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Chemical modification of barite for improving the performance of weighting materials for water-based drilling fluids

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Petroleum Science 2024年第1期21卷 551-566页

作者： Li-Li Yang Ze-Yu Liu Shi-bo Wang Xian-Bo He guan-cheng jiang Jie Zhang MOE Key Laboratory of Petroleum Engineering State Key Laboratory of Petroleum Resources and ProspectingChina University of Petroleum(Beijing)Changping DistrictBeijing102249China MOE Key CNPC Drilling Research Institute Changping DistrictBeijing102206China

With increasing drilling depth and large dosage of weighting materials,drilling fluids with high solid content are characterized by poor stability,high viscosity,large water loss,and thick mud cake,easier leading to reservoir damage and wellbore *** this paper,micronized barite(MB)was modified(mMB)by grafting with hydrophilic polymer onto the surface through the free radical polymerization to displace conventional API barite *** suspension stability of water-based drilling fluids(WBDFs)weighted with API barite:mMB=2:1 in 600 g was significantly enhanced compared with that with API barite/WBDFs,exhibiting the static sag factor within 0.54 and the whole stability index of *** viscosity and yield point reached the minimum,with a reduction of more than 40%compared with API barite only at the same *** multi-stage filling and dense accumulation of weighting materials and clays,filtration loss was decreased,mud cake quality was improved,and simultaneously it had great reservoir protection performance,and the permeability recovery rate reached 87%.In addition,it also effectively improved the lubricity of *** sticking coefficient of mud cake was reduced by 53.4%,and the friction coefficient was ***,mMB can serve as a versatile additive to control the density,rheology,filtration,and stability of WBDFs weighted with API barite,thus regulating comprehensive performance and achieving reservoir protection *** work opened up a new path for the productive drilling of extremely deep and intricate wells by providing an efficient method for managing the performance of high-density WBDFs.

关键词： Drilling fluids Weighting materials Filtration control Reservoir protection Stability property

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Natural rubber latex as a potential additive for water-based drilling fluids

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Petroleum Science 2024年第4期21卷 2677-2687页

作者： Jun Yang guan-cheng jiang Jing-Tian Yi Yin-Bo He Li-Li Yang Teng-Fei Dong Guo-Shuai Wang College of Petroleum Engineering China University of Petroleum (Beijing) National Engineering Research Center of Oil & Gas Drilling and Completion Technology Changqing Drilling General Company CNPC Chuanqing Drilling Engineering Company Limited

The environmental hazards and "carbon footprint" of oil and gas drilling can be significantly reduced by replacing traditional petroleum-based chemical additives with natural materials derived from plants and animals. This paper explored for the first time the interaction mechanism between natural rubber latex(NRL) and bentonite suspensions(BTs) through a series of characterization experiments, as well as the potential applications in water-based drilling fluids(WBDF). The gel viscoelasticity experiments showed that NRL could decrease the consistency coefficient(k) and flow index(n) of BTs, and enhance the shear thinning performance of BTs as pseudo-plastic fluids. In addition, 0.5 w/v% NRL not only increased the critical yield stress and strengthened the structural strength between the bentonite particles, but also facilitated the compatibility of pressure loss and flow efficiency. The evaluation of colloidal stability and WBDF performance indicated that NRL particles could promote the hydration and charge stability on the surface of BTs particles, and optimize the particle size distribution and flow resistance of WBDF under the "intercalation-exfoliation-encapsulation" synergistic interaction. Moreover, NRL can improve the rheological properties of WBDF at high temperatures(<150.C), and form a dense blocking layer by bridging and sealing the pores and cracks of the filter cake, which ultimately reduces the permeability of the cake and the filtration loss of WBDF.

关键词： Natural materials Water-based drilling fluids Natural rubber latex Bentonite suspensions Filtration loss

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A new environmentally friendly water-based drilling fluids with laponite nanoparticles and polysaccharide/polypeptide derivatives

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Petroleum Science 2022年第6期19卷 2959-2968页

作者： Xin-Liang Li guan-cheng jiang Yi Xu Zheng-Qiang Deng Kai Wang College of Chemistry and Chemical Engineering Southwest Petroleum UniversityChengdu610500SichuanChina College of Petroleum Engineering China University of Petroleum(Beijing)Beijing102249China Drilling Fluid Technology Service Corporation CNPC Chuanqing Drilling Engineering Company LimitedChengdu610051SichuanChina Changqing General Drilling Company CNPC Chuanqing Drilling Engineering Company LimitedXi’an710018ShaanxiChina

