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Particuology 2024年第1期84卷 81-88页

作者： Junhua Li Lingshu Gao Junmao Hong Xiaofeng Shi Sifang Kong Jingyu Wang hassan algadi Benbin Xu Zhanhu Guo School of Chemistry and Chemical Engineering North University of ChinaTaiyuan030051China School of Traffic&Environment Shenzhen Institute of Information TechnologyShenzhen518172China Department of Electrical Engineering Faculty of EngineeringNajran UniversityNajran11001Saudi Arabia Mechanical and Construction Engineering Faculty of Engineering and EnvironmentNorthumbria UniversityNewcastle Upon TyneNE18STUK

Terephthalic acid reformed Al/Zn metal organic nanoflake was prepared and functionalized with trie-thylamine(T-AlZn).Without adding terephthalic acid,there was no product of metal organic nanoflake.T-AlZn has a remarkable performance in removing trace lead(Ⅱ)ions(Pb^(2+)).The adsorption equipoise with the removal rate≥97%was reached within 35 min.The removal rates of T-AlZn for Pb^(2+)declined by only 16.73%after four regenerations.The adsorption of T-AlZn for Pb^(2+)follows the Langmuir isotherms model and pseudo-second-order dynamics model.The utmost adsorption competence was calculated as 215.27 mg g^(-1).The T-AlZn adsorbent exhibits a bright prospect in the adsorption for Pb^(2+)and is a considerable candidate in the disposal of industrial sewage.

关键词： Metal organic complex Nanoflake Trace level Pb^(2+) Adsorption

MXene Enhanced 3D Needled Waste Denim Felt for High‑Performance Flexible Supercapacitors

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Nano-Micro Letters 2024年第2期16卷 383-394页

作者： Wei Fan Qi Wang Kai Rong Yang Shi Wanxi Peng Handong Li Zhanhu Guo Ben Bin Xu Hua Hou hassan algadi Shengbo Ge Key Laboratory of Functional Textile Material and Product of the Ministry of Education School of Textile Science and EngineeringInstitute of Flexible electronics and Intelligent TextileXi’an Polytechnic UniversityXi’an 710048People’s Republic of China Co‑Innovation Center of Efficient Processing and Utilization of Forest Resources College of Materials Science and EngineeringNanjing Forestry UniversityNanjing 210037People’s Republic of China Henan Province International Collaboration Lab of Forest Resources Utilization School of ForestryHenan Agricultural UniversityZhengzhou 450002People’s Republic of China Integrated Composites Lab Department of Mechanical and Construction EngineeringNorthumbria UniversityNewcastle Upon Tyne NE18STUK College of Materials Science and Engineering Taiyuan University of Science and TechnologyTaiyuan 030024People’s Republic of China Department of Electrical Engineering Faculty of EngineeringNajran University11001 NajranSaudi Arabia

MXene,a transition metal carbide/nitride,has been prominent as an ideal electrochemical active material for supercapacitors.However,the low MXene load limits its practical applications.As environmental concerns and sustainable development become more widely recognized,it is necessary to explore a greener and cleaner technology to recycle textile by-products such as cotton.The present study proposes an effective 3D fabrication method that uses MXene to fabricate waste denim felt into ultralight and flexible supercapacitors through needling and carbonization.The 3D structure provided more sites for loading MXene onto Z-directional fiber bundles,resulting in more efficient ion exchange between the electrolyte and electrodes.Furthermore,the carbonization process removed the specific adverse groups in MXenes,further improving the specific capacitance,energy density,power density and electrical conductivity of supercapacitors.The electrodes achieve a maximum specific capacitance of 1748.5 mF cm-2 and demonstrate remarkable cycling stability maintaining more than 94%after 15,000 galvanostatic charge/discharge cycles.Besides,the obtained supercapacitors present a maximum specific capacitance of 577.5 mF cm^(-2),energy density of 80.2μWh cm^(-2)and power density of 3 mW cm^(-2),respectively.The resulting supercapacitors can be used to develop smart wearable power devices such as smartwatches,laying the foundation for a novel strategy of utilizing waste cotton in a high-quality manner.

