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Controlled growth and composition of multivariate metal-organic frameworks-199 via a reaction-diffusion process

Nano Research 2021年第2期14卷 423-431页

作者： Razan lssa fayrouz abou ibrahim Mazen Al-Ghoul Mohamad Hmadeh Department of Chemistry American University of BeirutP.O.Box 11-0236RiadEl-Solh 11072020BeirutLebanon Department of Chemistry McGill University801 Sherbrooke Street WestMontreal H2A 0B8Canada

In this paper,we exploit our prior successful synthesis of MOF-199 single crystals using the reaction-diffusion framework(RDF),to synthesize multivariate metal-organic frameworks(MTV-MOFs)version with enhanced *** MTV-MOFs are synthesized by creating defects within the MOF-199 crystal structure by integrating organic linkers entailing different functional ***,5-aminoisophthalic acid(NH_(2)-BDC)and 5-hydroxyisophthalic acid(OH-BDC)are separately mixed with 1,3,5-benzenetricarboxylic acid(BTC)in three different starting ratios of X-BDC:BTC(1:3,1:1)and(3:1).The effects of this linker on the morphology of the synthesized MTV-MOFs,their thermal stability,and their surface area are *** extent of the incorporation of the linkers in the framework is elucidated via^(1)H-NMR spectroscopy and it is shown that the incorporation varies as a function of the location along the tubular reactor,a characteristic of *** enhanced properties of the synthesized MTV-MOFs are further demonstrated by measuring its adsorptive capability for methylene blue(MB)and rhodamine B(Rh B)in aqueous solution,and compared with that of the as-synthesized *** kinetic and thermodynamic studies reveal that MTV-MOFs with the ratio of X-BDC:BTC(1:1)exhibit the best uptakes of MB(263 mg/g)for X=OH and Rh B(156 mg/g)for X=NH_(2).The adsorbents are also easily regenerated for three consecutive cycles without losing their *** finally demonstrate that MTV-MOFs can be designed to tune the dye removal selectivity and enhance the removal capacity of both MB and RhB in a binary aqueous solution of these dyes.

关键词： reaction-diffusion framework(RDF) multivariate metal-organic frameworks(MTV-MOFs) adsorption methylene blue(MB) rhodamine B(Rh B)

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Thermomechanical Analysis of (Cu_(0.5)Tl_(0.5))-1223 Substituted by Pr and La

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Journal of Materials Science & Technology 2012年第2期28卷 169-176页

作者： A.I.abou Aly R.Awad I.H.ibrahim M.Kamal M.Anas Physics Department Faculty of ScienceAlexandria University Physics Department Faculty of ScienceMansoura University

The thermomechanical analysis （TMA） of Cu0.5T10.5Ba2Ca2-xRxCu30110-δ, where R=Pr and La, with 0.0〈x〈0.15, was carried out in temperature range from 450 to 1145 K. The samples were prepared by singlestep solid state reaction technique. The prepared samples were characterized by X-ray diffraction （XRD） and scanning electron microscopy （SEM）. The superconductivity of the prepared samples was investigated by electrical resistivity measurement. The results showed that low substitution content enhanced the （Cu0.5Tlo.5）- 1223 phase formation, while the higher substitution content degraded this phase. The higher superconducting transition temperatures Tc were found to be 114 K and 109 K at x= 0.025 for Pr- and La-substitutions, respectively. The average linear thermal expansion coefficient increased as x increased, while the shrinkage temperature decreased as x increased. Those results were emphasized by porosity and Vickers microhardness calculations. Debye temperature 0D was calculated from the linear thermal expansion coefficient data and correlated to Tc to estimate the electron-phonon coupling λep.

关键词： (Cu0.5Tl0.5)-1223 Thermomechanical analysis Thermal expansion coefficient Debye temperature

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New scope on the relationship between rotifers and Biom phalaria alexandrina snails

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Asian Pacific Journal of Tropical Biomedicine 2013年第8期3卷 595-603页

作者： Shereen Farouk Mossallam Eglal ibrahim Amer Iman Fathy abou-El-Naga Medical Parasitology Department Faculty of MedicineAlexandria UniversityEgypt

Objective:To investigate the effect of rotifer internalization into snail tissue on the development of ***:Susceptible laboratory-bred Biomphalaria alexandrina(***)snails were exposed to lab-maintained rotifers;Philodinaspp.,two weeks before and after being infected with Schistosoma mansoni(***)*** consequent histopathological impact on snail tissues and cercarial biology were investigated before and after emergence from ***:Contamination of *** with philodina,two weeks before miracidial exposure,was found to hinder the preliminary development of *** inside the snail ***,when snails were contaminated with rotifers two weeks post miracidial exposure;growth of already established cercariae was found to be *** consequent influence of internalized rotifers within the snail tissue was clearly reflected on cercarial em ergence,activity and infectivity along the four weeks duration of *** the present study,comparison of snail histopathological findings and altered cercarial biology observed between the experimental and control groups indicated that the rotifers may have affected the levels of snail's energy reservoirs,which eventually was found to have had an adverse impacton reproduction,growth and survival of the parasite within the snail host,coupled with its performance outside the ***:In future biological control strategies of schistosomiasis,ritifers should be considered as a parasitic scourge of humanity.