Considering the increasing environmental pressure,environmentally friendly and high-performance water-based drilling fluids(WBDFs)have been widely studied in recent years to replace the commonly used oil-based drilling fluids(OBDFs).However,few of these drilling fluids are entirely composed of natural materials,which makes it difficult to achieve real environmental *** laponite nanoparticles and various derivatives of natu ral mate rials,including cro sslinked starch,cellulose composite,gelatin ammonium salt,poly-l-arginine,and polyanionic cellulose,a kind of environmentally friendly water-based drilling fluid(EF-WBDF)was built for drilling in environment-sensitive *** properties of this EF-WBDF were evaluated by thermal stability tests on rheology,filtration,inhibition,and salt ***,biological toxicity,biodegradability,heavy mental content and wheat cultivation tests were conducted to investigate the environmental factor of *** showed that EF-WBDF displayed satisfactory thermal resistance up to 150℃,and the rheological properties did not suffer significant fluctuation,showing potential application in high-temperature *** optimal rheological model of EF-WBDF was Herschel-Bulkley *** EF-WBDF performed an eligible filtration of 14.2 mL at 150℃and a differential pressure of 3.5 *** fluid could still maintain colloidal stability after being contaminated by 7.5%NaCl or 0.5%CaC1_(2).Meanwhile,rather low clay swelling degree of 2.44 mm and high shale recovery of more than 95%ensured the inhibitive capability of ***,EF-WBDF presented a half maximal effective concentration(EC_(50))of51200 mg/L and a BOD/COD ratio of 47.55%,suggesting that EF-WBDF was non-toxic and easily *** wheat cultivated in EF-WBDF could grow healthily,beneficial for reducing the adverse impact on ecological *** formed EF-WBDF has a promising future for drilling in environment-sensitive and high-te

关键词： Water-based drilling fluids Environmental protection High-temperature resistance Laponite nanoparticles Natural materials Wellbore stability

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Double network self-healing hydrogel based on hydrophobic association and ionic bond for formation plugging

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Petroleum Science 2022年第5期19卷 2150-2164页

作者： Ying-Rui Bai Qi-Tao Zhang Jin-Sheng Sun guan-cheng jiang Kai-He Lv School of Petroleum Engineering China University of Petroleum(East China)Qingdao266580ShandongChina CNPC Engineering Technology R&D Company Limited Beijing102206China College of Petroleum Engineering China University of Petroleum(Beijing)Beijing102249China

Self-healing hydrogels have attracted tremendous attention in the field of oil and gas drilling and production engineering because of their excellent self-healing performance after physical *** this study,a series of double network self-healing(DN_(SA))hydrogels based on hydrophobic association and ionic bond were prepared for plugging pores and fractures in formations in oil and gas drilling and production *** mechanical,rheological,and self-healing properties of the DN_(SA)hydrogels were *** revealed that the DN_(SA)hydrogels exhibited excellent mechanical properties with a tensile stress of 0.67 MPa and toughness of 7069 kJ/cm^(3) owing to the synergistic effect of the double *** addition,the DN_(SA)hydrogels exhibited excellent compression resistance,notch insensitivity,and self-healing *** DN_(SA)-2 hydrogel was granulated and made into gel particles with different particle sizes and used as a plugging *** self-healing mechanism of DN_(SA)-2 hydrogel particles in fractures was explored,and it’s plugging effect on fractures of different widths and porous media of different permeabilities were *** results revealed that the plugging capacity of the DN_(SA)-2 hydrogel particles for a fracture with width of 5 mm and a porous medium with a permeability of 30μm^(2) was 3.45 and 4.21 MPa,respectively,which is significantly higher than those of commonly used plugging agents in the *** DN_(SA)hydrogels with excellent mechanical and self-healing properties prepared in this study will provide a new approach for applying hydrogels in oil and gas drilling and production engineering.

关键词： Self-healing hydrogel Hydrophobic association Ionic bond Mechanical property Rheological property Formation plugging

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Plugging performance and mechanism of an oil-absorbing gel for lost circulation control while drilling in fractured formations

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Petroleum Science 2022年第6期19卷 2941-2958页

作者： Ying-Rui Bai Li-Yao Dai Jin-Sheng Sun guan-cheng jiang Kai-He Lv Rong-Chao cheng Xiao-Sen Shang School of Petroleum Engineering China University of Petroleum(East China)Qingdao266580ShandongChina CNPC Engineering Technology R&D Company Limited Beijing102206China College of Petroleum Engineering China University of Petroleum(Beijing)Beijing102249China

Lost circulation of drilling fluid is one of the most common engineering problems in the drilling process of fractured *** this study,an oil-absorbing polymer gel synthesized using compound monomers with rigid and flexible chains was applied to control the oil-based drilling fluid loss while *** microstructure,oil-absorbing performance,and plugging performance the gel was investigated.A large number of dense pores on the surface of the gel were observed,which allowed the oil molecules to enter the internal space of the *** initial oil absorption capacity of the gel was fast,and it increased with the increase in the temperature and decrease in the particle size,reaching 20.93 g/g at140℃.At a high temperature of 140℃,the bearing pressure capacity of the gel formula containing particles of different particle sizes reached 7.6 MPa for a fracture of a width of 3 mm,showing that the oil-absorbing gel have excellent plugging performance at high *** mechanism of the gel was investigated through visualized fracture plugging *** show that the dynamic migratio n,particle-swelling,particle-bridging,particle-aggregation,deformation-filling,and compaction-plugging contribute to the whole lost circulation control process,reflecting that the plugging performance can be effectively enhanced by improving the aggregation and filling degrees of the gel with different particle sizes.

