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Static recrystallization behaviors and mechanisms of 7Mo super-austenitic stainless steel with undissolved sigma precipitates during double-stage hot deformation

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Journal of Iron and Steel Research(International) 2024年第2期31卷 475-487页

作者： Shi-guang Xu Jin-shan He Run-ze zhang fu-cheng zhang Xi-tao Wang Collaborative Innovation Center of Steel Technology University of Science and Technology BeijingBeijing100083China State Key Laboratory of Metastable Materials Science and Technology Yanshan UniversityQinhuangdao066004HebeiChina Shandong Provincial Key Laboratory for High Strength Lightweight Metallic Materials Advanced Materials InstituteQilu University of Technology(Shandong Academy of Science)Jinan250353ShandongChina

Static recrystallization(SRX)behaviors and corresponding recrystallization mechanisms of 7Mo super-austenitic stainless steel were studied under different deformation conditions.The order of influence of deformation parameters on static recrystallization behaviors,from high to low,is followed by temperature,first-stage strain and strain rate.Meanwhile,the effect of holding time on static recrystallization behaviors is significantly controlled by temperature.In addition,with the increase in temperature from 1000 to 1200°C,the static recrystallization mechanism evolves from discontinuous static recrystallization and continuous static recrystallization(cSRX)to metadynamic recrystallization and cSRX,and finally to cSRX.The cSRX exists at all temperatures.This is because high stacking fault energy(56 mJ m−2)promotes the movement of dislocations,making the deformation mechanism of this steel is dominated by planar slip of dislocation.Large undissolved sigma precipitates promote static recrystallization through particle-stimulated nucleation.However,small strain-induced precipitates at grain boundaries hinder the nucleation of conventional SRX and the growth of recrystallized grains,while the hindering effect decreases with the increase in temperature.

关键词： 7Mo super-austenitic stainless steel Double-stage hot deformation Conventional static recrystallization Metadynamic recrystallization Strain-induced precipitation

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Comparison on wear resistance of nanostructured bainitic bearing steel with and without residual cementite

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Journal of Iron and Steel Research(International) 2022年第2期29卷 339-349页

作者： Yu-man Qin Chang-bo Liu Chun-sheng zhang Xu-biao Wang Xiao-yan Long Yan-guo Li Zhi-nan Yang fu-cheng zhang State Key Laboratory of Metastable Materials Science and Technology Yanshan UniversityQinhuangdao066004HebeiChina National Engineering Research Center for Equipment and Technology of Cold Rolled Strip Yanshan UniversityQinhuangdao066004HebeiChina

The sliding wear property of high-carbon nanostructured bainitic bearing steel with the equal initial hardness and different microstructures was investigated,and the reasons for the difference of wear resistance between the cementite-bearing(CB)and cementite-free(CF)specimens were analyzed.The results show that CF specimens have lower mass loss and surface roughness and shallower wear depth than CB specimens during wear process.Compared with CB specimen,CF specimen presents superior wear resistance.This is due to two reasons:(1)a lot of retained austenite in CF specimen is easy to produce TRIP effect and be transformed into martensite during wear process,which notably increased the surface hardness of worn specimen;(2)there is a nondestructive oxide layer in the surface of cementite-free worn specimen,which can protect the surface of worn specimen from destruction.Under the combined effect of retained austenite and oxide layer,the loss of matrix is reduced.Thus,CF specimen exhibits high wear resistance.It reveals that the wear mechanism of high-carbon nanostructured bainitic bearing steel with different microstructures can provide a reference for improving the wear resistance in high-carbon nanostructured bainitic bearing steel in future.

关键词： Cementite Nanostructured bainite Bearing steel Microstructure Wear resistance

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In situ observation of the effect of Al N particles on bainitic transformation in a carbide-free medium carbon steel

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International Journal of Minerals,Metallurgy and Materials 2020年第5期27卷 620-629页

作者： Xiao-jie Zhao Zhi-nan Yang fu-cheng zhang State Key Laboratory of Metastable Materials Science and Technology Yanshan UniversityQinhuangdao 066004China National Engineering Research Center for Equipment and Technology of Cold Strip Rolling Yanshan UniversityQinhuangdao 066004China

The bainitic transformation of the steels with different mass fractions of N, ~0.002% and 0.021%, was observed in situ by using high-temperature metalloscope. Micrometer-and nanometer-sized aluminum nitride(AlN) particles were found in the steel with 0.021% N.Grain boundaries, the interior of the grains, and Al N particles were used as initial nucleation sites of bainitic ferrite, and bainitic ferrite subunits served as new nucleation sites to induce secondary nucleation. The lengthening rate of bainitic ferrite varied at different nucleation sites, which was controlled by the repeated nucleation and growth of bainitic subunits. The Al N particles not only provided several nucleation sites, but also increased the autocatalytic effect on the transformation, further shortening the incubation period, promoting the bainitic transformation, and refining the bainitic microstructure.

