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Process intensification for the synthesis and purification of battery-grade Li_(2)CO_(3)with microfluidics

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Particuology 2024年第7期90卷 106-117页

作者： Haodu Li Jie Zhang Lin Dai Le du Jiqin Zhu The State Key Laboratory of Chemical Resource Engineering College of Chemical EngineeringBeijing University of Chemical TechnologyBeijing 100029China

Battery-grade lithium carbonate(Li_(2)CO_(3))with a purity of higher than 99.5 wt%is of great importance as a high value-added lithium ***,influences of different reaction systems and process control on product purity remain ***,a membrane dispersion microreactor was used to enhance the mass transfer of preparation and purification processes in homogeneous and heterogeneous *** systems of Na_(2)CO_(3)–LiCl,NH_(4)HCO_(3)–LiCl,and NH_(3)·H_(2)O−CO_(2)−LiCl,CO_(2)purification based on carbonation and decomposition were *** Li_(2)CO_(3)purity was increased by the improvement of mixing *** carbonation time was reduced by 62.5%and 58.3%for the NH_(3)·H_(2)O−CO_(2)and CO_(2)purification systems,*** the two ammonia-based systems,Li_(2)CO_(3)particles with a purity of 99.7–99.8 wt%were one-step prepared with a size of 3–5μm,which also met the requirement of the battery-grade *** purity was further increased to 99.9 wt%by CO_(2)purification and LiHCO_(3)*** investigation could provide a feasible alternative for the controllable preparation of battery-grade Li_(2)CO_(3)in one or multiple steps.

关键词： Microfluidics Battery grade Li_(2)CO_(3) Process intensification High purity

Real-Time Energy Management for Net-Zero Power Systems Based on Shared Energy Storage

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Journal of Modern Power Systems and Clean Energy 2024年第2期12卷 371-380页

作者： Pengbo du Bonan Huang Ziming Liu Chao Yang Qiuye Sun School of Information Science and Engineering Northeastern UniversityShenyang 110004China Information and Communication Branch State Grid Liaoning Electric Power Company Ltd.Shenyang 110004China IEEE

Battery energy storage systems(BESSs)serve a crucial role in balancing energy fluctuations and reducing carbon emissions in net-zero power ***,the efficiency and cost performance have remained significant challenges,which hinders the widespread adoption and development of *** address these challenges,this paper proposes a real-time energy management scheme that considers the involvement of prosumers to support net-zero power *** scheme is based on two shared energy storage models,referred to as energy storage sale model and power line lease *** energy storage sale model balances real-time power deviations by energy interaction with the goal of minimizing system costs while generating revenue for shared energy storage providers(ESPs).Additionally,power line lease model supports peer-to-peer(P2P)power trading among prosumers through the power lines laid by ESPs to connect each *** model allows ESP to earn profits from the use of power lines while balancing power deviations and better consuming renewable *** results validate the effectiveness of the proposed scheme,ensuring stable power supply for net-zero power systems and providing benefits for both the ESP and prosumers.

关键词： Shared energy storage energy storage provider(ESP) energy management peer-to-peer(P2P)trading net-zero power system

Infrared radiation characteristics of dagger-type hypersonic missile

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Chinese Journal of Aeronautics 2024年第4期37卷 137-150页

作者： Xubo du Qingzhen YANG Haoqi YANG Jin BAI Yongqiang SHI School of Power and Energy Northwestern Polytechnical UniversityXi’an 710129China

Hypersonic vehicles emit strong infrared radiation from their high-temperature exhaust plume and body, which is critical for infrared early warning, tracking, and guidance. In this work, a comprehensive analysis is conducted on the factors involved in air dissociation reaction within the shock layer of hypersonic missile heads, as well as the multi-component afterburning effect of the exhaust plume. A novel Reverse Monte Carlo Method(RMCM) is proposed for infrared radiation calculation, which utilizes two-dimensional Low-Discrepancy Sequences(LDS) to improve computational accuracy. The numerical calculations for a dagger-type missile show that afterburning reactions increase the temperature on the centerline of the outlet exhaust plume by about 1000 K. The total infrared radiation intensity of the missile is the highest in the 1–3 μm band, with the hightemperature wall of the nozzle being the primary source of solid radiation, and gas radiation primarily coming from H_(2)O. The radiation intensity of the missile exhaust plume in the 3–5 μm band is the highest, with radiation sources primarily coming from CO_(2), CO, and HCl. Afterburning reactions of the exhaust plume increase the total infrared radiation intensity of the missile by about 0.7times. These results can provide reference for the detection and guidance of hypersonic missiles.

