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Effects of Hybrid Voltages on Oxide Formation on 6061 Al-alloys During Plasma Electrolytic Oxidation

Chinese Journal of Aeronautics 2009年第5期22卷 564-568页

作者： Kai Wang Bon Heun Koo Chan Gyu Lee Young Joo Kim Sunghun Lee eungsun byon School of Nano & Advanced Materials Engineering Changwon National University Changwon 641-773 Korea Surface Technology Research Center Korea Institute of Materials Science Changwon 641-010 Korea

Plasma electrolytic oxidation （PEO） is carried out on 6061 Al-alloys in a weak alkaline electrolyte containing NaOH, Na2SiO3 and NaCl. Centered on the correlation of composition and structure, analyses by means of X-ray diffration （XRD）, scanning electron microscope （SEM） and energy dispersive spectrometry （EDS） are conducted on the specimens, which have been PEO-treated under hybrid voltages of different direct current （DC） values （140-280 V） with constant alternate current （AC） amplitude （200 V）. Attention is paid to the composition, properties and growth mechanism of oxide layers formed with hybrid voltages. Moreover, the main effects of DC value are discussed. Ceramic layers with a double-layer structure which combines hard outer and soft inner layers are found to be consist of α-Al2O3,γ-Al2O3 and mullite. With the DC values increasing, the growth of the ceramic layers tends to have increasingly obvious three-stage feature.

关键词： plasma electrolytic oxidation oxide layer aluminum alloys alkaline electrolyte hybrid voltages

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Effects of electrolytes variation on formation of oxide layers of 6061 Al alloys by plasma electrolytic oxidation

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中国有色金属学会会刊：英文版 2009年第4期19卷 866-870页

作者： Kai WANG Bon-Heun KOO Chan-Gyu LEE Young-Joo KIM Sung-Hun LEE eungsun byon School ofNano ＆ Advanced Materials Engineering Changwon National University Changwon 641-773 Korea Surface Technology Research Center Korea Institute of Materials Science Changwon 641-010 Korea

Plasma electrolytic oxidation(PEO) processes were carried out to produce ceramic layers on 6061 aluminum substrates in four kinds of electrolytes such as silicate and aluminate solution with and without sodium *** PEO processes were carried out under a hybrid voltage(260 V DC combined with 200 V,60 Hz AC amplitude) at room temperature for 5 *** composition,microstructure and element distribution analyses of the PEO-treated layers were carried out by XRD and SEM & *** effect of the electrolyte contents on the growth mechanism,element distribution and properties of oxide layers were *** is obvious that the layers generated in aluminate solutions show smoother surfaces than those in silicate ***,an addition of fluorine ion can effectively control the layer porosity;therefore,it can enhance the properties of the layers.

关键词：等离子电解氧化 6061合金氧化层对格质变等离子体电解氟硅酸钠铝酸钠溶液

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