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Tungsten 2023年第1期5卷 169-178页

作者： Jiao-Hui Yan Zi-Jing Song Wei Fang Xin-Bo He Ruo-Bin Chang Shao-Wu Huang Jia-Xin Huang Hao-Yang Yu fu-xing yin Research Institute for Energy Equipment Materials School of Materials Science and EngineeringHebei University of TechnologyTianjin 300132China Tianjin Key Laboratory of Materials Laminating Fabrication and Interface Control Technology Tianjin 300132China Institute for Advanced Materials and Technology University of Science and Technology BeijingBeijing 100083China

A method which combines electronegativity difference,CALculation of PHAse Diagrams(CALPHAD) and machine learning has been proposed to efficiently screen the high yield strength regions in Co-Cr-Fe-Ni-Mo multi-component phase diagram.First,the single-phase region at a certain annealing temperature is obtained by combining CALPHAD method and machine learning,to avoid the formation of brittle phases.Then high yield strength points in the single-phase region are selected by electronegativity difference.The yield strength and plastic deformation behavior of the designed Co_(14)Cr_(30)Ni_(50)Mo_(6)alloy are measured to evaluate the proposed method.The validation experiments indicate this method is effective to predict high yield strength points in the whole compositional space.Meanwhile,the interactions between the high density of shear bands and dislocations contribute to the high ductility and good work hardening ability of Co_(14)Cr_(30)Ni_(50)Mo_(6)alloy.The method is helpful and instructive to property-oriented compositional design for multi-principal element alloys.

关键词： High entropy alloys Multi-principal element alloys Yield strength Electronegativity difference CALculation of PHAse Diagrams Machine learning

Microstructure and mechanical properties of nanobainitic steel subjected to multiple isothermal heat treatments

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Journal of Iron and Steel Research(International) 2018年第10期25卷 1062-1067页

作者： Ning Liu Xin Zhang Jing Ding Jun He fu-xing yin School of Material Science and Engineering and ResearchInstitute for Energy Equipment Materials Hebei Universityof Technology Tianjin 300130 China

Nanostructured bainite in 62MnSiCr steel was prepared by two-stage transformation process at different temperatures for less than 2 h. Microstructures, phase distribution and mechanical properties of the obtained steel were investigated. The results showed that the thickness of bainite plate and the amount of retained austenite decreased obviously after the twostage transformation, while the carbon concentration in the retained austenite showed a small change. With increase in the second holding temperature within the bainite transformation range, all of them increased slightly. The additional formation of bainite at the second transformation stage is beneficial to refining the austenite and further enriching it with carbon, resulting in the enhancement of the mechanical stability. Bainite transformed in two-stage process showed a better comprehensive performance. Absorbed impact energy of 88 J and an ultimate tensile strength of 1818 MPa have been achieved by isothermal heat treatment at 300 ℃ followed by 260 ℃. Meanwhile, there was a slight change in mechanical properties when the second transformation temperature varied from 260 to 220 ℃.

关键词： Nanostructured bainite Heat treatment Microstructure Mechanical property

Microstructure and mechanical properties of weld metal in laser and gas metal arc hybrid welding of 440-MPa-grade high-strength steel

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Journal of Iron and Steel Research(International) 2021年第7期28卷 853-861页

作者： fu-xing yin Xu-chen Li Cui-xin Chen Lin Zhao Yun Peng Zhi-ling Tian School of Materials Science and Engineering Hebei University of TechnologyTianjin 300130China Tianjin Key Laboratory of Laminating Fabrication and Interface Control Technology for Advanced Materials Hebei University of TechnologyTianjin 300130China Research Institute for Energy Equipment Materials Hebei University of TechnologyTianjin 300130China Central Iron and Steel Research Institute Beijing 100081China

Fiber laser and gas metal arc hybrid welding of 440-MPa-grade high-strength marine steel was carried out at different welding speeds.The influence of welding speed on the micro structure and mechanical properties of weld metal was investigated.The weld-metal microstructure mainly consisted of pre-eutectoid ferrite,side-plate ferrite,acicular ferrite and lath bainite at a low welding speed.With the increase in welding speed,acicular ferrite and lath bainite were the dominant weld-metal microstructures.All samples failed at the base metal during tensile tests,which indicates that there is no soft zone in the hybrid welds.The welding speed had a significant effect on the impact toughness of the weld metal.The impact absorbed energy of the weld metal increased from 35 to 105 J with the increase in welding speed from 0.8 to 2.0 m/min.Large amounts of acicular ferrite and lath bainite were formed in the weld metal at a high welding speed,which resulted in an excellent impact toughness.