关键词： Hypersonic vehicles Infrared radiation Monte Carlo methods Low-discrepancy sequences Exhaust plume Afterburning

Feature-aided pose estimation approach based on variational auto-encoder structure for spacecrafts

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Chinese Journal of Aeronautics 2024年第8期37卷 329-341页

作者： Yanfang LIU Rui ZHOU Desong du Shuqing CAO Naiming QI Department of Aerospace Engineering Harbin Institute of TechnologyHarbin 150001China Suzhou Research Institute of HIT Suzhou 215104China Shanghai Institute of Spaceflight Control Technology Shanghai 201109China Shanghai Key Laboratory of Aerospace Intelligent Control Technology Shanghai 201109China

Real-time 6 Degree-of-Freedom(DoF)pose estimation is of paramount importance for various on-orbit *** from the development of deep learning,Convolutional Neural Networks(CNNs)in feature extraction has yielded impressive achievements for spacecraft pose *** improve the robustness and interpretability of CNNs,this paper proposes a Pose Estimation approach based on Variational Auto-Encoder structure(PE-VAE)and a Feature-Aided pose estimation approach based on Variational Auto-Encoder structure(FA-VAE),which aim to accurately estimate the 6 DoF pose of a target *** methods treat the pose vector as latent variables,employing an encoder-decoder network with a Variational Auto-Encoder(VAE)*** enhance the precision of pose estimation,PE-VAE uses the VAE structure to introduce reconstruction mechanism with the whole ***,FA-VAE enforces feature shape constraints by exclusively reconstructing the segment of the target spacecraft with the desired *** evaluation against leading methods on public datasets reveals similar accuracy with a threefold improvement in processing speed,showcasing the significant contribution of VAE structures to accuracy enhancement,and the additional benefit of incorporating global shape prior features.

关键词： Pose estimation Variational auto-encoder Feature-aided Pose Estimation Approach On-orbit measurement tasks Simulated and experimental dataset

Distributed power conditioning unit of large-scale space solar power station

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Chinese Journal of Aeronautics 2024年第8期37卷 421-434页

作者： Xintong LI Jianwei MI Yiqun ZHANG Guanheng FAN Jie du School of Mechano-electronic Engineering Xidian UniversityXi’an 710071China Shaanxi Key Laboratory of Space Solar Power Station System Xidian UniversityXi’an 710071China Academy of Advanced Interdisciplinary Research Xidian UniversityXi’an 710071China

In this paper,a multi-bus distributed Power Conditioning Unit(PCU)is proposed for the Space Solar Power Station with large scale photovoltaic(PV)array and power levels reaching MW *** this unit,there are multiple independent PV *** each PV array,there are multiple independent PV *** this paper,a V-P droop control method with adaptive droop coefficient is proposed,which modifies the droop intercept based on the bus voltage deviation and the power per unit value of the PV *** method ensures the accuracy of bus voltage and achieves proportional distribution of power between PV arrays based on the proposed topology structure in this *** the load changes or the output power of the PV array fluctuates,this method can ensure that power is distributed *** principle and control method of the proposed droop control method is analyzed in this *** effectiveness of the method is verified through MATLAB/Simulink simulation and *** and experimental results show that the proposed method can achieve power distributed proportionally when load changes and PV output power fluctuates,reduce bus voltage error caused by line impedance and differences in rated power of different PV arrays,and improve the performance of PV power generation system applied to space.