关键词： bainitic steel In situ observation phase transformation aluminum nitride

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Effect of increased nitrogen content on continuous cooling transition of γ→α in hot-deformed low-C Mo-V-Ti steels

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Journal of Iron and Steel Research(International) 2019年第7期26卷 733-742页

作者： Xin-ping Xiao Gen-hao Shi Shu-ming zhang Yu-wei Gao Qing-feng Wang fu-cheng zhang State Key Laboratory of Metastable Materials Science and Technology Yanshan University Qinhuangdao 066004 Hebei China Qinhuangdao Vocational and Technical College Qinhuangdao 066100 Hebei China National Engineering Research Center for Equipment and Technology of Cold Strip Rolling Yanshan University Qinhuangdao 066004 Hebei China

The two-stage controlled rolling and cooling at 0.5-50℃/s of low-carbon Mo-V-Ti steels with the increasing nitrogen content from 0.0032 to 0.0081 and 0.0123 wt.% were simulated through a Gleeble 3500 system. The continuous cooling transition (CCT) of γ→α in each steel was estimated via microstructure characterization and CCT diagram. The results indicated that CCT diagram for each steel was divided into three regions of γ→ferrite,γ→pearlite and γ→ bainite, and the increasing N content elevated all the starting temperatures for γ→α. Consequently, the polygonal ferrite (PF) and pearlite formed in each steel cooled at 1℃/s and, however, the increasing N content led to slightly coarser ferrite grain and pearlite colony. With the increased cooling rate to 10 and 30℃/s, a mixed microstructure of acicular ferrite (AF), granular bainite (GB) and lath bainite (LB) formed in 32N steel and in contrast, the mixture of PF+AF+GB in 8IN and 123N steels. The increasing N content promoted (Ti,V)(C,N) precipitation, enhanced the intragranular PF/AF nucleation, increased martensite/austenite constituent and depressed LB. In addition, the mechanisms dominating the effect of increasing N on this CCT of γ→α were discussed.

关键词： V-N microalloyed steel Continuous cooling transition Microstructure Precipitation Intragranular ferrite

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Effect of welding heat input on microstructure and impact toughness in CGHAZ of X100Q steel

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Journal of Iron and Steel Research(International) 2019年第6期26卷 637-646页

作者： Hui-bin Wang Fei-long Wang Gen-hao Shi Yu Sun Jiang-cheng Liu Qing-feng Wang fu-cheng zhang State Key Laboratory of Metastable Materials Science and Technology Yanshan University Qinhuangdao 066004. Hebei China Technical Center Tianjin Pipe (Group) Co. Ltd. Tianjin 300301 China National Engineering Research Center for Equipment and Technology of Cold Strip Rolling Yanshan University Qinhuangdao 066004 Hebei China

The coarse-grained heat-affected zones (CGHAZs) of X100Q steel were reproduced via simulating their welding thermal cycles with the varying heat input (Ef) from 10 to 55 kJ/cm in Gleeble3500 system. The microstructures were characterized, and the impact toughness was estimated from each simulated sample. The results indicate that the microstructure in each simulated CGHAZ was primarily constituted of lath-like bainite. With the decreased heat input and accordingly the lowered Ar3 (the onset temperature for this transition), the prior austenite grain and the bainitic packet/block/lath substructure were refined remarkably, and the impact toughness was enhanced due to the microstructure refinement. The bainitic packet was the microstructural unit most effectively controlling the impact properties in CGHAZ of X100Q steel, due to their close correlation with the 50% fracture appearance transition temperatures, their size equivalent to the cleavage facet and their boundaries impeding the crack propagation.

关键词： X100Q bainitic steel Coarse-grained heat-affected zone Impact property Bainitic substructure Fractography

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Hydrocarbon generation history constrained by thermal history and hydrocarbon generation kinetics:A case study of the Dongpu Depression,Bohai Bay Basin,China

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Petroleum Science 2022年第2期19卷 472-485页

作者： Mei-Hua Yang Yin-Hui Zuo Kang-Nan Yan Yong-Shui Zhou Yun-Xian zhang cheng-fu zhang State Key Laboratory of Oil and Gas Reservoir Geology and Exploitation Chengdu University of TechnologyChengduSichuan 610059China Energy&Geoscience Institute University of UtahSalt Lake CityUT84108USA Research Institute of Exploration and Development Zhongyuan OilfieldSINOPECPuyangHenan 457001China

