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Biological silicon nanoparticles improve Phaseolus vulgaris L. yield and minimize its contaminant contents on a heavy metals-contaminated saline soil

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Journal of Environmental Sciences 2021年第8期33卷 1-14页

作者： mohamed T.el-Saadony el-sayed m.desoky Ahmed m.Saad Rania S.m.Eid Eman Selem Ahmed S.elrys Department of Agricultural microbiology Faculty of AgricultureZagazig UniversityZagazig 44511Egypt Botany Department Faculty of AgricultureZagazig UniversityZagazig 44511Egypt Biochemistry Department Faculty of AgricultureZagazig UniversityZagazig 44511Egypt Agricultural Botany Department Faculty of AgricultureBenha University13736Egypt Botany and microbiology Department Faculty of ScienceZagazig University44511Egypt Soil Science Department Faculty of AgricultureZagazig University44511ZagazigEgypt

The synthesis of biological silicon nano-particles(Bio-Si-NPs)is an eco-friendly and lowcost *** is no study focusing on the effect of Bio-Si-NPs on the plants grown on saline soil contaminated with heavy *** this study,an attempt was made to synthesis Bio-Si-NPs using potassium silica florid substrate,and the identified Aspergillus tubingensis Am11 isolate that separated from distribution systems of the potable water.A twoyear field trial was conducted to compare the protective effects of Bio-Si-NPs(2.5 and 5.0 mmol/L)and potassium silicate(10 mmol/L)as a foliar spray on the antioxidant defense system,physio-biochemical components,and the contaminants contents of Phaseolus vulgaris *** on saline soil contaminated with heavy *** findings showed that all treatments of Bio-Si-NPs and potassium silicate significantly improved plant growth and production,chlorophylls,carotenoids,transpiration rate,net photosynthetic rate,stomatal conductance,membrane stability index,relative water content,free proline,total soluble sugars,N,P,K,Ca2+,K+/Na+,and the activities of peroxidase,catalase,ascorbic peroxidase and superoxide oxide *** of Bio-Si-NPs and potassium silicate significantly decreased electrolyte leakage,malondialdehyde,H2 O2,O2·-,Na+,Pb,Cd,and Ni in leaves and pods of Phaseolus vulgaris *** to ***-Si-NPs were more effective compared to potassium *** of Bio-Si-NPs at the rate of 5 mmol/L was the recommended treatment to enhance the performance and reduce heavy metals content on plants grown on contaminated saline soils.

关键词： Bean Silicon Nano-silicon Aspergillus tubingensis Am11 Salinity Heavy metals

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Spirulina platensis extract improves the production and defenses of the common bean grown in a heavy metals-contaminated saline soil

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Journal of Environmental Sciences 2023年第7期129卷 240-257页

作者： mostafa m.Rady Ahmed S.elrys Eman Selem Ahmed A.A.mohsen Safaa m.A.I.Arnaout Ahmed H.el-Sappah Khaled A.el-Tarabily el-sayed m.desoky Botany Department Faculty of AgricultureFayoum UniversityFayoum 63514Egypt College of Tropical Crops Hainan UniversityHaikou 570228China Soil Science Department Faculty of AgricultureZagazig UniversityZagazig 44511Egypt Botany and microbiology Department Faculty of ScienceZagazig UniversityZagazig 44511Egypt Horticulture Department Faculty of AgricultureZagazig UniversityZagazig 44511Egypt Botany Department Faculty of AgricultureZagazig UniversityZagazig 44511Egypt Genetics Department Faculty of AgricultureZagazig UniversityZagazig 44511Egypt Department of Biology College of ScienceUnited Arab Emirates UniversityAl-Ain 15551United Arab Emirates Khalifa Center for Genetic Engineering and Biotechnology United Arab Emirates UniversityAl-Ain 15551United Arab Emirates Harry Butler Institute Murdoch UniversityMurdoch 6150Australia

