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Synthesis of Graphene Oxide from Hydrogenated Diamond Like Carbon and Protein Immobilization onto It: Characterization and Study of Practical Utility

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Journal of Materials Science and Chemical Engineering 2021年第1期9卷 32-41页

作者： Subhashis Bala Reshmi Bose Shaona Chaterjee Sanjit Sarkar Indranil Saha hari shankar biswas Department of Chemistry Surendranath College Kolkata India Chakdaha Nadia India Department of Basic Science and Humanities University of Engineering and Management Newtown India Department of Chemistry Presidency University Kolkata India Department of Physics Surendranath Evening College Kolkata India Sripat Singh College Jiagangj Murshidabad West Bengal India

In the last few years, Graphene oxide material and biomolecules studies have increased. The various synthesis methods of graphene oxide are constantly pursued to improve and provide safer and more effective alternatives. Though the preparation of graphene oxide from Graphite powder or Graphite flake through Hummers method is one of the oldest techniques but still now it is one of the most suitable methods. Here, Graphene Oxide has been prepared from a tunable material Hydrogenated diamond like carbon (HDLC) which is an atomically smooth surface that can be deposited on high-surface area Silicon (100) wafer plate. The HDLC film was heated at a fixed temperature of 900°C for 30 min in high vacuum ~1 × 10−6 torr and oxygenated at room temperature. A synthetic sequence is described involving Oxidation of annealed HDLC (A-HDLC). Raman measurements confirm the G and D peak by Oxidation of A-HDLC and FTIR confirms functional groups. Atomic force microscopy (AFM) images describe the surface of A-HDLC, Oxidized Graphene and BSA immobilized GO. This GO onto Silicon substrate offers many technical advantages than as oxidized graphene Synthesis from other Chemical methods.

关键词： Carbon Diamond Graphene Oxide AFM Raman FTIR

Comparative measurement of CO_(2),CH_(4)and CO at two traffic interjunctions having inflated vehicular flow in Delhi

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Journal of Environmental Sciences 2024年第7期141卷 314-329页

作者： Komal Daya Soni Khem Singh shankar G.Aggarwal CSIR-National Physical Laboratory Dr.K.S.Krishnan MargNew Delhi 110012India Academy of Scientific&Innovative Research(AcSIR) Ghaziabad 201002India

Vehicular emissions are considered one of the major anthropogenic sources of greenhouse gases and poor air quality in metropolitan *** study aims to see the correlation of CO_(2),CH_(4),and CO through monitoring over a period from December 2020 to October 2021 covering three seasons’winter,summer,and monsoon at two different traffic locations of Delhi having different traffic volumes,road patterns,and traffic *** annual average morning concentration of CO_(2),CH_(4)and CO was found(533±105),(7.3±3.1),(10.7±3.0)ppm at Najafgarh and(480±70),(5.2±1.8),(7.8±2.8)ppm at Rajendra Place,respectively.A relationship between concentration of all three gases and meteorological parameters such as temperature,humidity,wind speed and wind direction has also been investigated using Pearson correlation coefficient and pollution rose diagram.A comparable pattern in concentration was observed for all three gases in spatial(location)and temporal(diurnal)*** concentration trend of CO_(2)in different seasons is winter>summer>monsoon,while in the case of CH_(4)winter=summer>monsoon but not any seasonal trend was noted in CO *** is observed that CO_(2)has a good relation with CO(a tracer for vehicular emission)in terms of diurnal variation,whereas,CH_(4)does not represent a relation with CO and CO_(2)diurnally,suggesting that vehicles are the source of CO_(2)but not much contributing to other greenhouse gases like CH_(4).

关键词： Vehicular emission Greenhouse gases Harmful pollutants Meteorological parameters

Dynamics of some new solutions to the coupled DSW equations traveling horizontally on the seabed

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Journal of Ocean Engineering and Science 2024年第2期9卷 154-163页

作者： Raj Kumar Ravi shankar Verma Department of Mathematics Faculty of Engineering&TechnologyVeer Bahadur Singh Purvanchal UniversityJaunpur 222003India

The system of(1+1)-coupled Drinfel’d-Sokolov-Wilson equations describes the surface gravity waves travelling horizontally on the *** objective of the present research is to construct a new variety of analytical solutions for the *** invariants are derived with the aid of Killing form by using the optimal algebra classification via Lie symmetry *** invariant solutions involve time,space variables,and arbitrary *** adequate constraints on arbitrary constants,solutions are represented graphically to make them more applicable in designing sea *** behavior of solutions shows asymptotic,bell-shaped,bright and dark soliton,bright soliton,parabolic,bright and kink,kink,and periodic *** constructed results are novel as the reported results[26,28,29,30,33,38,42,49]can be deduced from the results derived in this *** remaining solutions derived in this study,are absolutely different from the earlier *** this study,the physical character of analytical solutions of the system could aid coastal engineers in creating models of beaches and ports.