With the increasing exploration and development of typical hydrocarbon-rich depressions,such as the Dongpu Depression,the exploitation difficulty of shallow formations is increasing.There is an urgent need to clarify the hydrocarbon generation mode and hydrocarbon generation histories in deep formations.In this study,a gold tube-autoclave closed system was used to simulate the hydrocarbon generation processes and establish the hydrocarbon generation mode of different types of kerogen.Then,constrained by the thermal history and hydrocarbon generation kinetics,hydrocarbon generation histories were modeled.The results show that hydrocarbon generation evolution can be divided into five stages,and the maturity of each stage is different.The hydrocarbon generation history of the source rocks of the Shahejie 3 Formation mainly dates from the early depositional period of the Shahejie 1 Formation to the middle depositional period of the Dongying Formation.Hydrocarbon generation history constrained by thermal history and hydrocarbon generation kinetics is more in line with actual geological conditions.Moreover,this research can provide important hydrocarbon generation parameters for deep oil and gas exploration and exploitation of the Shahejie 3 Formation in the Dongpu Depression.

关键词： Dongpu depression Thermal history Hydrocarbon generation kinetics Hydrocarbon generation mode Hydrocarbon generation history

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Reactive molecular dynamics insight into the thermal decomposition mechanism of 2,6-Bis(picrylamino)-3,5-dinitropyridine

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Defence Technology（防务技术） 2024年第3期33卷 134-146页

作者： Jianbo fu Hui Ren Xinzhou Wu Yongjin Chen Mi zhang Yazhi cheng State Key Laboratory of Explosion Science and Technology Beijing Institute of TechnologyBeijing 100081China

2,6-bis(picrylamino)-3,5-dinitropyridine(PYX)has excellent thermostability,which makes its thermal decomposition mechanism receive much attention.In this paper,the mechanism of PYX thermal decomposition was investigated thoroughly by the ReaxFF-lg force field combined with DFT-B3LYP(6-311++G)method.The detailed decomposition mechanism,small-molecule product evolution,and cluster evolution of PYX were mainly analyzed.In the initial stage of decomposition,the intramolecular hydrogen transfer reaction and the formation of dimerized clusters are earlier than the denitration reaction.With the progress of the reaction,one side of the bitter amino group is removed from the pyridine ring,and then the pyridine ring is cleaved.The final products produced in the thermal decomposition process are CO_(2),H_(2)O,N_(2),and H_(2).Among them,H_(2)O has the earliest generation time,and the reaction rate constant(k_(3))is the largest.Many clusters are formed during the decomposition of PYX,and the formation,aggregation,and decomposition of these clusters are strongly affected by temperature.At low temperatures(2500 K-2750 K),many clusters are formed.At high temperatures(2750 K-3250 K),the clusters aggregate to form larger clusters.At 3500 K,the large clusters decompose and become small.In the late stage of the reaction,H and N in the clusters escaped almost entirely,but more O was trapped in the clusters,which affected the auto-oxidation process of PYX.PYX's initial decomposition activation energy(E_(a))was calculated to be 126.58 kJ/mol.This work contributes to a theoretical understanding of PYX's entire thermal decomposition process.

关键词： PYX Thermal decomposition ReaxFF-lg MD simulations Excellent thermostable explosives

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Mesoporous polymers:soft-template self-assembly synthesis and applications

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Science China Chemistry 2024年第5期67卷 1442-1464页

作者： Facai Wei Tingting zhang Jianwei fu chengbin Jing Jiangong cheng Shaohua Liu State Key Laboratory of Precision Spectroscopy Engineering Research Center of Nanophotonics&Advanced Instrument(Ministry of Education)School of Physics and Electronic ScienceEast China Normal UniversityShanghai 200241China School of Materials Science and Engineering Zhengzhou UniversityZhengzhou 450052China State Key Lab of Transducer Technology Shanghai Institute of Microsystem and Information TechnologyChinese Academy of SciencesShanghai 200050China

Mesoporous polymers combine the advantages of polymer materials(abundant polar functional groups,lightweight,flexibility,and processability)and mesoporous structures(high specific surface area,adjustable pore structure,and large pore volume);hence,they have great application potential in sensing,adsorption,catalysis,energy storage,biomedicine,etc.Currently,developing advanced synthetic strategies for mesoporous polymers and investigating their intrinsic applications have become hot research topics.Soft-template-based self-assembly is regarded as a promising approach for synthesizing mesoporous polymers.This work reviews recent progress in the synthetic strategy for producing various mesoporous polymers using soft-template selfassembly,focusing on the synthesis of conductive polymers,phenol-based polymers,and resin-based polymers and their potential applications.Finally,perspectives on future applications of mesoporous polymers,along with a few challenges that need to be resolved,are also discussed in this review.