Plants have to cope with several abiotic stresses,including salinity and heavymetals(Hms).Under these stresses,several extracts have been used as effective natural biostimulants,however,the use of Spirulina platensis(SP)extract(SPE)remains *** effects of SPE were evaluated as soil addition(SA)and/or foliar spraying(FS)on antioxidant defenses and Hms content of common bean grown in saline soil contaminated with ***(40 or 80 mg SPE/hill added as SA or 20 or 40 mg SPE/plant added as FS)or integrative(SA+FS)applications of SPE showed significant improvements in the following order:SA-80+FS-40>SA-80+FS-20>SA-40+FS-40>SA-40+FS-20>SA-80>SA-40>FS-40>FS-20>***,the integrative SA+FS with 40 mg SP/plant was the most effective treatment in increasing plant growth and production,overcoming stress effects and minimizing contamination of the edible *** significantly increased plant growth(74%–185%)and yield(107%–227%)by enhancing net photosynthetic rate(78.5%),stomatal conductance(104%),transpiration rate(124%),and contents of carotenoids(60.0%),chlorophylls(49%–51%),and NPK(271%–366%).These results were concurrent with the marked reductions in malondialdehyde(61.6%),hydrogen peroxide(42.2%),nickel(91%–94%),lead(80%–9%),and cadmium(74%–91%)contents due to the improved contents of glutathione(87.1%),ascorbate(37.0%),andα-tocopherol(77.2%),and the activities of catalase(18.1%),ascorbate peroxidase(18.3%),superoxide dismutase(192%),and glutathione reductase(52.2%)as reinforcing ***,this most effective treatment is recommended to mitigate the stress effects of salinity and Hms on common bean production while minimizing Hms in the edible part.

关键词： Antioxidant defense system Biostimulants Heavy metals microalgae extracts Saline soil Soil pollution

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Use of breakthrough experiment to evaluate the performance of hydrogen isotope separation for metal-organic frameworks m-mOF-74(m=Co, Ni, mg, Zn)

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Science China Chemistry 2020年第7期63卷 881-889页

作者： Yanan Si Wenjing Wang el-sayed m.el-sayed Daqiang Yuan State Key Laboratoty of Structural Chemistry Fujian Institute o f Research on the Structure of MatterChinese Academy of SciencesFuzhou 350002China University of the Chinese Academy of Sciences Beijing 100049China Chemical Refining Laboratory Refining DepartmentEgyptian Petroleum Research InstituteNasr CityCairoEgypt

The unique adsorption performance of metal-organic frameworks(mOFs) indicates a new direction for gas separation and purification. The low-temperature distillation, as a traditional technique for hydrogen isotope separation, is limited as it is a high energy-and cost-intensive process. Instead of utilizing such a conventional separation route, we use ordered microporous frameworks based on a physical adsorption mechanism to solve the challenge of hydrogen isotope separation. Herein we analyze m-mOF-74(m=Co, Ni, mg, Zn), featuring a hexagonal channel about 11 ? and high density of open metal sites, for their ability to separate and purify deuterium from the hydrogen isotope mixture by dynamic column breakthrough experiments. Our results show that the combination of the strength of binding sites, density of coordinatively unsaturated metal sites and hydrogen isotope adsorption capacity of materials renders Co-mOF-74 as an optimal adsorbent for the capture of deuterium from hydrogen isotope mixtures in a simulated industrial process.

关键词： hydrogen isotope separation breakthrough experiment mOF-74

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Effects of Nickel Distribution on the Strengthening and Toughening of Alumina Ceramics

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Journal of materials Science & Technology 2008年第5期24卷 723-728页

作者： mohamed.m.el-sayed Seleman Department of materials and metallurgical Eng. Faculty of Petroleum and Mining Eng.Post Code 43721SuezEgypt

Three types of composite materials were designed and fabricated by hot pressing powder blends of alumina with 20 vol. pct nickel particles. The composites differ in the shape, size and distribution of the nickel particles. Composite microstructures are described and measurements of density, hardness, flexure strength, and fracture toughness are reported. The results showed that the fracture strength of the composite with dispersed nickel particles is higher than the other two composites （network microstructure and mixed microstructure） and the alumina matrix. For all the composites studied, tougher materials than the monolithic alumina were produced. The fracture toughness of the composite with a network microstructure is much higher than that of the other composites. The toughening mechanisms were described based on the observation of the fracture surfaces and the crack-particle interactions. moreover, the parameters for microstructural tailoring of these materials have been deduced. The toughening of the produced composites was explained in light of the interracial bond strength.

