziv complexity

Enhancing volatile fatty acids production from waste activated sludge: The role of pretreatment by N,N-bis(carboxymethyl)-L-glutamate (GLDA)

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Environmental Science and Ecotechnology 2024年第5期21卷 149-157页

作者： Chang Liu Lin Li Linji Xu Tanglong zhang Qiang he Xiaodong xin Key Laboratory of the Three Gorges Reservoir Region's Eco-environment Ministry of EducationCollege of Environment and EcologyChongqing UniversityChongqing400045PR China Research Center for Eco-Environmental Engineering Dongguan University of TechnologyDongguan523808PR China

N,N-bis(carboxymethyl)-L-glutamate(GLDA)is an eco-friendly chelating agent that effectively extracts multivalent metal ions from waste activated sludge(WAS)flocs,which could potentially alter their ***,the effect of GLDA on the production of volatile fatty acids(VFAs)from WAS is not well ***,we demonstrate that pretreatment with GLDA at a concentration of 200 mmol per kg VSS results in a significant increase of 142%in extractable extracellular polymeric substances and enhances the total VFAs yield by 64%compared to untreated *** reveal GLDA's capability to mobilize organic-binding multivalent metal ions within sludge ***,post-pretreatment analyses showed the release of 69.1 mg L^(-1) of Ca and 109.8 mg L^(-1) of Fe ions from the flocs,leading to a more relaxed floc structure and a reduced apparent activation energy(10.6 versus 20 kJ mol1)for WAS *** dynamic simulations further demonstrate GLDA's preferential binding to Fe3þand Ca2þover Mg2þ.Our study suggests that GLDA pretreatment causes minimal disruption to reactor stability,thereby indicating the stability of microbial community *** has emerged as a viable pretreatment agent for enhancing volatile fatty acids production from waste activated sludge.

关键词： Anaerobic fermentation Pretreatment Resource recovery Multivalent metals Solubilization

Artificial Self-Recovery Opens up a New Journey of Autonomous health of Mechanical Equipments

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Engineering 2024年第6期37卷 22-26页

作者： xin Pan Haoyu zhang Jinji Gao Weimin Wang Zhinong Jiang Lidong he Beijing Key Laboratory of health Monitoring and Self-recovery for High-end Mechanical Equipment Beijing University of Chemical TechnologyBeijing 100029China Engineering Research Center of Chemical Safety Ministry of Education Beijing University of Chemical TechnologyBeijing 100029China

*** With the implementation of modern production strategies,such as“Industry 4.0”and“Made in China 2025,”the development of high-end mechanical equipment is gradually reaching a high degree of parameterization,digitalization,networking,and intelligence[1].High-end mechanical equipment no longer consists of traditional single devices,but is closely linked to the overall production process;that is,a variety of devices interact with each other and collectively form a complex ***,faults can lead to production delays throughout the system and even seriously threaten the safety of workers[2].In addition,equipment operating in unmanned air or space vehicles(including space robots)cannot be repaired by humans if they break down[3].Until recently,the typical method of addressing machine faults was primarily the“fault cure”method,which involves manually shutting down,inspecting,and repairing the equipment to restore normal ***,the maintenance cycle of the traditional“fault cure”method is time-consuming,and the quality of the maintenance depends on the skills of the technician[4].

关键词： collective consuming Open

Bioinspired Hollow Mesoporous Silica Nanoparticles Coating on Titanium Alloy with Hierarchical Structure for Modulating Cellular Functions

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Journal of Bionic Engineering 2024年第3期21卷 1427-1441页

作者： Jiaxin zhang he Liu Jincheng Wang Jing Shang Mingwei Xu Xiujie Zhu Chao Xu Haotian Bai xin Zhao Orthopedic Institute of Jilin Province Orthopedic Medical CenterThe Second Hospital of Jilin UniversityChangchun130041China Key Laboratory of Bionic Engineering(Ministry of Education) Jilin UniversityChangchun130025China Institute of Structured and Architected Materials Liaoning Academy of MaterialsShenyang110167China

3D-printed Porous Titanium Alloy Implants(pTi),owing to their biologically inertness and relatively smooth surface morphology,adversely affect the biological functions of surrounding *** address the challenges,constructing a bioinspired interface that mimics the hierarchical structure of bone tissue can enhance the cellular functions of *** this context,Hollow Mesoporous Silica Nanoparticles(HMSNs),renowned for their unique physicochemical properties and superior biocompatibility,offer a promising direction for this *** this research,the initially synthesized HMSNs were used to construct a“hollow-mesoporous-macroporous”hierarchical bioinspired coating on the pTi surface through the Layer-by-Layer ***,diverse morphologies of coatings were established by adjusting the deposition strategy of PDDA/HMSNs on the pTi surface(pTi-HMSN-2,pTi-HMSN-4,pTi-HMSN-6).A range of techniques were employed to investigate the physicochemical properties and regulation of cellular biological functions of the diverse HMSN coating ***,the pTi-HMSN-4 and pTi-HMSN-6 groups exhibited the uniform coatings,leading to a substantial enhancement in surface roughness and ***,the coating constructed strategy of pTi-HMSN-4 possessed commendable *** on the aforementioned findings,both pTi-HMSN-4 and pTi-HMSN-6 facilitated the adhesion,spreading,and pseudopodia extension of BMSCs,which led to a notable upsurge in the expression levels of vinculin protein in *** analysis indicates that the coating,when PDDA/HMSNs are deposited four times,possesses favorable overall *** research will provide a solid theoretical basis for the translation of HMSN bioinspired coatings for orthopedic implants.

