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In Situ TiC/FeCrNiCu High-Entropy Alloy Matrix Composites:Reaction Mechanism,Microstructure and Mechanical Properties

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Acta Metallurgica Sinica(English Letters) 2020年第8期33卷 1091-1102页

作者： Hao Wu Si-Rui Huang Cheng-Yan zhu Ji-Feng Zhang he-guo zhu Zong-Han Xie College of Materials Science and Engineering Nanjing University of Science and TechnologyNanjing 210094China School of Mechanical Engineering University of AdelaideSA 5005Australia School of Engineering Edith Cowan UniversityJoondalupWA 6027Australia

In situ TiC particles-reinforced FeCrNiCu high-entropy alloy matrix composites were prepared by vacuum induction melting *** reaction mechanisms of the mixed powder(Ti,Cu and C)were analyzed,and the mechanical properties of resultant composites were ***4Tiwere formed in the reaction of Cu and Ti when the temperature rose to 1160 *** the temperature further increased to 1182 K,newly formed Cu4Tireacted with C to give rise to TiC particles as reinforcement *** apparent activation energy for these two reactions was calculated to be 578.7 kJ/mol and 1443.2 kJ/mol,*** hardness,tensile yield strength and ultimate tensile strength of the 15 vol%TiC/FeCrNiCu composite are 797.3 HV,605.1 MPa and 769.2 MPa,respectively,representing an increase by 126.9%,65.9%and 36.0%as compared to the FeCrNiCu high-entropy base alloy at room ***,the elongation-to-failure is reduced from 21.5 to 6.1%with the formation of TiC *** was revealed that Orowan mechanism,dislocation strengthening and load-bearing effect are key factors responsible for a marked increase in the hardness and strength of the high-entropy alloy matrix composites.

关键词： High-entropy alloy matrix composite TiC particle Reaction mechanism Mechanical properties Strengthening mechanism

Effect of vanadium content on microstructure and properties of in situ TiC reinforced V_(x)FeCoNiCu multi-principal-element alloy matrix composites

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Journal of Iron and Steel Research International 2021年第11期28卷 1471-1480页

作者： Chun-lei Tu Xiao-dong Sun Jie Li he-guo zhu Xiang-dong Li College of Mechanical Engineering Southeast UniversityNanjing 210094JiangsuChina Special Equipment Safety Supervision Inspection Institute of Jiangsu Province Nanjing 210036JiangsuChina College of Materials Science and Engineering Nanjing University of Science and TechnologyNanjing 210094JiangsuChina

V_(x)FeCoNiCu high entropy alloy matrix composites reinforced by in situ TiC particles(10 vol.%),i.e.,V_(x)FeCoNiCu/TiC composites,were fabricated from V–Fe–Co–Ni–Cu–Ti–C system using vacuum inductive melting *** the content of vanadium increasing,the size of TiC particles decreased ***,vanadium agglomeration occurred *** reaction mechanism of the mixed powder(Fe,V,Ti and C)and the mechanical properties of obtaining V_(x)FeCoNiCu/TiC composites were *** was found that three reactions occurred(Fe-Ti-FeTi-Fe_(2)Ti,FeTi-Fe_(2)Ti-Fe-Ti and Ti-C-TiC)in the heating *** apparent activation energy for these three reactions was calculated and found to be 26.4,698.3 and 1879.0 kJ/mol,*** room temperature,tensile strength and elongation increased first and then decreased with the increase in vanadium content and the microhardness increased *** maximum tensile strength of the composites was determined to be 666 MPa,representing a 17.7%increase over that of FeCoNiCu/TiC high entropy alloy composites.

关键词： High entropy alloy matrix composite Vacuum inductive melting Reaction mechanism Apparent activation energy Tensile strength

Buried interface bridging for inverted cesium-formamidinium triiodide perovskite solar cells with long operational stability

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Science China Chemistry 2025年第1期68卷 163-173页

作者： Chenhui Zhang Chunjun Liang Fulin Sun Ting zhu Xinghai Huang Yuzhu guo Xinyu guo Kunyang Ge Dan Li Fangtian You Zhiqun he Key Laboratory of Luminescence and Optical Information Ministry of Education Institute of Optoelectronic TechnologyBeijing Jiaotong University Department of Physics School of Physical Science and Engineering Beijing Jiaotong University

In the field of perovskite solar cells(PSCs), the research on defects in the buried interface has been relatively limited due to its non-exposure; however, this interface significantly impacts the performance enhancement of inverted PSCs. This study employs phenylethylammonium chloride(PEACl) molecules as a buffer layer to modify the buried interface of p-i-n structured PSCs,aiming to enhance the uniformity of self-assembled monolayers(SAMs) and facilitate the uniform nucleation and growth of perovskite films on the substrate. Furthermore, the introduction of the PEACl buffer layer effectively passivates defects at the bottom of the perovskite layer and notably enhances the crystal quality of the perovskite film by mitigating residual stress,thereby reducing nonradiative recombination loss. Following these optimizations, the MA-free PSCs treated with PEACl achieve a power conversion efficiency(PCE) of 24.11%, with significant improvements in storage, thermal stability, and operational stability. Particularly noteworthy is the device's performance in an unencapsulated state, whereas after 1,500 hours of continuous light operation stability testing, it retains 97% of its original efficiency. This study not only enriches the systematic understanding of the characteristics of the buried interface in PSCs but also contributes significantly to advancing the commercial production of perovskite photovoltaic technology.