关键词： MXene 3D needled waste denim felt Supercapacitors Carbonization

High-performance flexible all-solid-state asymmetric supercapacitors based on binder-free MXene/cellulose nanofiber anode and carbon cloth/polyaniline cathode

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Nano Research 2023年第5期16卷 7696-7709页

作者： Xiaoyu Bi Meichun Li Guoqiang Zhou Chaozheng Liu Runzhou Huang Yang Shi Ben Bin Xu Zhanhu Guo Wei Fan hassan algadi Shengbo Ge Jiangsu Co-Innovation Center of Efficient Processing and Utilization of Forest Resources International Innovation Center for Forest Chemicals and MaterialsCollege of Materials Science and EngineeringNanjing Forestry UniversityNanjing 210037China School of Petroleum Engineering China University of Petroleum(East China)Qingdao 266580China Integrated Composites Lab Department of Mechanical and Construction EngineeringNorthumbria UniversityNewcastle Upon TyneNE18STUK School of Textile Science and Engineering&Key Laboratory of Functional Textile Material and Product of Ministry of Education Xi'an Polytechnic UniversityXi'an 710048China College of Materials Science and Engineering Taiyuan University of Science and TechnologyTaiyuan 030024China Department of Electrical Engineering Faculty of EngineeringNajran UniversityNajran11001Saudi Arabia

The search for wearable electronics has been attracted great efforts,there is an ever-growing demand for all-solid-state flexible energy storage devices.However,it is a challenge to obtain both positive and negative electrodes with excellent mechanical strength and match positive and negative charges to achieve high energy densities and operate voltages to satisfy practical application requirements.Here,flexible MXene(Ti_(3)C_(2)Tx)/cellulose nanofiber(CNF)composite film negative electrodes(MCNF)were fabricated with a vacuum filtration method,as well as positive electrodes(CP)by combining polyaniline(PANI)with carbon cloth(CC)using an in-situ polymerization method.Both positive and negative free-standing electrodes exhibited excellent electrochemical behavior and bendable/foldable flexibility.As a result,the all-pseudocapacitance asymmetric device of MCNF//CP assembled with charge-matched between anode and cathode achieves an extended voltage window of 1.5 V,high energy density of 30.6 Wh·kg^(−1)(1211 W·kg^(−1)),86%capacitance retention after 5000 cycles,the device maintains excellent bendability,simultaneously.This work will pave the way for the development of all-pseudocapacitive asymmetric supercapacitors(ASC)with simultaneously preeminent mechanical properties,high energy density,wide operating voltage window.

关键词： MXene cellulose nanofiber polyaniline asymmetric supercapacitors

Tellurium intervened Fe-N codoped carbon for improved oxygen reduction reaction and high-performance Zn-air batteries

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Journal of Materials Science & Technology 2023年第6期137卷 215-222页

作者： Rui Wang Zihan Meng Xuemin Yan Tian Tian Ming Lei Rami Adel Pashameah Hala MAbo-Dief hassan algadi Nina Huang Zhanhu Guo Haolin Tang State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China Foshan Xianhu Laboratory of the Advanced Energy Science and Technology Guangdong Laboratory Xianhu Hydrogen ValleyFoshan 528200China College of Chemistry and Environmental Engineering Yangtze UniversityJingzhou 434023China State Key Laboratory of Information Photonics and Optical Communications Beijing University of Posts and TelecommunicationsBeijing 100876China Department of Chemistry Faculty of Applied ScienceUmm Al-Qura UniversityMakkah 24230Saudi Arabia Department of Science and Technology University College-RanyahTaif UniversityP.O.Box 11099Taif 21944Saudi Arabia Department of Electrical Engineering Faculty of EngineeringNajran UniversityP.O.Box 1988Najran 11001Saudi Arabia College of Materials Science and Engineering Taiyuan University of Science and TechnologyTaiyuan 030024China Department of Chemical and Bimolecular Engineering Integrated Composites Laboratory(ICL)University of TennesseeKnoxvilleTN 37996USA Guangdong Hydrogen Energy Institute of WHUT Xianhu Hydrogen ValleyFoshan 528200China

