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Interconnected microstructure and flexural behavior of Ti_(2)C-Ti composites with superior Young’s modulus

International Journal of Minerals,Metallurgy and Materials 2024年第9期31卷 2088-2101页

作者： fengbo sun Rui Zhang Fanchao Meng Shuai Wang Lujun Huang Lin Geng School of Materials Science and Engineering Harbin Institute of TechnologyHarbin 150001China Waikato Centre for Advanced Materials and Manufacturing School of EngineeringUniversity of WaikatoHamilton 3240New Zealand State Key Laboratory of Precision Welding&Joining of Materials and Structures Harbin Institute of TechnologyHarbin 150001China

To enhance the Young’s modulus(E)and strength of titanium alloys,we designed titanium matrix composites with intercon-nected microstructure based on the Hashin-Shtrikman *** to the results,the in-situ reaction yielded an interconnected microstructure composed of Ti_(2)C particles when the Ti_(2)C content reached 50vol%.With widths of 10 and 230 nm,the intraparticle Ti lamellae in the prepared composite exhibited a bimodal size distribution due to precipitation and the unreacted Ti phase within the grown Ti_(2)C *** composites with interconnected microstructure attained superior properties,including E of 174.3 GPa and ultimate flexural strength of 1014 *** with that of pure Ti,the E of the composite was increased by 55% due to the high Ti_(2)C content and interconnected *** outstanding strength resulted from the strong interfacial bonding,load-bearing capacity of interconnected Ti_(2)C particles,and bimodal intraparticle Ti lamellae,which minimized the average crack driving *** flexural tests revealed preferential crack initiation along the{001}cleavage plane and grain boundary of Ti_(2)C in the region with the highest tensile *** addition,the propagation can be efficiently inhibited by interparticle Ti grains,which prevented the brittle fracture of the composites.

关键词： titanium matrix composites titanium carbide interface Young’s modulus flexural behavior

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Fatigue Crack Initiation and Propagation Dominated by Crystallographic Factors in TiB/near α-Ti Composite

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Acta Metallurgica Sinica(English Letters) 2024年第5期37卷 763-776页

作者： Fanchao Meng Rui Zhang Shuai Wang fengbo sun Run Chen Lujun Huang Lin Geng School of Materials Science and Engineering Harbin Institute of TechnologyHarbin 150001China Waikato Centre for Advanced Materials and Manufacturing School of EngineeringUniversity of WaikatoHamilton 3240New Zealand State Key Laboratory of Advanced Welding and Joining Harbin Institute of TechnologyHarbin 150001China

Discontinuously reinforced titanium matrix composites(DRTMCs)with a network structure have been extensively researched due to their superior combination of strength and ***,their fatigue performance has remained *** order to elucidate the fatigue behavior of DRTMCs,a tension-tension fatigue test was performed on a TiB/nearα-Ti composite with network *** results showed that the variability of fatigue lifetime increased as the stress level *** analysis indicated that fatigue crack initiation was associated with facet formation,while the subsequent propagation was hindered by the network structure comprising TiB whiskers and *** characterization further revealed that facets formed due to a combination of shear and normal *** reduction in fatigue lifetime was attributed to an increase in the effective slip length,which was influenced by the orientation of grains near the crack-initiation sites toward basal slip in the life-limiting *** in situ observation suggested that the crack initiation was facilitated by both basal and prismatic slip ofα-Ti as well as fracture of *** propagation was found to be associated with basal and prismatic slip systems with high Schmid factors,regardless of whether the crack was intergranular or intragranular.