关键词： Biomphalaria alexandrina Schistosoma mansoni Rotifers Snail histopathology Cercarial biology

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Electrical and mechanical properties of (Bi, Pb)-2223 substituted by holmium

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Journal of Advanced Ceramics 2016年第1期5卷 54-69页

作者： W.ABDEEN S.MARAHBA R.AWAD A.I.abou ALY I.H.ibrahim M.MATAR Superconductivity and Metallic Glass Lab Physics Department Faculty of ScienceAlexandria University Alexandria EgyptPhysics Department University College at Al-Gamom Umm Al-Qura University Saudi Arabia Physics Department Faculty of Science Beirut Arab University(BA U) Beirut Lebanon Superconductivity and Metallic Glass Lab Physics Department Faculty of ScienceAlexandria University Alexandria Egypt

The effect of the partial substitution of Ca2+ by Ho3+ ions on the electrical and mechanical properties of the superconducting phase (Bi,Pb)-2223 was studied. Superconducting samples of the type (Bi1.8Pb0.4)Sr2Ca2.1−x Ho x Cu3.1O10+δ were prepared by solid-state reaction technique under ambient pressure, and characterized by means of X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). The superconducting transition temperature T c and pseudogap temperature T* were estimated from electrical resistivity measurements, while the critical current density J c was determined from I–V curves. The electrical resistivity data were discussed according to bipolaron model in the absence of thermally excited individual polarons. The sample with x = 0.025 showed the highest phase volume fraction, T c, and J c. Room temperature Vickers microhardness measurements were carried out at different applied loads (0.25–5 N) in order to investigate the performance of the mechanical properties of (Bi1.8Pb0.4)Sr2Ca2.1−x Ho x Cu3.1O10+δ phase. It was found that all the samples exhibit normal indentation size effect (ISE). The Vickers microhardness number H V increased as x increased from 0 to 0.025. The experimental results were discussed in view of Meyer’s law, Hays–Kendall (HK) approach, elastic/plastic deformation (EPD) model, and proportional specimen resistance (PSR) model. The load independent (true) microhardness of (Bi1.8Pb0.4)Sr2Ca2.1−x Ho x Cu3.1O10+δ superconducting samples showed identical behavior to that of the PSR model.

关键词： (Bi,Pb)-2223 phase Ho substitution Vickers microhardness bipolaron model pesudogap temperature

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Bach-Einstein Gravitational Field Equations as a Perturbation of Einstein Gravitational Field Equations

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Applied Mathematics 2022年第12期13卷 1022-1032页

作者： Fathy ibrahim Abdel-Bassier Ahmed Fouad Abdel-Wahab fayrouz Mostafa Abdel-Maboud Mathematics Department Faculty of Science Minia University El-Minia Egypt Higher Institute for Engineering and Technology El-Minia Egypt

The Bach equations are a version of higher-order gravitational field equations, exactly they are of fourth-order. In 4-dimensions the Bach-Einstein gravitational field equations are treated here as a perturbation of Einstein’s gravity. An approximate inversion formula is derived which admits a comparison of the two field theories. An application to these theories is given where the gravitational Lagrangian is expressed linearly in terms of R, R2, |Ric|2, where the Ricci tensor Ric = Rαβdxαdxβ is inserted in some formulas which are of geometrical or physical importance, such as;Raychaudhuri equation and Tolman’s formula.

关键词： Gravitational Theory Higher Order Gravity Buchdahl’s Formula Bach-Einstein Gravitational Field Equations Raychaudhuri Equation Tolman’s Formula

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Improvement of Selected Morphological, Physiological, and Biochemical Parameters of Banana (Musa acuminata L.) Using Potassium Silicate under Drought Stress Condition Grown in vitro

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Phyton-International Journal of Experimental Botany 2023年第4期92卷 1019-1036页