Pyrolysis-acquired iron and nitrogen codoped carbon(Fe-N-C)has been comprehensively investigated for its promising oxygen reduction reaction(ORR)catalytic performance and structural complexity.The modification of non-metal elements with larger atomic radius and the corresponding intrinsic microstructure-property relations are rarely reported.In this study,tellurium(Te)intervened Fe-N-C was prepared by micelles-induced polymerization with Te nanowires as an in-situ intervening agent.The out-plane bonding of Te with Fe induced the increase of both N content and proportion of pyridinic N on the material surface,thus improving the ORR catalytic performance.The assembled Zn-air battery demonstrated a maximum power density of 250 mW/cm^(2)and excellent rate capability under various discharge current densities,which was much better than the Pt/C.Overall,the current work demonstrates a novel Te/Fe-N-C material and reveals an original Te intervened Fe-N-C strategy and N reconfiguration mechanism,which is of great significance for the design of key materials in energy-related fields.

关键词： Te/Fe-N-C Assembly ORR Electrocatalysis Zn-air battery

Influence of mass ratio and calcination temperature on physical and photoelectrochemical properties of ZnFe-layered double oxide/cobalt oxide heterojunction semiconductor for dye degradation applications

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Particuology 2023年第3期74卷 141-155页

作者： Yufei Zhang Junjie Zheng Jiejie Nan Chengjie Gai Qian Shao Vignesh Murugadoss Srihari Maganti Nithesh Naik hassan algadi Mina Huang Ben Bin Xu Zhanhu Guo College of Chemical and Biological Engineering Shandong University of Science and TechnologyQingdao266590China College of Materials Science and Engineering Taiyuan University of Science and TechnologyTaiyuan030024China Integrated Composites Laboratory(ICL) Department of Chemical and Bimolecular EngineeringUniversity of TennesseeKnoxvilleTN37996United States Department of Mechanical&Manufacturing Engineering Manipal Institute of TechnologyManipal Academy of Higher EducationManipal576104KarnatakaIndia Mechanical and Construction Engineering Faculty of Engineering and EnvironmentNorthumbria UniversityNewcastle Upon TyneNE18STUK Department of Electrical Engineering Faculty of EngineeringNajran UniversityNajran11001Saudi Arabia

A visible light-active photoelectrocatalyst,ZnFe-layered double oxide(LDO)/cobalt(II,III)oxide(Co_(3)O_(4))composites were obtained by calcining the Co loaded ZnFe-layered double hydroxide(LDH)prepared by a hydrothermal and microwave hydrothermal method.The morphological studies revealed that the ZnFe-LDO/Co_(3)O_(4) composites exhibited a flower-like structure comprising Co_(3)O_(4) nanowires and ZnFe-LDO nanosheets.Further,when the mass ratio of Co(NO_(3))_(2)·6H_(2)O/LDH was 1:1.8 and the calcination temperature was 550℃,the ZnFe-LDO/Co_(3)O_(4) composite exhibited 93.3%degradation efficiency for methylene blue(MB)at the applied voltage of 1.0 V under visible light after 3 h.Furthermore,the Mott-Schottky model experiments showed that the formation of a p-n heterojunction between ZnFe-LDO and Co_(3)O_(4) could effectively inhibit the recombination of electrons and holes in the photoelectrocatalytic process.Meanwhile,free radical scavenging experiments showed that the active radicals of⋅OH played an important role in the degradation of MB.Therefore,the photoelectrocatalytic effect of ZnFe-LDO/Co_(3)O_(4) provides a simple and effective strategy for the removal of organic pollutants.

关键词： ZnFe-LDO/Co_(3)O_(4) Photoelectrocatalytic p-n heterojunction Methylene blue

Effect of K_(2)CO_(3) doping on CO_(2) sorption performance of silicate lithium-based sorbent prepared from citric acid treated sediment

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Chinese Journal of Chemical Engineering 2022年第11期51卷 10-20页

作者： Junya Wang Kai Chen Yi Wang Jiuming Lei Abdullah Alsubaie Ping Ning Shikun Wen Taiping Zhang Abdulraheem S.AAlmalki AAlhadhrami Zhiping Lin hassan algadi Zhanhu Guo Faculty of Environmental Science and Engineering Kunming University of Science and TechnologyKunming 650500China Ecological Environment Monitoring Station Linxiang BranchLincang Municipal Bureau of Ecology and EnvironmentLincang 677000China Department of Physics College of KhurmaTaif UniversityP.O.Box 11099Taif 21944Saudi Arabia Department of Chemistry Faculty of ScienceTaif UniversityP.O.Box 11099Taif 21944Saudi Arabia Integrated Composites Laboratory(ICL) Department of Chemical and Bimolecular EngineeringUniversity of TennesseeKnoxvilleTN 37996United States Department of Electrical Engineering Faculty of EngineeringNajran UniversityP.O.Box 1988Najran 11001Saudi Arabia College of Materials Science and Engineering Taizhou UniversityTaizhou 318000China