关键词： Lost circulation Oil-absorbing gel Oil absorption capacity Plugging mechanism Fractured formation

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Preparation and properties of magnesium oxysulfate cement and its application as lost circulation materials

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Petroleum Science 2021年第5期18卷 1492-1506页

作者： Kai-Xiao Cui guan-cheng jiang Li-Li Yang Zheng-Qiang Deng Lei Zhou State Key Laboratory of Petroleum Resources and Prospecting MOE Key Laboratory of Petroleum EngineeringChina University of Petroleum(Beijing)Beijing102249China CCDC Drilling Fluid Technical Service Company Chengdu610056SichuanChina Zhundong Drilling Company of CNPC Xibu Drilling Engineering Company Limited Karamay834000XinjiangChina

Loss of drilling fluids in large porous and fractured zones inevitably up-regulates the overall cost of *** a type of acid-soluble cement,magnesium oxysulfate(MOS)cement is arousing huge attention for the less hygroscopic nature and less damaging to steel casings compared with magnesium oxychloride(MOC)*** present study developed MOS cement as a fast setting,high strength and acid-soluble lost circulation material to reduce the problem of *** suggested in this study,a higher strength of MOS cement at 70℃could be achieved by elevating M_(g)O/MgSO_(4)·7 H_(2)O molar ratio or downregulating H_(2)O/MgSO_(4)·7 H_(2)O molar *** acid and borax could act as effective *** slurry based on MOS cement could effectively block the simulated porous loss zones exhibiting a diameter from 1.24 mm to 1.55 mm,as well as the fractured loss zones with a width from 2 mm to 5 mm and bearing a pressure difference up to 8 *** recovery test demonstrated that it facilitated future oil and gas *** successful field application in the Junggar Basin,Xinjiang,China verified the significant plugging effect of MOS cement for severe loss problems.

关键词： Magnesium oxysulfate cement Lost circulation material Severe loss Acid soluble plug Formation damage

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Subsection and superposition method for reservoir formation damage evaluation of complex-structure wells

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Petroleum Science 2023年第3期20卷 1843-1856页

作者： guan-cheng jiang Yi-Zheng Li Yin-Bo He Teng-Fei Dong Ke-Ming Sheng Zhe Sun Collge of Petroleum Engineering China University of Petroleum(Beijing)Bejing102249China State Key Laboratory of Petroleum Resources and Prospecting MOE Key Laboratory of Petroleum EngineeringChina Universityof Petroleum(Beijing)Beijing102249China College of Artificial Intelligence China University of Petroleum(Bejing)Beijing102249China Calgary Centre for Innovative Technology University of CalgaryCalgaryAB T2N 1N4Canada National Engineering Research Center of Oil&Gas Drilling and Completion Technology

Kinds of complex-structure wells can effectively improve production,which are widely ***,in the process of drilling and completion,complex-structure wells with long drilling cycle and large exposed area of reservoir can lead to the fact that reservoir near wellbore is more vulnerable to the working fluid invasion,resulting in more serious formation *** order to quantitatively describe the reservoir formation damage in the construction of complex-structure well,taking the inclined well section as the research object,the coordinate transformation method and conformal transformation method are given according to the flow characteristics of reservoir near wellbore in anisotropic *** the local skin factor in orthogonal plane of wellbore is *** the un-even distribution of local skin factor along the wellbore,the oscillation decreasing model and empirical equation model of damage zone radius distribution along the wellbore direction are established and then the total skin factor model of the whole well is superimposed to realize the reservoir damage evaluation of complex-structure *** the skin factor model with the production model,the production of complex-structure wells can be predicted more *** two field application cases show that the accuracy of the model can be more than 90%,which can also fully reflect the invasion characteristics of drilling and completion fluid in any well section of complex-structure wells in anisotropic reservoir,so as to further provide guidance for the scientific establish-ment of reservoir production system.