关键词： Hollow mesoporous silica nanoparticles Bioinspired coating Titanium alloy Hierarchical structure Cellular functions

MoS_(2) nanoflowers and PEDOT:PSS nanocomposite enabling wearable dual-mode pressure sensors

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Science China(Technological Sciences) 2024年第6期67卷 1737-1747页

作者： WANG FengMing YANG WeiJia MA Ke SheN GengZhe SU DaoJian LI BaiJun WANG ShuangPeng QIN BoLong zhang Chi xin Yue CAO XiaoBing he xin School of Applied Physics and Materials Wuyi UniversityJiangmen529020China Biomaterials R&D Center Zhuhai Institute of Advanced TechnologyChinese Academy of SciencesZhuhai519003China Joint Key Laboratory of the Ministry of Education Institute of Applied Physics and Materials EngineeringUniversity of MacaoMacao999078China

A versatile sensing platform employing inorganic MoS_(2) nanoflowers and organic poly(3,4-ethylene dioxythiophene):poly(styrene sulfonate)(PEDOT:PSS)has been investigated to develop the resistive and capacitive force-sensitive *** microstructure of the sensing layer heightens the sensitivity and response time of the dual-mode pressure sensors by augmenting electron pathways and inner stress in response to mechanical ***,the capacitive and resistive sensors exhibit sensitivities of 0.37 and 0.12 kPa^(-1),respectively,while demonstrating a remarkable response time of approximately 100 ***,it is noteworthy that the PEDOT:PSS layer exhibits excellent adhesion to polydimethylsiloxane(PDMS)substrates,which contributes to the development of highly robust force-sensitive sensors capable of enduring more than 10000loading/unloading *** combination of MoS_(2)/PEDOT:PSS layers in these dual-mode sensors has shown promising results in detecting human joint movements and subtle physiological ***,the sensors have achieved a remarkable precision rate of 98%in identifying target *** outcomes underscore the significant potential of these sensors for integration into applications such as electronic skin and human-machine interaction.

关键词： MoS_(2)/PEDOT:PSS nanocomposite force-sensitive sensor multi-scaled microstructure physiological signals monitoring object grasping recognition

Microstructure evolution and strengthening mechanism of high -performance powder metallurgy TA15 titanium alloy by hot rolling

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International Journal of Minerals,Metallurgy and Materials 2024年第6期31卷 1426-1436页

作者： Ying Gao Ce zhang Jiazhen zhang xin Lu Beijing Advanced Innovation Center for Materials Genome Engineering State Key Laboratory for Advanced Metals and MaterialsInstitute for Advanced Ma-terials and TechnologyUniversity of Science and Technology BeijingBeijing 100083China National Engineering Research Center for Advanced Rolling Technology National Engineering Research Center for Flat Rolling EquipmentInstitute of Engin-eering TechnologyUniversity of Science and Technology BeijingBeijing 100083China

Hot deformation of sintered billets by powder metallurgy(PM)is an effective preparation technique for titanium alloys,which is more significant for high-alloying *** this study,Ti–6.5Al–2Zr–Mo–V(TA15)titanium alloy plates were prepared by cold press-ing sintering combined with high-temperature hot *** microstructure and mechanical properties under different process paramet-ers were *** microscope,electron backscatter diffraction,and others were applied to characterize the microstructure evolution and mechanical properties strengthening *** results showed that the chemical compositions were uniformly dif-fused without segregation during sintering,and the closing of the matrix craters was accelerated by increasing the sintering *** block was hot rolled at 1200℃ with an 80%reduction under only two passes without *** strength and elongation of the plate at 20–25℃ after solution and aging were 1247 MPa and 14.0%,respectively,which were increased by 24.5%and 40.0%,respect-ively,compared with the as-sintered alloy at 1300℃.The microstructure was significantly refined by continuous dynamic recrystalliza-tion,which was completed by the rotation and dislocation absorption of the substructure surrounded by low-angle grain *** hot rolling combined with heat treatment,the strength and plasticity of PM-TA15 were significantly improved,which resulted from the dense,uniform,and fine recrystallization structure and the synergistic effect of multiple slip systems.