关键词： Alumina-nickel composites Nickel morphology Interfacial bonding Fracturetoughness Flexure strength

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FIRST-ORDER mETHODS FOR SOLVING THE OPTImAL STATIC H∞-SYNTHESIS PROBLEm

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Journal of Computational mathematics 2007年第6期25卷 672-689页

作者： el-sayed m.E. mostafa Department of mathematics Faculty of Science Alexandria University Alexandria Egypt

In this paper, we consider the static output feedback （SOF） H∞-synthesis problem posed as a nonlinear semi-definite programming （NSDP） problem. Two numerical algorithms are developed to tackle the NSDP problem by solving the corresponding Karush- Kuhn-Tucker first-order necessary optimality conditions iteratively. Numerical results for various benchmark problems illustrating the performance of the proposed methods are given.

关键词： Static output feedback H∞-synthesis Semi-definite programming Nonlinear programming.

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Processing of Ceramic Based Nanocomposite Usingα-Al_2O_3 Powder and FeCl_2 Solution as Starting materials

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Journal of materials Science & Technology 2007年第6期23卷 837-842页

作者： mohamed m.el-sayed Seleman Department of materials and metallurgical Engineering Faculty of Petroleum and Mining EngineeringPost Code 43721SuezEgypt

Alumina-iron nanocomposite powders were prepared by a two-step process. In the first step, α-Al2O3-FeCl2 powder mixture was formed by mixing α-Al2O3 powders with FeCl2 solution followed by drying. In the second step, the FeCl2 in the dry power mixture was selectively reduced to iron particles. A reduction temperature of 750℃ for 15 min in dry H2 was chosen based on the thermodynamic calculations. The concentration of iron in FeCl2 solution was calculated to be 20 vol. pct in the final composite. Two techniques were used to produce composite bulk materials. The Al2O3 nanocomposite powders were divided to two batches. The first batch of the produced mixture was hot pressed at 1400℃ and 27 mPa for 30 min in a graphite die. To study the effect of oxygen on the Al2O3/Fe interface bonding and mechanical properties of the composite, the second batch was heat treated in air at 700℃ for 20 min to partially oxidize the iron particles before hot pressing. Characterization of the composites was undertaken by conventional density measurements, X-ray diffractometry （XRD）, scanning electron microscopy （SEm）, transmission electron microscopy （TEm） and electron probe micro analysis （EPmA）. The suggested processing route （mixing, reduction and hot pressing） produces ceramic-metal nanocomposite much tougher than the pure Al2O3. The fracture strength of the produced Al2O3/Fe nanocomposite is nearly twice that of the pure Al2O3. The presence of spinel phase, FeAl204, as thick layer around the Fe particles in the Al2O3 matrix has a detrimental effect on interfacial bonding between Fe and AI203 and the fracture properties of the composite.

关键词： Ferrous chloride Reduction Alumina-iron nanocomposite Spinel phase

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Thermal explosion of a reactive gas mixture at constant pressure for non-uniform and uniform temperature systems

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Defence Technology（防务技术） 2022年第10期18卷 1842-1851页

作者： Saad A.el-sayed mechanical Power Engineering Dept.Zagazig University ZagazigAlshrkiaEgypt

In this study,the approximate and exact solutions for the stationary-state of the solids model with neglecting reactant consumption for both non-uniform and uniform temperature systems were applied on gas ignition under a constant pressure *** criticality conditions for a slab,an infinite cylinder,and a sphere are determined and discussed using dimensionless temperatures under constant ambient and surface temperatures for a non-uniform temperature *** solution for a Semenov model with convection heat loss was also *** solution of the Semenov problem for constant volume or density as a solid and constant pressure were *** critical parameterδis calculated and compared with those of Frank-Kamenetskii solution *** validation of the calculated ignition temperatures with other exact solution and experimental results were *** relation between critical parameters form Semenov and *** solution was introduced.