关键词： Laser-arc hybrid welding High-strength steel Microstructure Mechanical property

Effect of Ti and rare earth on microsegregation and large-sized precipitates of H13 steel

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Journal of Iron and Steel Research(International) 2021年第12期28卷 1591-1604页

作者： Fa Ji Rui Xu Yu-long Gao Qing-chao Tian Lu Wang Zhi-xia Xiao fu-xing yin School of Materials Science and Engineering Hebei University of TechnologyTianjin300130China Research Institute for Energy Equipment Materials Hebei University of TechnologyTianjin300130China State Key Laboratory of Advanced Special Steel&Shanghai Key Laboratory of Advanced Ferrometallurgy&School of Materials Science and Engineering Shanghai UniversityShanghai200444China

Large-sized precipitates are fatal to the thermal fatigue of H13 hot work die steel.Different amounts of Ti and/or rare earth(RE)were added in H13 steel during electroslag remelting to improve the element segregation and refine the large-sized precipitates.The results show that as Ti content increases from 0.0032 to 0.057 wt.%,the segregation of Cr,Mo and V becomes more severe.V-rich M(C,N)carbides are shorter,and their branches are denser in 3D observation.Moreover,the number density of V-rich M(C,N)carbides with a size less than 2μm increases and that with other sizes decreases.In addition,Ti-rich MN nitrides with the size greater than 4μm increases significantly at high Ti content.When RE content increases from 0.0051 to 0.036 wt.%,the segregation of main alloying elements is first weakened and then aggravated.Compared with that in RE-free H13 steel,V-rich M(C,N)carbides are less developed in 3D observation,and the change in number density is similar to that of Ti-modified alloys.After composite modification of 0.024 wt.%Ti and 0.011 wt.%RE,the segregation of alloying element and V-rich M(C,N)carbides are not significantly improved.

关键词： H13 steel Segregation Primary carbide Ti Rare earth Precipitate

Effects of electrode configuration on electroslag remelting process of M2 high-speed steel ingot

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China Foundry 2019年第2期16卷 126-134页

作者： fu-xing yin Yu Liang Zhi-xia Xiao Jian-hang Feng Zhi-bin Xie Yong-wang Mi School of Materials Science and Engineering Hebei University of Technology Research Institute for Energy Equipment Materials Hebei University of Technology Tianjin Key Laboratory of Materials Laminating Fabrication and Interfacial Controlling Technology Heye Science and Technology Co. Ltd.

The electrode configuration determines the thermophysical field during the electroslag remelting(ESR) process and affects the final microstructure of the ingot. In this work, ingot with a diameter of 400 mm was prepared with two electrode configuration modes of single power ESR process, namely one electrode(OE) and two series-connected electrodes(TSCE). Finite element simulation was employed to calculate the electromagnetic field, flow field and temperature field of the ESR system. The results show that the temperature of the slag pool and the metal pool of the TSCE process is lower and more uniform than that of the OE process.The calculated temperature distribution of the ingot could be indirectly verified from the shape of the metal pool by the experiment. The experimental results show that the depth of the metal pool in the OE ingot is about 160 mm, while the depth of the TSCE ingot is nearly 40 mm shallower than that of the OE ingot. Microstructural comparisons indicate that coarse eutectic carbides are formed in the center of the OE ingot, whereas more even eutectic carbides appear in the center of the TSCE ingot. In general, compared with the OE process, the TSCE process is preferred to remelt high speed steel ingots.

关键词： electroslag remelting metal pool shape electromagnetic field eutectic carbides high speed steel

Effect of melting rate on microsegregation and primary MC carbides in M2 high-speed steel during electroslag remelting

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China Foundry 2021年第3期18卷 163-169页

作者： fu-xing yin Ming Su Fa Ji Qing-chao Tian Ya-guan Bai Jian-hang Feng Zhi-xia Xiao School of Materials Science and Engineering Hebei University of TechnologyTianjin 300130China Tianjin Key Laboratory of Layered Composite Materials Tianjin 300130China State Key Laboratory of Advanced Special Steel Shanghai Key Laboratory of Advanced FerrometallurgySchool of Materials Science and EngineeringShanghai UniversityShanghai 200444China Tianjin Heavy Industries Research and Development Co. Ltd.Tianjin 300457China

