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Eco-friendly polysaccharide coatings for antifouling and dragreduction and potential application for marine devices

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Friction 2024年第4期12卷 726-744页

作者： Hao YANG Liguo QIN Wenhui ZHAO Fagla Jules MAWIGNON Hui GUO Yongkang WU Yali ZHANG Guangneng DONG Key Laboratory of Education Ministry for Modern Design and Rotor-Bearing System Institute of Design Science and Basic ComponentsSchool of Mechanical EngineeringXi’an Jiaotong UniversityXi’an 710049China Key Laboratory of Biomedical Information of Ministry of Education School of Life Science and TechnologyXi’an Jiaotong UniversityXi’an 710049China Department of Endocrinology First Affiliated Hospital of Medical CollegeXi'an Jiaotong UniversityXi’an 710061China

Traditional antifouling agents usually have a certain toxic effect on marine environments and non-target organisms.In this study,Dictyophora indusiata polysaccharide(DIP)was applied as a natural antifouling surface modifier to prepare the surface coating for marine antifouling.Three DIP coatings were prepared:D.indusiata spore polysaccharide(DISP),D.indusiata volva polysaccharide(DIVP),and D.indusiata embryonic body polysaccharide(DIEP).The antifouling,tribological,and anticorrosion behavior of the coatings were examined.Results revealed that the three kinds of DIP coatings had excellent antifouling properties,which could effectively prevent the adhesion of Chlorella and the attachment of water-based and oily stains on the surface.Additionally,the coatings showed great mechanical stability and could maintain an extremely low coefficient of friction(COF<0.05)after continuous wear.The drag reduction rate of the coated surfaces reached 5%,showing a powerful lubrication performance.Furthermore,the DIP coatings presented an outstanding corrosion resistance,where the equivalent circuit impedances were 4-9 orders of magnitude higher than the control groups.This research showed a promising prospect of surface coating fabrication with DIP for marine devices to achieve the purpose of antifouling and drag reduction.

关键词： Dictyophora indusiata polysaccharide(DIP)coating antifouling anticorrosion lubrication and drag reduction

Origin of the tribofilm from MoS_(2) nanoparticle oil additives: Dependence of oil film thickness on particle aggregation in rolling point contact

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Friction 2021年第6期9卷 1436-1449页

作者： Hongxing WU Liping WANG Guangneng DONG State Key Laboratory of Solidification Processing Center of Advanced Lubrication and Seal MaterialsNorthwestern Polytechnical UniversityXi’an 710072China Petro China Lanzhou Lubricating Oil R&D Institute Lanzhou 730060China Key Laboratory of Education Ministry for Modern Design and Rotor-Bearing System Xi'an Jiaotong UniversityXi'an 710049China

The lubrication effectiveness of MoS_(2) nanoparticles as an oil additive remains unclear,restricting its application in industry to reduce friction.The goal of this work was to explore the lubrication mechanism of MoS_(2) nanoparticles as an oil additive.In this study,the oil film thickness behaviors of MoS_(2) nanoparticles in poly-alpha olefin(PAO4)base oil,PAO4 with 3 wt%dispersant(polyisobutyleneamine succinimide,PIBS),and 0W20 engine oil were investigated using an elastohydrodynamic lubrication(EHL)testing machine.Following the EHL tests,the flow patterns around the contact area and the tribofilm covering rate on contact area were studied using optical microscopy to understand the lubrication mechanism.The results indicate that both the dispersant and nanoparticle aggregation significantly affected the oil film thickness.The expected oil film thickness increase in the case of 0.1 wt%MoS_(2) in PAO4 base oil was obtained,with an increase from 30 to 60 nm over 15 min at a velocity of 50 mm/s.Flow pattern analysis revealed the formation of particle aggregation on the rolling path when lubricated with 0.1 wt%MoS_(2),which is associated with a tribofilm coverage rate of 41.5%on the contact area.However,an oil film thickness increase and particle aggregation were not observed during the tests with 0.1 wt%MoS_(2) blended with 3 wt%PIBS as the dispersant in PAO4 base oil,and for 0.75 wt%MoS_(2) in 0W20 engine oil.The results suggest that nanoparticles responsible for tribofilm formation originated from aggregates,but not the well-dispersed nanoparticles in point contact.This understanding should aid the advancement of novel lubricant additive design.