关键词： elemental powder powder metallurgy titanium alloy hot rolling strength and plasticity

Elaborate Design of Two Novel Fluorescent Zinc-based Metal-Organic Frameworks for Highly Efficient Tetracycline Antibiotics Detection

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Chemical Research in Chinese Universities 2024年第3期40卷 499-507页

作者： TAO he JI Chengshan zhang Jian YIN Yuanyuan JIA Wenwen JIANG xin XU Jie YANG Yulin MIT Key Laboratory of Critical Materials Technology for New Energy Conversion and Storage School of Chemistry and Chemical EngineeringHarbin Institute of TechnologyHarbin 150001P.R.China

The abuse of tetracycline antibiotics has caused great harm to human health and *** inexpensive,convenient and sensitive methods for the detection of tetracycline antibiotics is highly ***,based on the H_(4)ddp ligand[H_(4)ddp=3-(3,5-dicarboxyphenyl)pyridine-2,6-dicarboxylic acid],two novel zinc-based metal-organic frameworks(MOFs){[Zn_(3)(ddp)_(2)(H_(2)O)_(4)]·3H_(2)O}n(Zn1-ddp)and{[Zn_(3)(ddp)_(2)(H_(2)O)_(4)]·3H_(2)O}n(Zn2-ddp)were successfully designed by delicate structural *** Zn1-ddp and Zn2-ddp exhibited excellent water and chemical stability and showed excellent fluorescence quenching performance for tetracycline ***,the more advanced framework structure and better fluorescent performance make Zn1-ddp more sensitive than Zn2-ddp in fluorescent detection with a detection limit of 0.29µmol/L for tetracycline(TC),0.09µmol/L for doxycycline(DOX),0.10µmol/L for minocycline(MIN)and metacycline(MEL),0.19µmol/L for chlortetracycline(CTC),and 0.67µmol/L for oxytetracycline(OTC)among tetracycline *** fluorescence quenching mechanism of Zn1-ddp and Zn2-ddp for tetracycline antibiotics detection was deeply *** reasons for the superior detection performance of Zn1-ddp over Zn2-ddp were also analyzed in depth through Fourier transform infrared spectrophotometry(FTIR),X-ray photoelectron spectroscopy(XPS)analysis and framework structure *** developed method opens up a new perspective for antibiotics detection based on zinc-based MOFs.

关键词： Water system Metal-organic framework Fluorescent detection Tetracycline antibiotic

Recent advances in high charge density triboelectric nanogenerators

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International Journal of Extreme Manufacturing 2024年第4期6卷 1-19页

作者： xin Cui Jiaheng Nie Yan zhang School of Physics University of Electronic Science and Technology of ChinaChengdu 611731People's Republic of China School of Cybersecurity Chengdu University of Information TechnologyChengdu 610225People's Republic of China Beijing Institute of Nanoenergy and Nanosystems Chinese Academy of SciencesBeijing 100083People's Republic of China School of Nanoscience and Technology University of Chinese Academy of SciencesBeijing 100049People's Republic of China

Triboelectric materials with high charge density are the building-block for the commercial application of triboelectric nanogenerators(TENGs).Unstable dynamic processes influence the change of the charge density on the surface and inside of triboelectric *** charge density of triboelectric materials depends on the surface and the internal charge transfer *** focus of this review is on recent advances in high charge density triboelectric materials and advances in the fabrication of *** summarize the existing strategies for achieving high charge density in triboelectric materials as well as their fundamental *** then review current optimization methods for regulating dynamic charge transfer processes to increase the output charge density:first,increasing charge injection and limiting charge dissipation to achieve a high average surface charge density,and second,regulating the internal charge transfer process and storing charge in triboelectric materials to increase the output charge ***,we present the challenges and prospects in developing high-performance triboelectric materials.

关键词： triboelectric nanogenerator charge density charge transfer charge store

Light-based 3D printing of stimulus-responsive hydrogels forminiature devices:recent progress and perspective

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Bio-Design and Manufacturing 2024年第5期7卷 721-746页

作者： Chen xin Neng Xia Li zhang Department of Mechanical and Automation Engineering The Chinese University of Hong KongHong Kong 999077China Multi-Scale Medical Robotics Center Hong Kong Science ParkShatin NTHong Kong 999077China Chow Yuk Ho Technology Center for Innovative Medicine The Chinese University of Hong KongHong Kong 999077China Department of Surgery The Chinese University of Hong KongHong Kong 999077China CUHK T Stone Robotics Institute The Chinese University of Hong KongHong Kong 999077China

Miniature devices comprising stimulus-responsive hydrogels with high environmental adaptability are now considered competitive candidates in the fields of biomedicine,precise sensors,and tunable *** and advanced fabricationmethods are critical formaximizing the application capabilities ofminiature ***-based three-dimensional(3D)printing technology offers the advantages of a wide range of applicable materials,high processing accuracy,and strong 3D fabrication capability,which is suitable for the development of miniature devices with various *** paper summarizes and highlights the recent advances in light-based 3D-printed miniaturized devices,with a focus on the latest breakthroughs in lightbased fabrication technologies,smart stimulus-responsive hydrogels,and tunable miniature devices for the fields of miniature cargo manipulation,targeted drug and cell delivery,active scaffolds,environmental sensing,and optical ***,the challenges in the transition of tunable miniaturized devices from the laboratory to practical engineering applications are *** opportunities that will promote the development of tunable microdevices are elaborated,contributing to their improved understanding of these miniature devices and further realizing their practical applications in various fields.

关键词： 3D printing Stimulus-responsive hydrogels Miniature devices Shape-morphing