Large-size primary MC carbides can significantly reduce the performance of M2 high-speed steel.To better control the morphology and size of primary MC carbides,the effect of melting rate on microsegregation and primary MC carbides of M2 steel during electroslag remelting was investigated.When the melting rate is decreased from 2 kg·min^(-1) to 0.8 kg·min^(-1),the columnar dendrites are gradually coarsened,and the extent of segregation of Mo and V is alleviated,while the segregation of Cr becomes severe.At 2 kg·min^(-1),the number of primary MC carbides per unit area with the sizes in the range of 2 μm to 6 μm accounts for about 75% of all MC carbides,while the carbides are mainly concentrated on the size larger than 8 μm at 0.8 kg·min^(-1).Thermodynamic calculations based on the Clyne-Kurz (simplified to C-K) model shows that MC carbide can be precipitated in the final solidification stage and a smaller secondary dendrite arm spacing caused by higher melting rate (2 kg·min^(-1) in this experiment) facilitates the refinement of primary MC carbides.

关键词： high-speed steel MC carbide melting rate electroslag remelting microsegregation

Al−10Nb−3Ce−2.5B孕育剂对Zn−Al共析合金显微组织、阻尼和拉伸力学性能的影响

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Transactions of Nonferrous Metals Society of China 2024年第2期34卷 465-479页

作者：张建军殷福星余晖冀璞光刘力李玉芳焦志娴王清周河北工业大学材料科学与工程学院天津市材料层状复合与界面控制技术重点实验室天津300130 广东省科学院新材料研究所广州510651

制备一种新型Al−10Nb−3Ce−2.5B孕育剂,并系统研究其对锌铝共析(ZA22)合金显微组织、阻尼和拉伸力学性能的影响。结果表明,该孕育剂对ZA22合金中的α相具有显著的细化作用(α相最低可被细化至约16μm),并可使得α相的形貌从粗大枝晶状转... 详细信息

制备一种新型Al−10Nb−3Ce−2.5B孕育剂,并系统研究其对锌铝共析(ZA22)合金显微组织、阻尼和拉伸力学性能的影响。结果表明,该孕育剂对ZA22合金中的α相具有显著的细化作用(α相最低可被细化至约16μm),并可使得α相的形貌从粗大枝晶状转变为细小花瓣状。通过边−边匹配晶体学模型(E2EM)建立孕育剂中CeB_(6)和NbB_(2)颗粒与α相之间的位向关系(ORs),并基于该E2EM模型揭示孕育剂对ZA22合金的细化机理。与未细化ZA22合金相比,孕育细化ZA22合金的高温阻尼性能,特别是逆共析转变阻尼峰得到显著提升。此外,孕育细化ZA22合金的室温拉伸力学性能也得到了显著提高,具有最佳细化效果的ZA22合金的抗拉强度和伸长率分别比未细化ZA22合金的高18.56%和119.04%。对相关机理进行了讨论。

关键词： Zn−Al共析合金孕育剂显微组织细化阻尼拉伸力学性能

Recent Progress and Development in Extrusion of Rare Earth Free Mg Alloys: A Review

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Acta Metallurgica Sinica(English Letters) 2019年第2期32卷 145-168页

作者： Shuai-Ju Meng Hui Yu Shao-Da Fan Qi-Zhi Li Sung Hyuk Park Joung Sik Suh Young Min Kim Xiao-Long Nan Ming-Zhe Bian fu-xing yin Wei-Min Zhao Bong Sun You Kwang Seon Shin School of Materials Science and Engineering Hebei University of Technology School of Materials Science and Engineering Kyungpook National University Materials Implementation Department Korea Institute of Materials Science National Key Laboratory of Shock Wave and Detonation Physics Institute of Fluid Physics China Academy of Engineering Physics School of Materials Science and Engineering Anhui University of Technology Magnesium Technology Innovation Center School of Materials Science and Engineering Seoul National University