关键词： nanoparticle lubrication oil film thickness flow pattern particle aggregation

人工关节材料表面仿生树状分叉网络的润滑研究

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西安交通大学学报 2022年第2期56卷 66-73页

作者：任荣杰董光能西安交通大学现代设计及转子轴承系统教育部重点实验室西安710049

为提高人工关节假体材料(钛合金/超高分子量聚乙烯配副)的耐磨性,研究了材料仿生树状分叉网络织构的液体铺展流动性能与摩擦学性能。根据分支数与分支角不同,分别设计了3类仿生树状分叉网络织构(十字型网络、T型网络、Y型网络),每类树... 详细信息

为提高人工关节假体材料(钛合金/超高分子量聚乙烯配副)的耐磨性,研究了材料仿生树状分叉网络织构的液体铺展流动性能与摩擦学性能。根据分支数与分支角不同,分别设计了3类仿生树状分叉网络织构(十字型网络、T型网络、Y型网络),每类树状网络织构分别制备成织构率为10%、15%、20%的3种试样。通过试验,评价了树状网络的液体铺展流动性和摩擦学性能,结果发现:3种织构表面均可以降低瞬时接触角和实现液体完全铺展,并具有较好的减摩性能;Y型网络织构具有最好的液体铺展流动性能,2μL的液体在10%织构率时瞬时接触角为23.37°,仅0.95 s可以完全铺展;T型网络织构在15%织构率时摩擦系数仅为0.077,较原始表面降低了38%。研究内容对人工关节自润滑减摩设计具有重要参考意义。

关键词：人工关节树状分叉织构钛合金接触角摩擦学性能

Dry Friction and Wear Characteristics of Impregnated Graphite in a Corrosive Environment

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Chinese Journal of Mechanical Engineering 2014年第5期27卷 965-971页

作者： JIA Qian YUAN Xiaoyang ZHANG Guoyuan dong guangneng ZHAO Weigang Key Laboratory of Education Ministry for Modem Design and Rotor-bearing System Xi'an Jiaotong University School of Electromechanical Engineering Xidian University Xi'an Aerospace Propulsion Institute China Aerospace Science and Technology Corporation

Tribological properties of impregnated graphite are greatly influenced by preparation technology and working conditions and it’s highly susceptible to corrosion environmental impacts,but the experimental research about it are few.In this paper,three kinds of impregnated graphite samples are prepared with different degree of graphitization,the tribological properties of these samples in the dry friction environment and in a corrosive environment are analyzed and contrasted.The tribo-test results show that the friction coefficient of samples is reduced and the amount of wear of samples increase when the graphitization degree of samples increases in dry friction condition.While in a corrosive environment（samples are soaked N2O4）,the friction coefficient and amount of wear are changed little if the graphitization degree of samples are low.If the degree of graphitization increase,the friction coefficient and amount of wear of samples increase too,the amount of wear is 2 to 3 times as the samples tested in the non-corrosive environment under pv value of 30MPa？m/s.The impregnated graphite,which friction coefficient is stable and graphitization degree is in mid level,such#2,is more appropriate to have a work in the corrosion conditions.In this paper,preparation and tribological properties especially in corrosive environment of the impregnated graphite is studied,the research conclusion can provide an experimental and theoretical basis for the selection and process improvement of graphite materials,and also provide some important design parameters for contact seal works in a corrosive environment.