关键词： Complex-structure wells Reservoir formation damage Reservoir anisotropy Skin factor Production prediction model

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Eco-friendly aqueous foam stabilized by cellulose microfibers with great salt tolerance and high temperature resistance

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Petroleum Science 2023年第4期20卷 2499-2511页

作者： Li-Li Yang Xian-Bo He Yi-Xiu cheng guan-cheng jiang Ze-Yu Liu Shi-Bo Wang Shi-Xin Qiu Jian-Hua Wang Wei-Guo Tian MOE Key Laboratory of Petroleum Engineering State Key Laboratory of Petroleum Resources and EngineeringChina University of Petroleum(Beijing)Changping DistrictBeijing102249China Beijing National Laboratory for Molecular Sciences CAS Key Laboratory of Engineering PlasticsInstitute of Chemistry Chinese Academy of Sciences(CAS)Haidian DistrictBeijing100190China MOE Key CNPC Drilling Research Institute Changping DistrictBeijing102206China

A low-cost eco-friendly aqueous foam,especially the robust foam with great tolerance to high salinity and high temperature,is in great demand in the oil industry,e.g.,oil and gas well or geothermal well ***,an ultra-stable aqueous foam was developed using the biodegradable cellulose microfiber(CMF)as a foam *** foam stabilized by CMF shows excellent tolerance to the high concentration of NaCl(6.0 wt%)and CaCl_(2)(0.25 wt%)and the related drainage half-life times(T_(0.5))reach 1750 and 2340 s *** contrast,the foams without CMF are completely drained(T_(0.5)=0 s)when NaCl concentration is greater than 6.0 wt%or CaCl_(2) concentration is greater than 0.20 wt%.Notably,T0.5 of the foams stabilized by CMF at these saline concentrations still can maintain above 1000 s even after aging at 120℃ for 16 h,exhibiting an outstanding foam-stabilizing performance at high *** results suggest that the salt and high-temperature tolerance of CMF in foam stabilization is attributed to the electrically uncharged surfaces,the formation of a gel-like structure and the excellent thermal *** work not only provides a promising candidate of aqueous foam stabilizer to deal with high temperature and high salinity but also presents a natural-based solution for an environmentally friendly drilling industry in the future.

关键词： Aqueous foam Foam stabilizer Cellulose microfiber Salt tolerance Sustainable

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Effect of Ca Micro-Alloying on the Microstructure and Anti-Corrosion Property of Mg0.5Zn0.2Ge Alloy

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Acta Metallurgica Sinica(English Letters) 2024年第7期37卷 1147-1160页

作者： Bishan cheng Depeng Li Baikang Xing Ruiqing Hou Pingli jiang Shijie Zhu Shaokang guan School of Materials Science and Engineering and Henan Key Laboratory of Advanced Magnesium Alloys Zhengzhou UniversityZhengzhou450001China Center of Advanced Analysis and Gene Sequencing Zhengzhou UniversityZhengzhou450001China Key Laboratory of Materials Processing and Mold Technology Ministry of EducationZhengzhou450002China

Magnesium and its alloys have attracting rising attention as one of biodegradable metallic ***,the rapid corrosion and severe localized corrosion still hinder their extensive applications in *** this study,micro-alloying of Ca(≤0.1 wt%)into Mg0.5Zn0.2Ge alloy developed in our previous work was explored to further enhance the corrosion resistance and alleviate the localized corrosion of the *** results reveal that the addition of Ca leads to the transformation of the cathodic Mg_(2)Ge phase in Mg0.5Zn0.2Ca alloy into anodic MgCaGe phase in Ca-containing alloys,thereby changing the galvanic couples in alloys during *** preferential dissolution of MgCaGe phase promotes the participation of Ca and Ge into the formation of corrosion products,resulting in the enrichment of Ca and Ge in the outmost of corrosion product layer,which stabilizes and passivates the corrosion product layer on Mg alloy ***,the enrichment of Zn at the corrosion interface seems to further hinder the corrosion of Mg *** of these factors confer a slower and more uniform corrosion on Mg0.5Zn0.2GexCa(x<0.1 wt%)alloy,which provides favorable candidates for the further processing to gain suitable biodegradable Mg alloys.

关键词： Magnesium alloy Micro-alloying Calcium Corrosion resistance

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An improved initial rotor position estimation method using high-frequency pulsating voltage injection for PMSM

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Defence Technology（防务技术） 2024年第3期33卷 19-29页

作者： Yang jiang Ming cheng School of Electrical Engineering Southeast UniversityNanjing 210096China

High frequency pulsating voltage injection method is a good candidate for detecting the initial rotor position of permanent magnet synchronous ***,traditional methods require a large number of filters,which leads to the deterioration of system stability and dynamic *** order to solve these problems,a new signal demodulation method is proposed in this *** proposed new method can directly obtain the amplitude of high-frequency current,thus eliminating the use of filters,improving system stability and dynamic performance and saving the work of adjusting filter *** addition,a new magnetic polarity detection method is proposed,which is robust to current measurement ***,experiments verify the effectiveness of the method.

关键词： Initial position detection Signal demodulation algorithm Magnetic polarity detection Filter elimination

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