关键词： mesoporous polymer porous material self-assembly soft templates interface synthesis

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Fermented Lentinus edodes extract containingα-glucan ameliorates concanavalin A-induced autoimmune hepatitis in mice

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Food Science and Human Wellness 2024年第4期13卷 2102-2115页

作者： Xin Hu Dan cheng Yingxia zhang Po Li Xiaoping Wu Junsheng fu College of Life Sciences Fujian Agriculture and Forestry UniversityFuzhou 350002China Mycological Research Center Fujian Agriculture and Forestry UniversityFuzhou 350002China Shanghai Lithy One-Health Group Technology Co. Ltd.Shanghai 200235China

Autoimmune hepatitis(AIH)is a chronic inflammatory liver disease that threatens human health worldwide.The aim of this study was to detect the protective effect of a fermented Lentinus edodes extract containingα-glucan(FLA),in a concanavalin A(Con A)-induced AIH mouse model and to determine the underlying liver-protective mechanism.The results showed that compared with the model group,the level of proinflammatory cytokines in serum of FLA pretreated mice was significantly decreased,and the degree of inflammatory cell infiltration in liver,thymus and spleen was significantly reduced.Quantitative polymerase chain reaction,immunohistochemistry,and Western blotting showed that FLA pre-treatment inhibited the Con A-induced apoptosis of hepatocytes by down-regulating the expression of BAX and up-regulating the expression of BCL-2.further research found that FLA may improve liver injury in mice by activating NRF2 signaling pathway and inhibiting TRAF6/NF-κB signaling pathway.Thus,FLA may improve liver injury in mice by shifting gut microbial composition to reduce the release of inflammatory cytokines in the serum and prevent the necrosis of hepatocytes.Up-regulation of NRF2 signaling pathway,down-regulation of TRAF6/NF-κB signaling pathway,and an increase in the relative abundance of Lactobacillus_johnsonii and Ligilactobacillus_murinus play a protective role in liver.

关键词： Autoimmune hepatitis Concanavalin A Lentinus edodes TRAF6/NF-κB NRF2

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A multifunctional electrolyte additive for zinc-ion capacitors with low temperature resistant and long lifespan

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Journal of Energy Chemistry 2024年第7期94卷 477-485页

作者： Ming Sun Zekai zhang Shuqing fu Yifan zhang Ruoyu Wang Hongchun Mu cheng Lian Wenqiang Wang Gengchao Wang Shanghai Engineering Research Center of Hierarchical Nanomaterials Shanghai Key Laboratory of Advanced Polymeric MaterialsSchool of Materials Science and EngineeringEast China University of Science and TechnologyShanghai 200237China State Key Laboratory of Chemical Engineering Shanghai Engineering Research Center of Hierarchical NanomaterialsFrontiers Science Center for Materiobiology and Dynamic Chemistryand School of Chemistry and Molecular EngineeringEast China University of Science and TechnologyShanghai 200237China State Key Laboratory of Molecular Engineering of Polymers Department of Macromolecular ScienceFudan UniversityShanghai 200438China

Aqueous zinc-ion capacitors(ziCs)are considered as potential candidates for next generation electro-chemical energy storage devices due to their high safety and low cost.However,the existing aqueous ZiCs usually have the problems of zinc dendrite growth and unsatisfactory performance at low temper-ature.Herein,an erythritol(Eryt)additive with inhibition of zinc dendrites and anti-freezing capability was introduced into the ZnSO_(4) electrolyte.The experimental characterization and theoretical calculation confirm that the Eryt adsorbed on the surface of zinc anodes regulates the deposition orientation of Zn^(2+)and inhibits the formation of dendrites.It also reconstructs the solvation structure in the electrolyte to reduce water activity,enabling the electrolyte to have a lower freezing point for operation at low tem-perature.With the assistance of Eryt,the ZnZn symmetric cell exhibits a long cycle life of 2000 h,while the ZIC assembled with activated carbon(AC)cathode and zinc anode(ZnllAC)maintains a capacity retention of 98.2%after 30,000 cycles at a current density of 10 A g^(-1)(even after 10,000 cycles at-20°C,the capacity retention rate reached 94.8%.).This work provides a highly scalable,low-cost and effective strategy for the protection of the anodes of low-temperature aqueous ZiCs.

关键词： Zinc-ioncapacitors Electrolyte additive Dendrite-free Freeze-resistant electrolyte

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