关键词： corrosive environment impregnated graphite graphitization dry friction coefficient of friction amount of wear

Tribological behaviors of spot-textured TiN coatings on M2 high-speed steel under boundary lubricated conditions

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Journal of University of Science and Technology Beijing 2007年第4期14卷 350-355页

作者： Guangneng DONG Meng Hua Jian Li Hing-Yin Ma Youbai Xie Lubrication Theory and Bearing Institute Key Laboratory of the Education Ministry for Modern Design and Rotor-Bearing System Xi＇an Jioatong University Xi＇an 710049 China Department of Manufacturing Engineering and Engineering Management City University of Hong Kong 83 Tat Chee Avenue Kowloon Tong Kowloon Hong Kong China Wuhan Research Institute of Materials Protection Wuhan 430030 China

The effect of sliding duration on the tribological behaviors of spot patterned coatings was investigated. Two patterns based on physical vapor deposition （PVD） TiN coatings were used, such as, in-lined （IN） and staggered （ST） spots. The tribological behaviors were evaluated by using a Cameron-Plint wear test rig. The M2 steel discs deposited TiN coatings with IN and ST patterns slid against the ASSAB 17 tool steel pins at a speed of 0.23 m/s, in Shell Tellus T32 lubricant and were loaded with 900 N. The testing results on disc specimens with two types of PVD TiN spot patterns, all coated with a bias voltage of-180 V and slid for 4, 8 and 11 h respectively, were presented. The results revealed that the in-lined coatings possessed relatively better wear behaviors than the staggered pattern coatings. Mechanisms for such superiority and for the cause of peeling were discussed. A relevant design approach was suggested for the application of such patterned coatings.

关键词： vapor deposited coating texture friction wear boundary lubrication

Molecular dynamics simulation of the deposition process of hydrogenated diamond-like carbon (DLC) films

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Chinese Science Bulletin 2008年第7期53卷 1094-1099页

作者： ZHANG Yujun dong guangneng MAO JunHong XIE YouBai Theory of Lubrication and Bearing Institute Key Laboratory of Education Ministry for Modern Design and Rotor-Bearing System Xi'an Jiaotong University Xi'an 710049 China

The deposition process of hydrogenated diamond-like carbon (DLC) film greatly affects its frictional properties. In this study, CH3 radicals are selected as source species to deposit hydrogenated DLC films for molecular dynamics simulation. The growth and structural properties of hydrogenated DLC films are investigated and elucidated in detail. By comparison and statistical analysis, the authors find that the ratio of carbon to hydrogen in the films generally shows a monotonously increasing trend with the increase of impact energy. Carbon atoms are more reactive during deposition and more liable to bond with substrate atoms than hydrogen atoms. In addition, there exists a peak value of the number of hydrogen atoms deposited in hydrogenated DLC films. The trends of the variation are opposite on the two sides of this peak point, and it becomes stable when impact energy is greater than 80 eV. The average relative density also indicates a rising trend along with the increment of impact energy, while it does not reach the saturation value until impact energy comes to 50 eV. The hydrogen content in source species is a key factor to determine the hydrogen content in hydrogenated DLC films. When the hydrogen content in source species is high, the hydrogen content in hydrogenated DLC films is accordingly high.

关键词：分子动力学沉积程序氢化作用 DLC 薄膜

钝化处理对Co-Cr-Mo合金摩擦性能的影响

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真空科学与技术学报 2014年第11期34卷 1197-1201页

作者：郭飞飞董光能西安交通大学润滑理论与轴承研究所西安710049

利用高温钝化处理方法,在Co-Cr-Mo合金表面得到钝化膜。标准摩擦试验考察了不同温度钝化试样在牛血清白蛋白溶液润滑下的摩擦学特性。表面轮廓仪、硬度测试仪、扫描电镜及X-射线衍射光谱仪分别表征了钝化膜的表面形貌、硬度及化学组成物... 详细信息