关键词： Titanium matrix composite TiBw Fatigue lifetime variability Crack initiation Crack propagation

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Hot deformation behavior and microstructure evolution of GH3536-TiB_(2) composites fabricated by powder metallurgy

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Science China(Technological Sciences) 2024年第7期67卷 2107-2124页

作者： ZHOU ShiPeng WANG Shuai HUANG LuJun ZHANG Rui CHEN Xin MENG FanChao CHEN Run sun fengbo WANG CunYu GENG Lin School of Materials Science and Engineering Harbin Institute of TechnologyHarbin 150001China Waikato Centre for Advanced Materials and Manufacturing School of EngineeringUniversity of WaikatoHamilton 3240New Zealand State Key Laboratory of Advanced Welding and Joining Harbin Institute of TechnologyHarbin 150001China

The hot deformation behavior and microstructure evolution of GH3536-TiB2composites fabricated by powder metallurgy(PM)were examined in the temperature range of 950–1150℃ and strain rate range of 0.001–1 s^(-1). The hot compression stress-strain curves and the constitutive equation were obtained. In addition, the hot processing map was drawn, which indicated that the appropriate hot working window was 950–1050℃/0.001–0.1 s^(-1)and 1050–1100℃/0.001–0.01 s^(-1). The microstructure analysis showed that the splitting and spheroidization of M3B2led to a decrease in size and volume fraction at 950–1100℃. At 1150℃,the eutectic microstructure of M_(3)B_(2)+ γ was formed due to the dissolution of M_(3)B_(2), which caused macroscopic cracking of the deformed sample. Additionally, the deformation temperature and the strain rate had little effect on the size and volume fraction of M_(3)B_(2). Besides, discontinuous dynamic recrystallization(DDRX) and continuous dynamic recrystallization(CDRX) were found in the deformed microstructure, while the former was dominant. Within the test range of this work, the dynamic recrystallization(DRX) fraction of the deformed composites was high due to the bulging nucleation of numerous interfaces. The DRX grain size increased with increasing deformation temperature or decreasing strain rate. Texture analysis showed that the deformation texture of //compression direction RD existed in the matrix when the deformation temperature was below 1100℃, and the texture type became //RD at 1100℃. Additionally, it was also found that the //RD texture was formed in M3B2under the strain rates of 0.1 and 0.01 s^(-1).

关键词： GH3536 alloy matrix composites powder metallurgy hot deformation behavior microstructure evolution

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Stratigraphy and Zircon Provenance of a Late Paleoproterozoic Terrestrial Sequence underlying the Xiong'er Volcanics in the Southern North China Craton

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Acta Geologica Sinica(English Edition) 2022年第5期96卷 1502-1515页

作者： sun fengbo ZHENG Deshun ZUO Pengfei LIU Weiqing Henan Polytechnic University JiaozuoHenan 454003China

The late Paleoproterozoic Dagushi Formation comprises a fluvial-lacustrine succession and represents the initial fill of the Xiong'er Basin in the southern North China *** integrated outcrop surveys and detrital zircon UPb-Hf dating,this study examines the provenance and depositional setting of the Dagushi *** major depositional facies,including braided channel,distributary channel,subaqueous stream/mouth bar,pro-delta and shallow lake,were identified,based on lithofacies and *** were interpreted as representing a braided river deltalacustrine *** ages of the last metamorphic event of the basement,covering volcanics and the youngest zircon together constrain a depositional age of ca.1.79 Ga for the Dagushi *** age distributions reveal a provenance change from ca.2.7–2.5 Ga rocks in the lower part,to ca.2.3–1.9 Ga sources in the middle-upper part of the Dagushi *** the vertical sedimentology,this provenance change could be induced by the rising water-level caused by a tectonic *** ca.2.7–2.5 Ga zircons are suggested to be locally sourced from the late Neoarchean–Paleoproterozoic metamorphic *** northeast Zhongtiao Mts area(current co-ordinates)is supposed to have appeared as a paleo-uplift and served as a source area for the Paleoproterozoic *** Dagushi Formation records an early‘underfilled'stage of the Xiong'er Rift.