In this paper,a low-cost and environmental-friendly leaching agent citric acid(C_(6)H_(8)O_(7))was used to treat the sediment of Dianchi Lake(SDL)to synthesize lithium silicate(Li_(4)SiO_(4))based CO_(2)sorbent.The results were compared with that treated with strong acid.Moreover,the effects of preparation conditions,sorption conditions and desorption conditions on the CO_(2)sorption performance of prepared Li_(4)SiO_(4)were systematically studied.Under optimal conditions,the Li_(4)SiO_(4)sorbent was successfully synthesized and its CO_(2)sorption capacity reached 31.37%(mass),which is much higher than that synthesized from SDL treated with strong acid.It is speculated that the presence of some elements after C_(6)H_(8)O_(7)treatment may promote the sorption of synthetic Li_(4)SiO_(4)to CO_(2).In addition,after doping with K_(2)CO_(3),the CO_(2)uptake increases from the original 12.02%and 22.12%to 23.96%and 32.41%(mass)under the 20%and 50%CO_(2)partial pressure,respectively.More importantly,after doping K_(2)CO_(3),the synthesized Li_(4)SiO_(4)has a high cyclic stability under the low CO_(2)partial pressure.

关键词： CO_(2)sorbents Li_(4)SiO_(4) Sediment Citric acid Doped with K_(2)CO_(3)

An efficient bifunctional Ni-Nb_(2)O_(5)nanocatalysts for the hydrodeoxygenation of anisole

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Chinese Journal of Chemical Engineering 2022年第9期35卷 187-197页

作者： Juan Xu Ping Zhu Islam HEl Azab Ben Bin Xu Zhanhu Guo Ashraf YElnaggar Gaber AMMersal Xiangyi Liu Yunfei Zhi Zhiping Lin hassan algadi Shaoyun Shan Faculty of Chemical Engineering Kunming University of Science and TechnologyKunming 650500China College of Chemical Engineering Southwest Forestry UniversityKunming 650224China Yunnan Province Special Equipment Safety Inspection and Research Institute Kunming 650228China Department of Food Science and Nutrition College of ScienceTaif UniversityTaif 21944Saudi Arabia Department of Mechanical and Construction Engineering Faculty of Engineering and EnvironmentNorthumbria UniversityNewcastle upon Tyne NE18STUK Integrated Composites Lab(ICL) Department of Chemical&Biomolecular EngineeringUniversity of TennesseeKnoxvilleTN 37996USA Department of Chemistry College of ScienceTaif UniversityTaif 21944Saudi Arabia Taizhou University Taizhou 31800China Department of Electrical Engineering Faculty of EngineeringNajran UniversityNajran 11001Saudi Arabia

The Ni-Nb_(2)O_(5)nanocatalysts have been prepared by the solgel method,and the catalytic hydrodeoxygenation(HDO)performance of anisole as model compound is studied.The results show that Nb exists as amorphous Nb_(2)O_(5)species,which can promote Ni dispersion.The addition of Nb_(2)O_(5)increases the acidity of the catalyst.However,when the content of niobium is high,there is an inactive Nb-Ni-O mixed phase.The size and morphology of Ni grains in catalysts are different due to the difference of Nb/Ni molar ratio.The Ni_(0.9)Nb_(0.1)sample has the largest surface area of 170.8 m^(2)·g^(-1)among the catalysts prepared in different Nb/Ni molar ratios,which is mainly composed of spherical nanoparticles and crack pores.The HDO of anisole follows the reaction route of the hydrogenation HYD route.The Ni_(0.9)Nb_(0.1)catalyst displayed a higher HDO performance for anisole than Ni catalyst.The selectivity to cyclohexane over the Ni_(0.9)Nb_(0.1)sample is about 10 times that of Ni catalyst at 220℃and 3 MPa H_(2).The selectivity of cyclohexane is increased with the increase of reaction temperature.The anisole is almost completely transformed into cyclohexane at 240℃,3 MPa H_(2)and 4 h.

