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色谱 2008年第3期26卷 358-361页

作者： SHAHED Mirza NANDA Rabindra DEHGHAN Muhammad Hassan NASREEN Huda feroz shaikh Maulana Azad Educational Trust’s Y.B.Chavan College of Pharmacy Dr.Rafiq Zakaria CampusRauza BaghAurangabad-431001Maharashtra StateIndia Maulana Azad Educational Trust’s Y.B.Chavan College of Pharmacy Dr.Rafiq Zakaria CampusRauza BaghAurangabad-431001 Maharashtra StateIndia

A reversed-phase high performance liquid chromatography (HPLC) method was developed, validated, and used for the quantitative determination of gatifloxacin (GA) and ambroxol hydrochloride (AM), from its tablet dosage form. Chromatographic separation was performed on a HiQ Sil C18 column (250 mm×4.6 mm, 5 μm), with a mobile phase comprising of a mixture of 0.01 mol/L potassium dihydrogen orthophosphate buffer and acetonitrile (70∶30, v/v), and pH adjusted to 3 with orthophosphoric acid, at a flow rate of 1 mL/min, with detection at 247 nm. Separation was completed in less than 10 min. As per International Conference on Harmonisation (ICH) guidelines the method was validated for linearity, accuracy, precision, limit of quantitation, limit of detection, and robustness. Linearity of GA was found to be in the range of 10-60 μg/mL and that for AM was found to be 5-30 μg/mL. The correlation coefficients were 0.999 6 and 0.999 3 for GA and AM respectively. The results of the tablet analysis (n=5) were found to be 99.94% with ±0.25% standard deviation (SD) and 99.98% with±0.36% SD for GA and AM respectively. Percent recovery of GA was found to be 99.92%-100.02% and that of AM was 99.86%-100.16%. The assay experiment shows that the method is free from interference of excipients. This demonstrates that the developed HPLC method is simple, linear, precise, and accurate, and can be conveniently adopted for the routine quality control analysis of the tablet.

关键词：氢氯化物高效液体色谱分析分析方法药物剂量

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Melting Characteristics of a Phase Change Material Mixed with Nano Particles of Cobalt Oxide Bounded in a Trapezoidal Structure

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Computer Modeling in Engineering & Sciences 2022年第1期130卷 255-268页

作者： Waris Ali Asif Ali shaikh feroz Shah Sajjad Hussain Department of Basic Sciences and Related Studies Mehran University of Engineering and TechnologyJamshoroPakistan School of Mechanical and Aerospace Engineering Nanyang Technological UniversitySingapore Department of Mathematics Govt Postgraduate College LayyahPunjabPakistan

A novel trapezoidal design for storage of heat energy through melting of phase-change material(PCM)is *** heat thermal energy storage system(LHTES)is a promising option to diminish mis-match between energy consumption and *** this purpose,Paraffin:Rubitherm-35(RT35)material is successively melted in aluminum structure which is heated from one side and the other sides are kept *** of PCM is observed experimentally and melt fronts are photographed for various time *** fluid-solid module in COMSOL Multiphysics 5.4 has been *** transient heat conduction with enthalpy function is *** are carried out for enhancement of thermal conductivity through addition of nano-entities of cobalt oxide *** time is notably reduced with inclusion of nano-entities to enhance thermal *** time spans for melt start and total melt in case of pure PCM are 375 and 4500(s)respectively whereas for the nano mix case,these are 150 and 3000 *** 33%shorter time length is noticed for charging of the PCM trapezoidal matrix with nano entities of Co3O4 *** results fromsimulation and lab observations depict similar patterns and are in quite close comparison.

关键词： Trapezoidal enclosure nano entities heat transfer phase change material COMSOL multiphysics 5.4 numerical simulation

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