关键词： late Paleoproterozoic Dagushi Formation sedimentology zircon geochronology provenance Xiong'er Rift

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选区激光熔化成形2%TiB_(w)/TA15复合材料的显微组织与性能

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中国有色金属学报 2024年第4期34卷 1164-1178页

作者：贾畅颖安琦王存玉张芮崔丽华陈润孙枫泊黄陆军耿林哈尔滨工业大学材料科学与工程学院哈尔滨150000

本文通过选区激光熔化成形技术(Selective laser melting,SLM)制备原位自生2%(体积分数)TiB_(w)/TA15钛基复合材料,探究激光功率和扫描速率对该复合材料的显微组织和室温/高温力学性能的影响规律,并揭示其强化机理。结果表明:SLM-2%TiB_... 详细信息

本文通过选区激光熔化成形技术(Selective laser melting,SLM)制备原位自生2%(体积分数)TiB_(w)/TA15钛基复合材料,探究激光功率和扫描速率对该复合材料的显微组织和室温/高温力学性能的影响规律,并揭示其强化机理。结果表明:SLM-2%TiB_(w)/TA15复合材料中存在孔隙缺陷,其数量随激光功率的降低和扫描速率的增大而增加。该复合材料基体由一定生长方向的原始柱状β晶和细小层片状α相组成,TiB晶须呈弥散分布;其抗拉强度随激光功率的增大而减小,随扫描速率的增大而增大,最高室温抗拉强度为1337.8 MPa,与SLM-TA15合金相比提高了15.1%;600℃抗拉强度最高值为651.1 MPa,与SLM-TA15合金相比提高了10.1%。复合材料的维氏硬度最高为403.21HV,显著高于SLM-TA15合金(345.3HV)。该复合材料强度提升的主要强化机制为载荷传递强化、热错配强化和细晶强化。

关键词： TiB_(w)/TA15复合材料选区激光熔化显微组织力学性能强化机理

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树木生长应力形成机理

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林业科学 2024年第10期60卷 154-163页

作者：栾玉江梦虹杨雨婷刘焕荣马欣欣张秀标孙丰波费本华方长华国际竹藤中心竹藤科学与技术国家林业和草原局重点实验室北京100102

作为一种自然资源,树木具有重要的环境、社会和经济价值。树木生长成熟过程中,细胞间及细胞壁各层相互作用会产生生长应力,生长应力是木材组织正常发育的结果,是树干和树枝维持其垂直生长或特定角度生长的重要动力。此外,树木在抵御自... 详细信息

作为一种自然资源,树木具有重要的环境、社会和经济价值。树木生长成熟过程中,细胞间及细胞壁各层相互作用会产生生长应力,生长应力是木材组织正常发育的结果,是树干和树枝维持其垂直生长或特定角度生长的重要动力。此外,树木在抵御自身重力或光照、风雪、地势等环境刺激时,会形成具有更高水平生长应力的应力组织——应力木,从而达到调整或维持生长形态的目的。树木中的生长应力是影响木材成材和加工质量的重要力学问题,且生长应力水平与细胞结构、化学组分密切相关,开展树木生长应力研究、厘清树木生长应力分布和形成机理,对树木的定向培育、生物学结构与功能研究、木材加工与利用以及仿生新材料的开发具有重要意义。已有研究通过树木生长应力水平测试,结合其解剖结构、基因、化学组分、激素分布、力学材性等方面特征,对树木生长应力形成机理进行了深入分析,探索生长应力的产生来源;但由于生物材料结构复杂、变异性大,且研究者对生长应力形成机理的认识也在不断更新,树木生长应力形成机理尚未达成共识。本研究简述树木生长应力的生物力学作用及常用表征方法,综述主流的树木生长应力形成理论,对生长应力形成机理的一般性假说和特殊应力组织(应拉木和应压木)的生长应力形成假说进行重点分类阐述,并对各假说存在的争议性问题进行分析,以期全面认识树木生长应力,并为推动其进一步研究、为树木细胞结构和性质变异研究以及木材精细化利用提供参考,为探寻有效的降低树木生长应力的措施提供基础,为人工林的生物改良和栽培提供理论和实践支持。