关键词： Thermal explosion Approximate solution Critical conditions Distributed and uniform temperature systems

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The competitive and synergistic effect between adsorption enthalpy and capacity in D_(2)/H_(2)separation of m_(2)(m-dobdc)frameworks

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Chinese Chemical Letters 2021年第11期32卷 3562-3565页

作者： Fan Wu Liqiong Li Yanxi Tan el-sayed m.el-sayed Daqiang Yuan State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of MatterChinese Academy of SciencesFuzhou 350002China University of the Chinese Academy of Sciences Beijing 100049China College of Chemistry Fuzhou UniversityFuzhou 350108China Chemical Refining Laboratory Refining DepartmentEgyptian Petroleum Research InstituteNasr CityCairo 11727Egypt

Hydrogen isotope separation is a challenging task due to their similar ***,based on the chemical affinity quantum sieve(CAQS)effect,the D_(2)/H_(2)separation performance of m_(2)(m-dobdc)(m=Co,Ni,mg,mn;m-dobdc^(4-)=4,6-dioxido-1,3-benzenedicarboxylate),a series of honeycomb-shaped mOFs with high stability and abundant open metal sites,are studied by gases sorption and breakthrough experiments,in which two critical factors,gas uptake and adsorption enthalpy,are taken into *** these mOFs,Co_(2)(m-dobdc)exhibits the longest D_(2)retention time of 180 min/g(H_(2)/D_(2)/Ne:1/1/98)at 77 K because of its second-highest adsorption enthalpy(10.7 kJ/mol for H_(2)and 11.8 kJ/mol for D_(2))and the best sorption capacity(5.22 mmol/g for H_(2)and 5.49 mmol/g for D_(2))under low pressure of 1 kPa and 77 K,which make it a promising material for industrial hydrogen isotope ***,the results indicate that H_(2)and D_(2)capacities under low pressure(about 1 kPa)dominate the final D_(2)/H_(2)separation property of mOFs.

关键词： Breakthrough experiment Open metal sites Hydrogen isotope separation Sorption and separation Chemical affinity quantum sieve

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Yttria Tetragonal Zirconia Biomaterials:Kinetic Investigation

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Journal of materials Science & Technology 2011年第4期27卷 332-337页

作者： Ezzat S.elshazly S.m.el-Hout m.el-sayed Ali Department of mechanical Engineering Virginia Commonwealth University Deptartment of metallurgy Nuclear Research CenterAtomic Energy Authority

The low temperature aging behavior of polycrystalline tetragonal zirconia was investigated to explore the effects on phase transformation occurring during the process. XRD analysis was conducted for the phase identification and the tetragonal to monoclinic phase transformation was determined. The aging of tetragonal zirconia polycrystals doped with 3 mol% Y203 triggers tetragonal to monoclinic phase transformation on the surface of the specimen only, while the penetration inside the bulk of the specimen is very limited. A slight decrease in the mechanical properties was also observed after aging for 40 h. The transformation kinetics show a nucleation and growth mechanism on the specimen surface to be dominant in the low temperature aging in water environment.

关键词： Low temperature degradation 3Y-TZP Kinetics

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electrical Conductivity and Sensitive Characteristics of Ag-Added BaTiO_3-CuO mixed Oxide for CO_2 Gas Sensing

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Journal of materials Science & Technology 2011年第1期27卷 35-40页

作者： A.m.el-sayed F.m.Ismail S.m.Yakout Inorganic Chemistry Department National Research CentreTahrir StreetDokki P.C.12622 CairoEgypt

Carbon dioxide gas sensors based on BaTiO3-CuO composite with different concentrations of Ag addition（1,1.5 and 2 wt%） have been prepared by stander ceramic method and sintered at 500 and 700℃ for 5 *** conductivity and gas sensing properties of the prepared samples were *** conductivity measurement was used to characterize the obtained sintered sensor *** was found that electrical conductivity and the sensitivity to CO2 were improved with Ag addition and *** correlation between Ag content at different sintering temperature and sensing characteristics towards CO2 is discussed.

关键词： BaTiO3-CuO composite Ag addition electrical conductivity CO2 sensitive properties

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