关键词： Hydrodeoxygenation(HDO) Catalysts Ni-Nb_(2)O_(5) Solgel method Anisole

Controlled multilevel switching and artificial synapse characteristics in transparent HfAlO-alloy based memristor with embedded TaN nanoparticles

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Journal of Materials Science & Technology 2021年第36期95卷 203-212页

作者： Chandreswar Mahata hassan algadi Muhammad Ismail Daewoong Kwon Sungjun Kim Division of Electronics and Electrical Engineering Dongguk UniversitySeoul 04620Republic of Korea Department of Electrical Engineering Faculty of EngineeringNajran UniversityP.O.Box 1988Najran 11001Saudi Arabia Department of Electrical Engineering Inha UniversityIncheonRepublic of Korea

Atomic layer deposition technique has been used to prepare tantalum nitride nanoparticles(TaN-NPs)and sandwiched between Al-doped HfO;layers to achieve ITO/HfAlO/TaN-NP/HfAlO/ITO RRAM device.Transmission electron microscopy along with energy dispersive spectroscopy confirms the presence of TaN-NPs.X-ray photoelectron spectroscopy suggests that part of Ta N converted to tantalum oxynitride(TaO_(x)N_(y))which plays an important role in stable cycle-to-cycle resistive switching.Charge trapping and oxygen vacancy creation were found to be modified after the inclusion of Ta N-NPs inside RRAM structure.Also,HfAlO/TaO_(x)N_(y)interface due to the presence TaN-NPs improves the device-to-device switching reliability by reducing the probability of random rupture/formation of conductive filaments(CFs).DC endurance of more than 10^(3)cycles and memory data retention up to 10^(4)s was achieved with an insignificant variation of different resistance states.Multilevel conductance was attained by controlling RESET voltage with stable data retention in multiple states.The volatile threshold switching was monitored after controlling the CF forming at 200 nA current compliance with high selectivity of~10^(3).Synaptic learning behavior has been demonstrated by spike-rate-dependent plasticity(SRDP).Reliable potentiation and depression processes were observed after the application of suitable negative and positive pulses which shows the capability of the TaN–NPs based RRAM device for transparent synaptic devices.

关键词： RRAM ALD TaN-nanoparticles Threshold switching Spike-rate-dependent plasticity Multilevel conductance Synaptic properties

Boosted lithium storage performance by local build-in electric field derived by oxygen vacancies in 3D holey N-doped carbon structure decorated with molybdenum dioxide

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Journal of Materials Science & Technology 2023年第11期142卷 185-195页

作者： Chuanxin Hou Wenyue Yang Hideo Kimura Xiubo Xie Xiaoyu Zhang Xueqin Sun Zhipeng Yu Xiaoyang Yang Yuping Zhang Bin Wang Ben Bin Xu Deepak Sridhar hassan algadi Zhanhu Guo Wei Du School of Environmental and Material Engineering Yantai UniversityYantai 264005China Shandong Laboratory of Yantai Advanced Materials and Green Manufacturing Yantai 264005China Department of Chemical&Biomolecular Engineering University of TennesseeKnoxvilleTN 37996USA College of Materials Science and Engineering Taiyuan University of Science and TechnologyTaiyuan 030024China Mechanical and Construction Engineering Faculty of Engineering and EnvironmentNorthumbria UniversityNewcastle Upon Tyne NE18STUK Zentek Ltd. 24 Corporate CourtGuelphON N1G 5G5Canada Department of Electrical Engineering Faculty of EngineeringNajran UniversityNajran 11001Saudi Arabia Integrated Composites Laboratory(ICL) Mechanical and Construction EngineeringFaculty of Engineering and EnvironmentNorthumbria UniversityNewcastle Upon TyneNE18STUK