关键词：生长应力形成机理应力木应拉木应压木

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Mechanical and biocompatible properties of polymer-infiltrated-ceramic-network materials for dental restoration

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Journal of Advanced Ceramics 2020年第1期9卷 123-128页

作者： Bencang CUI Ranran ZHANG fengbo sun Qian DING Yuanhua LIN Lei ZHANG Cewen NAN School of Materials Science and Engineering Tsinghua UniversityBeijing 100084China Department of Prosthodontics School and Hospital of StomatologyPeking UniversityBeijing 100081China

Dental restorative materials with high mechanical properties and biocompatible performances are *** this work,polymer-infiltrated-ceramic-network materials(PICNs)were fabricated via infiltrating polymerizable monomers into porous ceramic networks and incorporated with hydroxyapatite *** results revealed that the flexural strength can be enhanced up to 157.32 MPa,and elastic modulus and Vickers hardness can be achieved up to 19.4 and 1.31 GPa,respectively,which are comparable with the commercial computer-aided design and computer-aided manufacturing(CAD/CAM)***,the adhesion and spreading of rat bone marrow mesenchymal stem cells(r BMSCs)on the surface of such materials can be improved by adding hydroxyapatite,which results in good *** PICNs are potential applicants for their application in the dental restoration.

关键词： dental restoration hydroxyapatite polymer-infiltrated-ceramic-network materials(PICNs) mechanical property biocompatible performance

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Improving flexural strength of Ti_(2)C-Ti cermet by hot compressive deformation:Microstructure evolution and fracture behaviors

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Science China(Technological Sciences) 2023年第11期66卷 3298-3308页

作者： sun fengbo WANG Shuai CHEN Xin ZHANG Rui AN Qi LIU WenQi HUANG LuJun GENG Lin School of Materials Science and Engineering Harbin Institute of TechnologyHarbin 150001China Waikato Centre for Advanced Materials and Manufacturing School of EngineeringUniversity of WaikatoHamilton 3240New Zealand State Key Laboratory of Advanced Welding and Joining Harbin Institute of TechnologyHarbin 150001China

In order to improve the microstructure and mechanical properties,the hot compressive deformation with 50%height reduction at 1100℃was conducted on a Ti_(2)C-Ti *** results showed that the lamellar Ti precipitates in Ti_(2)C grains were transformed to bimodal size distribution,which was approximately 290 nm and 5.8μm in diameter,respectively,after the hot *** bimodal Ti precipitates suppressed{011}cleavage surfaces of Ti_(2)C during flexural fracture,which resulted in an 18.5%increment of *** phenomenon can be attributed to the bimodal Ti precipitates that decreased the average crack driving force due to their gentle variation in elastic modulus compared with the monolithic lamellar Ti *** present work can guide further deformation and mechanical property improvement of Ti_(2)C cermets.

关键词： cermet sub-stoichiometric titanium carbide hot deformation precipitate fracture behavior

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Continuously released Zn^(2+)in 3D-printed PLGA/β-TCP/Zn scaffolds for bone defect repair by improving osteoinductive and anti-inflammatory properties

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Bioactive Materials 2023年第6期24卷 361-375页

作者： Chunxu Li fengbo sun Jingjing Tian Jiahao Li Haidan sun Yong Zhang Shigong Guo Yuanhua Lin Xiaodan sun Yu Zhao Department of Orthopedics Peking Union Medical College HospitalChinese Academy of Medical Sciences and Peking Union Medical CollegeBeijing100730China State Key Laboratory of Advanced Ceramics and Fine Processing School of MaterialsTsinghua UniversityBeijingChina Medical Science Research Center Peking Union Medical College HospitalChinese Academy of Medical Sciences and Peking Union Medical CollegeBeijingChina Core Facility of Instrument Institute of Basic Medical SciencesChinese Academy of Medical Sciences and School of Basic MedicinePeking Union Medical CollegeBeijingChina The State Key Laboratory of Medical Molecular Biology Institute of Basic Medical SciencesChinese Academy of Medical Sciences and School of Basic MedicinePeking Union Medical CollegeBeijingChina Department of Rehabilitation Medicine Southmead HospitalBristolUK