关键词： Coupled Drinfel’d-Sokolov-Wilson model Invariants Killing form Optimal sub algebra Lie symmetry reductions

An Interactive Operating Demand Response Approach for Hybrid Power Systems Integrating Renewable Energy Sources

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Protection and Control of Modern Power Systems 2024年第3期9卷 174-194页

作者： Abhishek Saxena Ravi shankar IEEE the Department of Electrical Engineering National Institute of Technology PatnaIndia

The increased deployment of renewable energy in existing power networks has jeopardized rotational inertia,resulting in system degradation and *** address the issue,this paper proposes a demand response strategy for ensuring the future reliability of the electrical power *** addition,a modified fuzzy logic control topology-based two-degree-of-freedom(fractional order proportional integral)-tilt derivative controller is designed to regulate the frequency within a demand response framework of a hybrid two-area deregulated power *** test system includes thermal power plants,renewable energy sources(such as wind,parabolic trough solar thermal plant,biogas),and electric vehicle *** adaptively tune the controller’s coefficients,a quasi-opposition-based harris hawks optimization(QOHHO)algorithm is *** effectiveness of this algorithm is compared to other optimization algorithms,and the stability of the system is *** results demonstrate that the designed control algorithm significantly enhances system frequency stability in various scenarios,including uncertainties,physical constraints,and high penetration of renewables,compared to existing ***,an experimental assessment through OPAL-RT is conducted to verify the practicality of the proposed strategy,considering source and load intermittencies.

关键词： Area control error demand response energy storage vertically integrated utility

A high aspect ratio surface micromachined accelerometer based on a SiC-CNT composite material

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Microsystems & Nanoengineering 2024年第2期10卷 219-230页

作者： Jiarui Mo Shreyas shankar Roberto Pezone Guoqi Zhang Sten Vollebregt Laboratory of Electronic Components Technology and Materials(ECTM)Department of MicroelectronicsDelft University of TechnologyDelftThe Netherlands

Silicon carbide(SiC)is recognized as an excellent material for microelectromechanical systems(MEMS),especially those operating in challenging environments,such as high temperature,high radiation,and corrosive ***,SiC bulk micromachining is still a challenge,which hinders the development of complex SiC *** address this problem,we present the use of a carbon nanotube(CNT)array coated with amorphous SiC(a-SiC)as an alternative composite material to enable high aspect ratio(HAR)surface *** using a prepatterned catalyst layer,a HAR CNT array can be grown as a structural template and then densified by uniformly filling the CNT bundle with LPCVD *** electrical properties of the resulting SiC-CNT composite were characterized,and the results indicated that the electrical resistivity was dominated by the *** demonstrate the use of this composite in MEMS applications,a capacitive accelerometer was designed,fabricated,and *** fabrication results showed that the composite is fully compatible with the manufacturing of surface micromachining *** Young’s modulus of the composite was extracted from the measured spring constant,and the results show a great improvement in the mechanical properties of the CNTs after coating with *** accelerometer was electrically characterized,and its functionality was confirmed using a mechanical shaker.

关键词： composite surface electrical

Structural build-up model for three-dimensional concrete printing based on kinetics theory

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Frontiers of Structural and Civil Engineering 2024年第7期18卷 998-1014页

作者： Prabhat Ranjan PREM P.S.AMBILY shankar KUMAR Greeshma GIRIDHAR Dengwu JIAO Advanced Materials Laboratory CSIR-Structural Engineering Research CentreChennai 600113India Department of Architecture and Civil Engineering City University of Hong KongHong Kong 999077China

The thixotropic structural build-up is crucial in extrusion-based three-dimensional(3D)concrete *** paper uses a theoretical model to predict the evolution of static and dynamic yield stress for printed *** model employs a structural kinetics framework to create a time-independent constitutive link between shear stress and shear *** model considers flocculation,deflocculation,and chemical hydration to anticipate structural *** reversible and irreversible contributions that occur throughout the build-up,breakdown,and hydration are defined based on the proposed structural ***,detailed parametric studies are conducted to evaluate the impact of model *** is revealed that the proposed model is in good agreement with the experimental results,and it effectively characterizes the structural build-up of 3D printable concrete.