Three-dimensional holey nitrogen-doped carbon matrixes decorated with molybdenum dioxide(MoO_(2))nanoparticles have been successfully synthesized via a NaCl-assisted template strategy.The obtained MoO_(2)/C composites offered multi-advantages,including higher specific surface area,more active sites,more ions/electrons transmission channels,and shorter transmission path due to the synergistic effect of the uniformly distributed MoO_(2) nanoparticles and porous carbon structure.Especially,the oxygen vacancies were introduced into the prepared composites and enhanced the Li^(+)intercalation/deintercalation process during electrochemical cycling by the Coulomb force.The existence of the local built-in electric field was proved by experimental data,differential charge density distribution,and density of states calculation.The uniquely designed structure and introduced oxygen vacancy defects endowed the MoO_(2)/C composites with excellent electrochemical properties.In view of the synergistic effect of the uniquely designed morphology and introduced oxygen vacancy defects,the MoO_(2)/C composites exhibited superior electrochemical performance of a high capacity of 918.2 mAh g^(-1) at 0.1 A g^(-1) after 130 cycles,562.1 mAh g^(-1) at 1.0 A g^(-1) after 1000 cycles,and a capacity of 181.25 mAh g^(-1) even at 20.0 A g^(-1).This strategy highlights the path to promote the commercial application of MoO_(2)-based and other transition metal oxide electrodes for energy storage devices.

关键词： MoO_(2)/C hybrid 3D holey structure Oxygen vacancies Lithium-ion batteries

Morphology controllable urchin-shaped bimetallic nickel-cobalt oxide/carbon composites with enhanced electromagnetic wave absorption performance

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Journal of Materials Science & Technology 2023年第17期148卷 250-259页

作者： Fushan Li Qiuyu Li Hideo Kimura Xiubo Xie Xiaoyu Zhang Nannan Wu Xueqin Sun Ben Bin Xu hassan algadi Rami Adel Pashameah Abdullah K.Alanazi Eman Alzahrani Handong Li Wei Du Zhanhu Guo Chuanxin Hou School of Environmental and Material Engineering Yantai UniversityYantai 264005China Shandong Laboratory of Yantai Advanced Materials and Green Manufacturing Yantai 264005China School of Material Science and Engineering Shandong University of Science and TechnologyQingdao 266590China Mechanical and Construction Engineering Faculty of Engineering and EnvironmentNorthumbria UniversityNewcastle Upon Tyne NE18STUK College of Materials Science and Engineering Taiyuan University of Science and TechnologyTaiyuan 030024China Department of Electrical Engineering Faculty of EngineeringNajran UniversityNajran 11001Saudi Arabia Department of Chemistry Faculty of Applied ScienceUmm Al-Qura UniversityMakkah 24230Saudi Arabia Department of Chemistry College of ScienceTaif UniversityP.O.Box 11099Taif 21944Saudi Arabia Integrated Composites Laboratory(ICL) Mechanical and Construction EngineeringNorthumbria UniversityNewcastle Upon Tyne NE18STUK Department of Chemical and Bimolecular Engineering University of TennesseeKnoxvilleTN 37996United States

The microscopic morphology of electromagnetic wave absorbers influences the multiple reflections of electromagnetic waves and impedance matching,determining the absorption properties.Herein,the urchin-shaped bimetallic nickel-cobalt oxide/carbon(NiCo_(2)O_(4)/C)composites are prepared via a hy-drothermal route,whose absorption properties are investigated by different morphologies regulated by changing calcination temperature.A minimum reflection loss(RL_(min))of-75.26 dB is achieved at a match-ing thickness of 1.5 mm,and the effective absorption bandwidth(EAB)of 8.96 GHz is achieved at 2 mm.Multi-advantages of the synthesized NiCo_(2)O_(4)/C composites contribute to satisfactory absorption proper-ties.First,the interweaving of the needle-like structures increases the opportunities for scattering and multiple reflections of incident electromagnetic waves,and builds up a conductive network to facilitate the enhancement of conductive losses.Second,the carbon component in the NiCo_(2)O_(4)/C composites en-hances the interfacial polarization and reduces the density of the absorber.Besides,generous oxygen va-cancy defects are introduced into the NiCo_(2)O_(4)/C composites,which induces defect polarization and dipole polarization.In summary,the ternary coordination of components,defects and morphology led to out-standing electromagnetic wave absorption,which lightened the path for improving the electromagnetic wave absorption property and enriching the family of NiCo_(2)O_(4) absorbers with excellent performance.

关键词： NiCo_(2)O_(4)/C Oxygen vacancies Interfacial polarization Electromagnetic wave absorber