Long-term nonunion of bone defects has always been a major problem in orthopedic *** bone graft materials such as Poly(lactic-co-glycolic acid)/β-tricalcium phosphate(PLGA/β-TCP)scaffolds are expected to solve this problem due to their suitable degradation rate and good ***,insufficient mechanical properties,lack of osteoinductivity and infections after implanted limit its large-scale clinical ***,we proposed a novel bone repair bioscaffold by adding zinc submicron particles to PLGA/β-TCP using low temperature rapid prototyping 3D printing *** first screened the scaffolds with 1 wt%Zn that had good biocompatibility and could stably release a safe dose of zinc ions within 16 weeks to ensure long-term *** designed,the scaffold had a multi-level porous structure of biomimetic cancellous bone,and the Young’s modulus(63.41±1.89 MPa)and compressive strength(2.887±0.025 MPa)of the scaffold were close to those of cancellous *** addition,after a series of in vitro and in vivo experiments,the scaffolds proved to have no adverse effects on the viability of BMSCs and promoted their adhesion and osteogenic differentiation,as well as exhibiting higher osteogenic and anti-inflammatory properties than PLGA/β-TCP scaffold without zinc *** also found that this osteogenic and anti-inflammatory effect might be related to Wnt/β-catenin,P38 MAPK and NFkB *** study lay a foundation for the follow-up study of bone regeneration mechanism of Zn-containing *** envision that this scaffold may become a new strategy for clinical treatment of bone defects.

关键词： 3D printing Zinc submicron particles Osteoinductivity Anti-inflammatory Bone defect repair

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Research on the Bending Impact Resistance and Transverse Fracture Characteristics of Bamboo under the Action of Falling Weight

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Journal of Renewable Materials 2023年第1期11卷 473-490页

作者： Hao Jia Benhua Fei Changhua Fang Huanrong Liu Xiubiao Zhang Xinxin Ma fengbo sun Department of Biomaterials International Centre for Bamboo and RattanBeijing100102China SFA and Beijing Co-Built Key Laboratory of Bamboo and Rattan Science&Technology State Forestry AdministrationBeijing100102China

Drop weight impact tester was used to accurately measure the bending impact resistance of various parts of Phyllostachys edulis,commonly known as moso bamboo,with a growth cycle of 3–8 *** crystallinity in the bottom(B),middle(M)and top(T)of bamboo at different ages was calculated using peak height analysis in X-ray *** of Spearman correlation analysis was used to represent the correlation between chemical composition and impact *** breaking load(BL),fracture energy(FE)and impact deflection(ID)of 3–8-year-old bamboo were found to be in the range of~670–2120 N,~5.17–15.55 J,and~3.60–~17.76 mm,*** the growth period of bamboo rises,the cellulose crystallinity at the B and T decreases first and then increases,while that for the M increases first and then remains ***,the bending impact performance of bamboo was found to become stable with its growth and *** flexural impact and toughness of the 4-year-old bamboo base material were better than other *** enhancement in the bending impact properties of bamboo at different growth periods was influenced by the lignin content,while the value of FE was mainly positively correlated with ash,cold and hot water extracts and benzyl alcohol *** the content of holocellulose and pentosan,air-dry density and,base density negatively influenced the *** the change in the height of the bamboo,the correlation between its impact mechanical properties and chemical composition gradually *** study provides data support and theoretical basis for the age-appropriate thinning and application of moso bamboo.

关键词： Moso bamboo lifespan bending impact breaking load fracture energy impact deflection chemical composition correlation

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