Mg and its alloys are the lightest structural metals available and are extremely attractive for applications as lightweight components, particularly in the automobile, electronic, and aerospace industries. The global market for wrought Mg alloys has steadily expanded over the past decade. And numerous studies have been carried out to meet this increasing demand of high-performance Mg alloys. However, Mg extrusion alloys have had a very limited usage so far. To overcome existing industrial challenges, one desirable approach is the development of low-cost rare earth(RE) free Mg extrusion alloys with superior mechanical properties. This review will introduce the recent research highlights in the extrusion of Mg alloys, specifi cally focusing on low-cost RE-free Mg alloy. The results from both the literature and our previous study are summarized and critically reviewed. Several aspects of RE-free Mg extrusion alloys are described in detail:(1) novel alloying designs including Mg–Al-, Mg–Zn-, Mg–Ca-, Mg–Sn-, and Mg–Bi-based alloys,(2) advanced extrusion techniques, and(3) extrusion-related severe plastic deformation(SPD) processing. Accordingly, considering the large gap in mechanical properties between the current RE-free Mg alloys and high-performance aluminum alloys, new alloy design, processing route control, and recommendations for future research on RE-free Mg extrusion alloys are also proposed. We hope this review will not only off er insightful information regarding the extrusion of RE-free Mg alloys but also inspire the development of new Mg extrusion technologies.

关键词： Mg alloy Extrusion Rare earth free Novel processing Mechanical properties

Annexin A1 in the nervous and ocular systems

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Neural Regeneration Research 2024年第3期19卷 591-597页

作者： Aijia Wang Hong Zhang xing Li yin Zhao Department of Ophthalmology 2Department of AnesthesiologyTongji HospitalTongji Medical CollegeHuazhong University of Science and TechnologyWuhanHubei ProvinceChina

The therapeutic potential of Annexin A1,an important member of the Annexin superfamily,has become evident in results of experiments with multiple human systems and animal models.The anti-inflammatory and pro-resolving effects of Annexin A1 are characteristic of pathologies involving the nervous system.In this review,we initially describe the expression sites of Annexin A1,then outline the mechanisms by which Annexin A1 maintains the neurological homeostasis through either formyl peptide receptor 2 or other molecular approaches;and,finally,we discuss the neuroregenerative potential qualities of Annexin A1.The eye and the nervous system are anatomically and functionally connected,but the association between visual system pathogenesis,especially in the retina,and Annexin A1 alterations has not been well summarized.Therefore,we explain the beneficial effects of Annexin A1 for ocular diseases,especially for retinal diseases and glaucoma on the basis of published findings,and we explore present and future delivery strategies for Annexin A1 to the retina.

关键词： Annexin A1(ANXA1) glaucoma nervous system neuroprotection neuroregeneration ocular disease retina

Distribution and bioavailability of mercury in size-fractioned atmospheric particles around an ultra-low emission power plant in Southwest China

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Journal of Environmental Sciences 2024年第4期138卷 141-152页

作者： Wei Zhang Jinjuan Li Hao Qiu xingqiang Guo Zhijun Fei Yi xing Deliang yin College of Resources and Environmental Engineering Guizhou UniversityGuiyang 550025China College of Resources and Environmental Engineering Guizhou Institute of TechnologyGuiyang 550003China Key Laboratory of Karst Georesources and Environment(Guizhou University) Ministry of EducationGuiyang 550025China School of Energy and Environmental Engineering University of Science&Technology BeijingBeijing 100083China

Ultra-low emission(ULE)technology retrofits significantly impact the particulate-bound mercury(Hg)emissions from coal-fired power plants(CFPPs);however,the distribution and bioavailability of Hg in size-fractioned particulate matter(PM)around the ULE-retrofitted CF-PPs are less understood.Here,total Hg and its chemical speciation in TSP(total suspended particles),PM_(10)(aerodynamic particle diameter≤10μm)and PM_(2.5)(aerodynamic particle diameter≤2.5μm)around a ULE-retrofitted CFPP in Guizhou Province were quantified.Atmospheric PM_(2.5)concentration was higher around this ULE-retrofitted CFPP than that in the intra-regional urban cities,and it had higher mass Hg concentration than other sizefractioned PM.Total Hg concentrations in PM had multifarious sources including CFPP,vehicle exhaust and biomass combustion,while they were significantly higher in autumn and winter than those in other seasons(P40%).Mass concentrations of exchangeable,HCl-soluble,elemental,and residual Hg in PM_(2.5)were higher than those in other size-fractioned PM,and were markedly elevated in autumn and winter(P<0.05).In PM_(2.5),HCl-soluble Hg presented a significantly positive relationship with elemental Hg(P<0.05),while residual Hg showed the significantly positive relationships with HCl-soluble Hg and elemental Hg(P<0.01).Overall,these results suggested that atmospheric PM-bound Hg around the ULE-retrofitted CFPP tends to accumulate in finer PM,and has higher bioavailable fractions,while has potential transformation between chemical speciation.

关键词： Size-fractioned particles Mercury Chemical speciation Coal-fired power plant Ultra-low emission