作者： Hosny Abdel Aziz Mohamed Sharaf Magdy Omar Ahmed abou El-Yazied Nada ibrahim AlJwaizea Shaimaa Ismail Mohamed M.A.Omar Khadiga Alharbi Amr Elkelish Moataz Tawfik Department of Horticulture Faculty of AgricultureAl-Azhar UniversityCairo11651Egypt Department of Biochemistry Faculty of AgricultureAl-Azhar UniversityCairo11651Egypt Department of Biochemistry and Molecular Biology College of Marine Life SciencesOcean University of ChinaQingdao266003China Department of Agricultural Botany Faculty of AgricultureAl-Azhar UniversityNasr CityCairo11751Egypt Department of Horticulture Faculty of AgricultureAin Shams UniversityCairo11566Egypt Department of Biology College of SciencePrincess Nourah bint Abdulrahman UniversityRiyadh11671Saudi Arabia Department of Biochemistry Faculty of AgricultureAin Shams UniversityCairo11566Egypt Biology Department College of ScienceImam Mohammad ibn Saud Islamic University(IMSIU)Riyadh11623Saudi Arabia Botany Department Faculty of ScienceSuez Canal UniversityIsmailia41522Egypt Botany Department Faculty of SciencePort Said UniversityPort Said42511Egypt

Drought stress has become more common in recent years as a result of climate change impacts on the production of banana crops and other fruit *** growth and productivity of Musa spp are severely impacted by the gradual degradation of water resources and the erratic distribution pattern of annual precipitation *** aim of the work includes increased drought tolerance in light of water scarcity in the world as a result of the bananas’being gluttonous for water *** investigation was carried out from 2019 to 2020 to study the effect of potassium silicate on morphological growth and biochemical parameters of Musa acuminata L under drought stress by *** a result,drought stress reduced the morphological characteristics such as shoots number,shoot length,roots number,and survival percentage and biochemical characteristics such as chlorophyll a,b,carotenoids,stomatal status,and *** proline content increased in the leaf of *** *** complemented with K2SiO3(2 to 6 mM)either individually or in combination with PEG led to an improvement in all morphological and biochemical *** activities of CAT,POD,and PPO enzymes increased significantly compared to ***,the lowest PPO,CAT,and POD activity were ***,K2SiO3 treatments under drought stress successfully enhanced the leaf stomatal *** results suggest that K2SiO3 can help to maintain plant integrity in the tested cultivar under drought stress.

关键词： Musa acuminata L potassium silicate photosynthetic pigments stomata enzymatic activity

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Improving the Antioxidant Properties of Fermented Camel Milk Using Some Strains of <i>Lactobacillus</i>

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Food and Nutrition Sciences 2021年第4期12卷 352-371页

作者： Mahmoud ibrahim El-Sayed Sameh Awad Nagwa Hussein Ismail abou-Soliman Department of Dairy Technology Research Food Technology Research Institute ARC Giza Egypt Dairy Microorganisms and Cheese Research Laboratory (DMCR) Department of Dairy Science and Technology Faculty of Agriculture Alexandria University Alexandria Egypt Animal Breeding Department Animal and Poultry Production Division Desert Research Centre Matariya Cairo Egypt

This study aimed at improving the antioxidant capacity of fermented camel milk using some single strains of Lactobacillus (Lb. helveticus B-734, Lb. casei subsp. casei B-1922, Lb. paracasei subsp. paracasei B-4560, Lb... 详细信息

关键词： Camel Milk Fermented Milk Antioxidant Activity Lactobacillus

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Antioxidant Properties of Fermented Camel Milk Prepared Using Different Microbial Cultures

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Food and Nutrition Sciences 2022年第11期13卷 861-877页

作者： Nagwa Hussein Ismail abou-Soliman Mahmoud ibrahim El-Sayed Sameh Awad Department of Animal Breeding Animal and Poultry Production Division Desert Research Centre Cairo Egypt Department of Dairy Technology Research Food Technology Research Institute Agricultural Research Center Giza Egypt Department of Dairy Science and Technology Faculty of Agriculture Alexandria University Alexandria Egypt

This study investigated the effect of using different combinations of commercial starter culture and lactobacilli strains on the antioxidant properties of fermented camel milk for 14 days. The bacterial strains included Lb. casei subsp. casei B-1922, Lb. paracasei subsp. paracasei B-4560, Lb. rhamnosus B-442 and Lb. rhamnosus B-1445. The antioxidant activity of fermented milk was estimated using DPPH radical scavenging activity, ferrous ion chelating activity (FCA) and ferric reducing power assays. The total phenolic content (TPC), titratable acidity, proteolysis degree and sensory acceptability of samples were also evaluated. The results showed that all the studied parameters were affected by both the type of starter culture and storage. Samples containing the commercial starter and Lb. rhamnosus B-1445 had the highest DPPH radical scavenging activity and TPC throughout storage. Fermented milks prepared using the commercial starter and Lb. rhamnosus B-442 or Lb. paracasei retained their high FCA and reducing power throughout storage compared to the other samples. Fermented milk containing the commercial starter and Lb. casei showed the lowest antioxidant activity. The DPPH scavenging activity for all fermented milks decreased sharply during storage, while the change in FCA, reducing power and TPC differed among the samples during storage. The highest acidity was observed in the samples containing the commercial starter and Lb. paracasei, while fermented milk prepared using commercial starter and Lb. rhamnosus B-1445 had the lowest acidity. Samples containing the commercial starter and Lb. casei had the greatest proteolysis during the first week of storage, while samples containing the commercial starter and Lb. rhamnosus B-1445 had the highest proteolysis on day 14. Fermented milks with commercial starter and Lb. rhamnosus B-1445 or Lb. paracasei were the most acceptable products, while samples containing the commercial starter and Lb. casei were less acceptable.