关键词： defect-induced recombination buried interfaces inverted perovskite solar cells crystallization lattice mismatch

Determination of the number of atoms of the long-lived nuclide ^(126)Sn by γ-ray spectrometry

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Chinese Physics C 2010年第1期34卷 143-147页

作者： SheN Hong-Tao JIANG Shan he Ming DONG Ke-Jun LI Chao-Li WANG Xiang-Gao he guo zhu GONG Jie LU Li-Yan LI Shi-zhuo ZHANG Da-Wei SHI guo-zhu HUANG Chun-Tang WU Shao-Lei WU Shao-Yong Department of Nuclear Physics China Institute of Atomic Energy College of Physical Science and Engineering Technology Guangxi University

By using HPGe γ-ray spectrometry, the activity of the long-lived fission product 126Sn in a SnOB2 sample was measured. The number of 126Sn atoms and the ratio of 126Sn to Sn were calculated based on the half-life value of 2.35×105a and the chemical stoichiometry. The result of the ratio of 126Sn to Sn, （1.033±0.037）×10-8, is consistent with the results measured by the accelerator mass spectrometry （AMS） within uncertainty limits, which confirms our procedures in the measurement of 126Sn by AMS and lays a foundation for the AMS measurement of 126Sn at much lower levels.

关键词： 126Sn activity measurement γ-ray spectrometry AMS

Sequence-activated chemiluminescence probes: programmable illumination for high-contrast in vivo sensing and imaging

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Science China Chemistry 2025年第1期68卷 26-34页

作者： Yutao Zhang Juan Li Wei-Hong zhu Zhiqian guo Shanghai Key Laboratory of Functional Materials Chemistry Joint International Research Laboratory of Precision Chemistry and Molecular Engineering Institute of Fine Chemicals School of Chemistry and Molecular Engineering East China University of Science and Technology State Key Laboratory of Bioreactor Engineering Shanghai Frontier Science Research Base of Optogenetic Techniques for Cell MetabolismEast China University of Science & Technology

Sequence-activated chemiluminescence(CL) technique offers a unique approach to detecting specific biomolecules or cellular events with high sensitivity and spatial resolution. The fundamental principle behind sequence-activated CL probes involves tailoring highly-controllable CL signals in response to specific sequences or events of interest, thus enabling high-contrast signals under complex physiological conditions. This sequential activation could be triggered by enzymes, reactive oxygen species(ROS), biothiols or changes in the microenvironment. These unique sequence-activated CL probes bestow several advantages, including minimal background, deep-tissue penetration, and the ability of non-invasive or minimally invasive detection. The sequence-activated CL techniques represent a significant advancement in molecular imaging and diagnostics. In this mini-review, we focus on the latest developments in sequential CL probes, addressing the technical challenges and discussing the future trajectory by harnessing CL signaling and molecular recognition.

关键词： chemiluminescnece sequence-activation in-vivo bioimaging cyclic peroxide

Practical approach for detecting k-nonseparability of multipartite quantum states

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Science China(Physics,Mechanics & Astronomy) 2025年第1期Mechanics & Astronomy) .卷 32-48页

作者： Jie guo Jinchuan Hou Xiaofei Qi Kan he College of Mathematics Taiyuan University of Technology School of Mathematics and Statistics Shanxi University Key Laboratory of Complex Systems and Data Science of Ministry of Education Shanxi University

The instantaneous detection of entanglement in quantum states poses a significant challenge in the fields of quantum computation and quantum information, and there are no practical methods or tools to complete this task satisfactorily so far. We propose a sufficient and necessary criterion of k-nonseparability for any n-partite finite or infinite dimensional systems, 2 ≤ k ≤ n. This criterion serves as the foundation for a practical scheme designed to detect entanglement and k-nonseparability across multipartite finite-dimensional systems. To exemplify the application of our scheme, we have developed a software tool that facilitates swift and precise identification of entanglement, k-nonseparability, and genuine entanglement within n-qubit systems, specifically tailored for systems with 2 ≤ n ≤ 4.

