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Microstructure and phase formation of mullite-Pr6O11 composite prepared by spark plasma sintering

Journal of Rare Earths 2023年第2期41卷 283-289页

作者： ehsan ghasali Davoud Ghahremani Yasin Orooji Aida Faeghi-nia Asghar Kazem-zadeh Touradj Ebadzadeh College of Geography and Environmental Sciences Zhejiang Normal UniversityJinhua 321004China Ceramic Dept. Materials and Energy Research CenterAlborzIran Department of Engineering Maybod BranchIslamic Azad UniversityMaybodIran

The present work investigates the effect of high praseodymium oxide(Pr6O11)content on the microstructure and phase formation of mullite(3Al_(2)O_(3)·2SiO_(2))precursor by means of the spark plasma sintering process.30 wt%Pr6O11was added to a mullite precursor consisting of aluminum nitrate nonahydrate and tetraethyl orthosilicate through a high energy mixer mill in ethanol *** spark plasma sintering was performed at a te mperature of 1200℃under 23 Pa vacuum co nditions by applying initial and final pressure of 10 and 30 MPa,*** analysis confirms the existence of mullite,alumina,Pr6O11,Pr2O3and quartz as the only crystalline *** images reveal an interesting deposition of hexagonal-shaped Al_(2)O_(3)particles on polished surfaces and complex oxide phases of the fiber network adhering to alumina particles in the form of tails seen on the fracture ***,the bending strength of 213±21 MPa,Vickers hardness of 9.3±0.1 MPa and fracture toughness of6.21±0.12 MPa·m1/2are obtained for the prepared composite.

关键词： Mullite Pr6O11 Composite Spark plasma sintering Rare earths

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Comprehensive insights into recent innovations:Magnesium-inclusive high-entropy alloys

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Journal of Magnesium and Alloys 2024年第4期12卷 1311-1345页

作者： Andrii Babenko ehsan ghasali Saleem Raza Kahila Baghchesaraee Ye Cheng Asif Hayat Peng Liu Shuaifei Zhao Yasin Orooji Shandong Vocational and Technical University of International Studies Rizhao 276826China Zhejiang Normal University Jinhua 321004China Geelong Institute for Frontier MaterialsDeakin UniversityVIC 3216Australia

This review focuses on thermodynamic and physical parameters,synthesis methods,and reported phases of Magnesium(Mg)containing high-entropy alloys(HEAs).Statistical data of publications concerning Mg-containing HEAs were collected and *** on the chemical elements included in Mg-containing HEAs,their theoretical end experimental densities,thermodynamic parameters,physical parameters,fabricated techniques and reported phases were also collected and *** the basis of this information,a new classification for HEAs was *** is also shown that the existing thermodynamic parameters cannot accurately predict the formation of a single phase solid solution for Mg-containing *** physical parameters of Mg-containing HEAs are within a wide range,and most of the synthesized Mg-containing HEAs have a complex multiphase structure.

关键词： Magnesium High-entropy alloys Classification Thermodynamic parameters Physical parameters

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