关键词： Antioxidant Activity Fermented Camel Milk Lactobacilli

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Physico-Chemical Characterization of Sludge from the Goudel Drinking Water Production Plant in Niamey (Niger)

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Natural Resources 2022年第10期13卷 206-216页

作者： ibrahim Soumaïla Siddo Mahaman Moustapha Adamou Fayçal Moumouni abou Rural Engineering Water Resources and Forestry Department Faculty of Agronomy Abdou Moumouni University Niamey Niger

Population growth and increasing needs make our current societies a considerable source of environmental threats. Going towards sustainable cities where harmony exists between economic, socio-cultural and environmental issues is a necessity that is essential if we want to bequeath a livable world to future generations. Cities produce huge quantities of domestic and industrial waste, the management of which is becoming a growing problem for city managers. Located on the banks of the Niger River, the city of Niamey, capital of the Republic of Niger, is supplied with drinking water from this river. Significant quantities of sludge are produced by the plant following the treatment of this water. This study focuses on the physico-chemical characterization of this sludge which is now directly discharged into the Niger River. A total of 12 samples of pasty sludge taken from the pre-settling ponds were analyzed. The samples were previously dried, crushed, sieved and packaged. Physical (pH, EC and particle size), chemical (Ca, Mg, Na, K, CEC, AE, P, C, MO and N) and metallic trace elements (Pb, Ni, Cu, Zn, Cd, Mn) parameters and Al) were analyzed in the laboratory. The results show that the sludge is weakly acidic (pH between 4.16 and 5.71), conductive (<0.35 mS/cm) and rich in fine elements (12.1% to 77.71% clay). The nutrient content is low in nitrogen (<0.25%), phosphorus (<2.5 ppm), potassium (between 1 to 188 Mèq/100g) and organic matter (less than 2.88%). The concentrations of ETM comply with the values admissible in residual materials (French decree of 08/01/1998). This sludge can be recovered, especially in agriculture.

关键词： Sludge Potable Water Water Treatment Niger River Niamey

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The Impact of Microbial Transglutaminase on the Quality and Antioxidant Activity of Camel-Milk Soft Cheese

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Food and Nutrition Sciences 2020年第3期11卷 153-171页

作者： Nagwa Hussein Ismail abou-Soliman Sameh Awad Mahmoud ibrahim El-Sayed Animal Breeding Department Animal and Poultry Production Division Desert Research Centre Matariya Cairo Egypt Department of Dairy Science and Technology Faculty of Agriculture Alexandria University Alexandria Egypt Department of Dairy Technology Research Food Technology Research Institute Agricultural Research Center Giza Egypt

This study aimed at investigating the impact of adding microbial transglutaminase (MTGase) after rennet addition on some properties of fresh soft cheese made from camel milk. MTGase was added to milk at concentration of 80, 100 and 120 U/L after 20 and 30 min of renneting. The chemical composition, yield, hardness, antioxidant activity and sensory properties of cheese were estimated. Enzymatic protein crosslinking was analyzed by SDS-PAGE. Results revealed that MTGase-treated cheeses were higher in moisture and lower in protein content compared to control. In addition, the concentration of MTGase and time of addition significantly (P 0.05) impacted these parameters. Among treated cheeses, samples with 80 U of MTGase and addition time of 20 min were the highest in total solids and protein content. Adding MTGase significantly (P 0.05) increased the cheese yield, however, increased MTGase concentration at any time of addition did not improve it. The electrophoretic patterns of MTGase-cheese proteins showed a reduction in the intensity of caseins bands and the appearance of new protein fractions with high molecular weights. However, the changes in the intensity of the whey proteins bands were not sufficiently clear as caseins. The cheese hardness was significantly (P 0.05) affected by adding MTGase. Cheese containing 80 U of MTGase had the highest hardness value compared to control and other treated samples. The antioxidant activity of cheese was negatively influenced by adding the enzyme. The use of MTGase enhanced the mouthfeel, texture and overall acceptability of cheese. However, the effect of MTGase concentration and addition time was not significant (P > 0.05) on the sensory attributes. In conclusion, adding MTGase to milk at concentration of 80 U after 20 min of renneting is recommended to improve the yield, textural and some sensory properties of fresh soft cheese made from camel milk.

关键词： Camel Milk Soft Cheese Transglutaminase Texture and Yield Antioxi-dant Activity

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