利用高温钝化处理方法,在Co-Cr-Mo合金表面得到钝化膜。标准摩擦试验考察了不同温度钝化试样在牛血清白蛋白溶液润滑下的摩擦学特性。表面轮廓仪、硬度测试仪、扫描电镜及X-射线衍射光谱仪分别表征了钝化膜的表面形貌、硬度及化学组成物质,并探讨了摩擦磨损机理。结果表明:钝化后试样表面均有尖晶石状Cr2O3晶体生长现象。钝化膜厚度及表面粗糙度、硬度均随钝化温度升高而增大。由于试样钝化后硬度增加,接触面间摩擦剪切力减小,从而引起摩擦系数值的降低。钝化试样表面耐磨性提高,其磨损形貌受到初始表面粗糙度及钝化膜与基材的结合力的综合影响。

关键词：钝化膜高温摩擦磨损 Co-Cr-Mo合金

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混合弹流润滑系统的建模与摩擦学特性研究

西安交通大学学报 2018年第1期52卷 107-114页

作者：董国忠张辉李月董光能西安交通大学现代设计及转子轴承系统教育部重点实验室西安710049 株洲中车时代电气股份有限公司湖南株洲412001

为了研究粗糙表面微凸体对混合弹流润滑区摩擦学特性的影响,建立了考虑粗糙表面微凸体的弹流润滑数学模型,可呈现粗糙表面的局部接触状态。通过生成虚拟粗糙表面,分别利用K-E弹塑性接触模型和平均流量雷诺方程计算微凸体接触压力与流体... 详细信息

为了研究粗糙表面微凸体对混合弹流润滑区摩擦学特性的影响,建立了考虑粗糙表面微凸体的弹流润滑数学模型,可呈现粗糙表面的局部接触状态。通过生成虚拟粗糙表面,分别利用K-E弹塑性接触模型和平均流量雷诺方程计算微凸体接触压力与流体动压力,并且利用快速傅里叶变换技术计算基体的弹性变形量;通过绘制润滑系统的Stribeck曲线,研究了虚拟微凸体、名义载荷、综合粗糙度和微凸体曲率半径对弹流润滑摩擦学特性的影响。结果表明:微凸体的接触压力产生基体弹性变形,使膜厚增加,导致流体动压力减小,微凸体承载比和摩擦因数增大;名义载荷增加导致低速时摩擦因数变小,润滑状态在更低速条件下从边界润滑过渡到混合润滑;综合粗糙度的减小会使Stribeck曲线向左移动;微凸体曲率半径的增大仅使润滑状态加快从边界润滑过渡到混合润滑,然而对从混合区域过渡到弹流区域几乎没有影响。

关键词：摩擦学混合弹流润滑粗糙表面建模

氧化石墨烯/聚乙二醇复合材料在人工关节材料上的润滑性能

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复合材料学报 2017年第11期34卷 2598-2604页

作者：任姗姗陆海林董光能西安交通大学机械工程学院西安710049

通过销盘试验分析氧化石墨烯(GO)、聚乙二醇(PEG)和不同比例的GO/PEG复合材料的摩擦学性能,考察GO增强PEG在人工关节材料UHMWPE-CoCrMo配副上的润滑效果,并利用FTIR、XRD、拉曼光谱等研究了GO/PEG复合材料的结构和性能。结果表明:混合... 详细信息

通过销盘试验分析氧化石墨烯(GO)、聚乙二醇(PEG)和不同比例的GO/PEG复合材料的摩擦学性能,考察GO增强PEG在人工关节材料UHMWPE-CoCrMo配副上的润滑效果,并利用FTIR、XRD、拉曼光谱等研究了GO/PEG复合材料的结构和性能。结果表明:混合比例为0.85wt%GO与40wt%PEG的GO/PEG复合材料在4.2 MPa加载载荷、0.024m/s的滑动速度条件下,平均摩擦系数为0.015,具有良好的润滑效果;GO均匀地分散在PEG溶液中,组分间较强的界面相互作用协同增强了GO/PEG复合材料的润滑性能。

关键词：氧化石墨烯聚乙二醇复合材料人工关节润滑