关键词： multipartite systems entanglement states entanglement witnesses ${\bm~k}$-nonseparability

Mechanical properties and fracture mechanism of as-cast MnFeCoCuNix high-entropy alloys

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Transactions of Nonferrous Metals Society of China 2021年第1期31卷 222-231页

作者： Cheng-yan zhu Hao WU he-guo zhu Xiang-dong LI Chun-lei TU Zong-han XIE School of Materials Science and Engineering Nanjing University of Science and TechnologyNanjing 210094China School of Mechanical Engineering Southeast UniversityNanjing 211189China School of Mechanical Engineering Nanjing University of Science and TechnologyNanjing 210094China School of Mechanical Engineering University of AdelaideSA 5005Australia School of Engineering Edith Cowan UniversityWA 6027Australia

MnFeCoCuNix high-entropy alloys(heAs)with different Ni contents were fabricated by vacuum induction *** and SEM−EDS were used to analyze the phase constitution and structure,and the tensile properties of the samples were determined using a universal tensile *** results show that the heAs consist of a dual-phase structure,in which FCC1 phase is rich in Fe and Co,while the FCC2 phase has high contents of Cu and *** Ni content increases,the segregation of Cu decreases,accompanied by the decrease of FCC2 ***,the tensile strength of the heAs increases first and then decreases,and the elongation increases *** is attributed to the combined effect of interface strengthening and solid solution *** in-situ stretched MnFeCoCuNi0.5 alloy shows obvious neck shrinkage during the tensile fracture *** the initial deformation stage,the slip lines show different morphologies in the dual-phase ***,in the later stage,the surface slip lines become longer and denser due to the redistribution of atoms and the re-separation of the dissolved phase.

关键词： high-entropy alloys dual-phase structure mechanical properties in-situ stretching fracture mechanism

Defect Engineering with Rational Dopants Modulation for High‑Temperature Energy Harvesting in Lead‑Free Piezoceramics

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Nano-Micro Letters 2025年第3期17卷 87-101页

作者： Kaibiao Xi Jianzhe guo Mupeng Zheng Mankang zhu Yudong Hou Key Laboratory of Advanced Functional Materials Ministry of EducationCollege of Materials Science and EngineeringBeijing University of TechnologyBeijing 100124People’s Republic of China

High temperature piezoelectric energy harvester(HTPEH)is an important solution to replace chemical battery to achieve independent power supply of HT wireless ***,simultaneously excellent performances,including high figure of merit(FOM),insulation resistivity(ρ)and depolarization temperature(Td)are indispensable but hard to achieve in lead-free piezoceramics,especially operating at 250°C has not been reported ***,well-balanced performances are achieved in BiFeO3–BaTiO3 ceramics via innovative defect engineering with respect to delicate manganese *** to the synergistic effect of enhancing electrostrictive coefficient by polarization configuration optimization,regulating iron ion oxidation state by high valence manganese ion and stabilizing domain orientation by defect dipole,comprehensive excellent electrical performances(Td=340°C,ρ250°C>10^(7)Ωcm and FOM_(250°C)=4905×10^(–15)m^(2)N^(−1))are realized at the solid solubility limit of manganese *** HT-PEHs assembled using the rationally designed piezoceramic can allow for fast charging of commercial electrolytic capacitor at 250°C with high energy conversion efficiency(η=11.43%).These characteristics demonstrate that defect engineering tailored BF-BT can satisfy high-end HT-PEHs requirements,paving a new way in developing selfpowered wireless sensors working in HT environments.

关键词： Lead-free piezoceramic Defect engineering Dopants modulation High-temperature Piezoelectric energy harvester

Dip2a regulates stress susceptibility in the basolateral amygdala

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Neural Regeneration Research 2025年第6期20卷 1735-1748页

作者： Jing Li Zixuan he Weitai Chai Meng Tian Huali Yu Xiaoxiao he Xiaojuan zhu Key Laboratory of Molecular Epigenetics Ministry of Education Institute of Genetics and CytologyNortheast Normal UniversityChangchunJilin ProvinceChina

Dysregulation of neurotransmitter metabolism in the central nervous system contributes to mood disorders such as depression, anxiety, and post–traumatic stress disorder. Monoamines and amino acids are important types of neurotransmitters. Our previous results have shown that disco-interacting protein 2 homolog A(Dip2a) knockout mice exhibit brain development disorders and abnormal amino acid metabolism in serum. This suggests that DIP2A is involved in the metabolism of amino acid–associated neurotransmitters. Therefore, we performed targeted neurotransmitter metabolomics analysis and found that Dip2a deficiency caused abnormal metabolism of tryptophan and thyroxine in the basolateral amygdala and medial prefrontal cortex. In addition, acute restraint stress induced a decrease in 5-hydroxytryptamine in the basolateral amygdala. Additionally, Dip2a was abundantly expressed in excitatory neurons of the basolateral amygdala, and deletion of Dip2a in these neurons resulted in hopelessness-like behavior in the tail suspension test. Altogether, these findings demonstrate that DIP2A in the basolateral amygdala may be involved in the regulation of stress susceptibility. This provides critical evidence implicating a role of DIP2A in affective disorders.

关键词： 5-hydroxytryptamine acute restraint stress basolateral amygdala CaMKII neurons DIP2A metabolomics neurotransmitters principal component analysis stress susceptibility tryptophan