关键词： structural build-up rheology thixotropy 3D printable concrete kinetics theory ultra high performance concrete

Numerical modelling of post-failure behaviors of coal specimens

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Journal of Rock Mechanics and Geotechnical Engineering 2024年第2期16卷 514-531页

作者： Ajeet Yadav Bhaskara Behera Gauri shankar Prasad Singh Sanjay Kumar Sharma Department of Mining Engineering Indian Institute of Technology(Banaras Hindu University)VaranasiUttar Pradesh221005India

A modelling approach consisting of best-fit relations to estimate the post-yield strength parameters is presented for simulating post-peak behavior beyond the point of residual strength of coal pillars having different w/h *** model was developed based on back-analysis of the complete stress-strain behavior of specimens belonging to six different Indian coal seams with different w/h ratios of 0.5 *** was found that the simultaneous degradation of the cohesion and friction angle of the Mohr-Coulomb rock material characterizes the post-peak strength behavior of the *** resulting expressions are simplistic as they require parameters that can be easily determined using uniaxial and triaxial compression ***,the developed model was validated by simulating the triaxial tests of coal specimens with different sizes under varying confining stresses and comparing its findings with the published test *** study showed that its implementation in the numerical model could reproduce laboratory-observed mechanical response,deformation behavior,and failure mechanism very closely.

关键词： Strain softening Dilatancy Interface Shape effect Residual strength

Optimization of variables and assessment of in-vitro and in-vivo antihyperlipidemic activity of Eudragit RS nanoparticles containing simvastatin

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Particuology 2024年第7期90卷 189-198页

作者： Bina Gidwani Vishal Jain Veenu Joshi Ravindra Kumar Pandey Shiv shankar Shukla Amber Vyas Columbia Institute of Pharmacy Raipur(C.G.)India University Institute of Pharmacy Pt Ravishankar Shukla UniversityRaipur(C.G.)India Center for Basic Science and Research Pt Ravishankar Shukla UniversityRaipur(C.G.)India

Simvastatin, a BCS class II drug, is associated with poor aqueous solubility, first-pass metabolism and short half-life. In the present work, nanoparticles were prepared and evaluated. Optimization of formulation and process parameters was done through the use of independent and dependent variables. Preliminary studies were done to determine suitable range of the concentration of Eudragit polymer (10%–30%) and the ratio of drug to polymer (1:1 to 1:5) for the formation of nanoparticles by emulsification and a solvent evaporation technique. Results revealed that the mean size of nanoparticles was affected by stirring speed from 5000 RPM, 8000 RPM, and 12000 RPM. The results of increase in association efficiency and percent yield with increase in amount of drug from 100 mg, 150 mg, and 200 mg in selected range were observed. In-vitro release studies showed that two formulations possess highest initial burst and slow sustained drug release. There was 2.93-fold decrease in total cholesterol and 3.27-fold increases in triglyceride level during in-vivo study.

关键词： Simvastatin Eudragit RS 100 Nanoparticles Hyperlipidemia

Gas hydrate saturation from NGHP 02 LWD data in the Mahanadi Basin

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Energy Geoscience

Energy Geoscience 2024年第2期5卷 279-289页

作者： Uma shankar Pradeep Kumar Yadav Sneha Devi Udham Singh Yadav Department of Geophysics Institute of ScienceBHUVaranasi221005India Oil and Natural Gas Corporation Ltd. Gas Hydrate Research&Technology Centre(GHRTC)Panvel410221Navi MumbaiIndia

During the Indian National Gas Hydrate Program(NGHP)Expedition 02,Logging-while-drilling(LWD)logs were acquired at three sites(NGHP-02-11,NGHP-02-12,and NGHP-02-13)across the Mahanadi Basin in area *** applied rock physics theory to available sonic velocity logs to know the distribution of gas hydrate at site NGHP-02-11 and *** physics modeling using sonic velocity at well location shows that gas hydrate is distributed mainly within the depth intervals of 150-265 m and 100 -215 mbsf at site NGHP-02-11 and NGHP-02-13,respectively,with an average saturation of about 4%of the pore space and the maximum concentration of about 40%of the pore space at 250 m depth at site NGHP-02-11,and at site NGHP-02-13 an average saturation of about 2%of the pore space and the maximum concentration of about 20%of the pore space at 246 m depth,as gas hydrate is distributed mainly within 100-246 mbsf at this *** of gas hydrate estimated from the electrical resistivity method using density derived porosity and electrical resistivity logs from Archie's empirical formula shows high saturation compared to that from the sonic ***,estimates of hydrate saturation based on sonic P-wave velocity may differ significantly from that based on resistivity,because gas and hydrate have higher resistivity than conductive pore fluid and sonic P-wave velocity shows strong effect on gas hydrate as a small amount of gas reduces the velocity significantly while increasing velocity due to the presence of *** site NGHP-02-11,gas hydrate saturation is in the range of 15%e30%,in two zones between 150-180 and 245-265 *** NGHP-02-012 shows a gas hydrate saturation of 20%e30%in the zone between 100 and 207 *** NGHP-02-13 shows a gas hydrate saturation up to 30%in the zone between 215 and 246 *** observations from rock physics modeling and Archie’s approximation show the gas hydrate concentrations are relatively low(<4%of the pore space)at the sites of the

关键词： Mahanadi Basin Gas hydrate Sonic log Effective medium modeling Electrical resistivity log Archie’s analysis Gas hydrate saturation