关键词： Space Solar Power Station Photovoltaics Droop control DC confluence Power conditioning unit

Polyoxometalates as the redox anolyte for efficient conversion of biomass to formic acid

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A stepwise approach to enhancing flotation of low-grade zinnwaldite through the cationic/DL-2-octanol/anionic reagent combinations: Behavior and mechanism analysis

结构化学 2024年第2期43卷 6-8页

作者： Huipeng Zhao Xiaoqiang du School of Chemistry and Chemical Engineering North University of ChinaXueyuan Road 3Taiyuan030051People's Republic of China

Electrolytic water is considered to be the first choice for large-scale industrial hydrogen production in the future due to its good matching with wind power,photovoltaic and other renewable energy power generation systems[1].In recent years,the emerging proton exchange membrane(PEM)water electrolysis for hydrogen production(Fig.1(a))has gradually become the mainstream development direction due to its advantages such as fast start and stop,high working current density(greater than 1 ***-2),small size of electrolytic cell,and good matching with renewable electric ***,in acidic electrolytes,the ki-netics of oxygen evolution reaction(OER)half-reaction is very *** addition,the lower commercial value of anode O2 further reduces the economic benefits of traditional PEM ***,from the perspective of reducing energy consumption and improving economic benefits,finding a more dynamic and/or thermodynamic OER alternative oxidation reaction has become the key to promote the practical appli-cation of hydrogen production by electrolytic water[2].

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International Journal of Mining Science and Technology 2024年第6期34卷 881-891页

作者： Zhonghua Xue Yali Feng Haoran Li Jinrong Ju Xingquan du School of Civil and Resource Engineering University of Science and Technology BeijingBeijing 100083China Key Laboratory of Biochemical Engineering Institute of Process EngineeringChinese Academy of SciencesBeijing 100190China University of Chinese Academy of Sciences Beijing 100049China

In order to alleviate the pressure on the supply of lithium resources, this research proposes the use of binary/ternary collectors with high selectivity and collecting ability to enhance the flotation purification of low-grade zinnwaldite ore. The binary collector is a mixture of dodecylamine polyoxyethylene ether and DL-2-octanol. A binary collector is added first, followed by sodium oleate, known as a ternary collector. Under acidic conditions, the recovery of Li2O in the concentrate was increased by 8.26% with the binary collector and 13.70% with the ternary collector, compared to the dodecylamine polyoxyethylene ether. The binary collector enhanced the dispersibility of the single collector, while co-adsorption strengthened the hydrophobic nature of the zinnwaldite surface. Consequently, zinnwaldite particles,after the application of binary collector, displayed inter-particle flocculation and attachment to bubbles within 60×10^(-9)m compared to other particles. Ternary collector exhibited the capacity to lower critical micelle concentration and surface tension, subsequently inducing a denser and thicker hydrophobic layer through electrostatic forces, hydrophobic interactions, and chemical reactions. The objective of this research is to facilitate the recovery of lithium resources from low-grade ores in order to meet the needs of sustainable development.

关键词： Zinnwaldite Molecular dynamics simulation Flotation Ternary collector Extended DLVO theory

基于ESO和动态逆的欠驱动船舶航迹跟踪控制设计

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船舶工程 2020年第8期42卷 103-109页

作者：谭聪杜佳璐许桂贤李东海大连海事大学船舶电气工程学院辽宁大连116026 清华大学热学工程系北京100084

针对欠驱动船航迹跟踪控制问题,考虑船舶动态不确定性、未知时变外部扰动和速度不可测的情况,将输出重定义方法和扩张状态观测(ESO)与动态逆控制方法相结合,设计欠驱动船舶航迹跟踪控制律。采用输出重定义方法解决系统欠驱动问题;构造E... 详细信息

针对欠驱动船航迹跟踪控制问题,考虑船舶动态不确定性、未知时变外部扰动和速度不可测的情况,将输出重定义方法和扩张状态观测(ESO)与动态逆控制方法相结合,设计欠驱动船舶航迹跟踪控制律。采用输出重定义方法解决系统欠驱动问题;构造ESO,估计由船舶动态不确定性、未知时变外部扰动和船舶各自由度运动状态变量间的耦合构成的总扰动和船速;在此基础上,采用动态逆控制方法设计航迹跟踪控制律,使欠驱动船舶跟踪期望航迹,并保证航迹跟踪闭环控制系统所有信号最终一致有界。以一艘欠驱动船为例进行仿真研究,仿真结果验证了该航迹跟踪控制律的有效性和优越性。

关键词：欠驱动船舶航迹跟踪输出重定义方法扩张状态观测器动态逆控制

MCDM technique using single-valued neutrosophic trigonometric weighted aggregation operators

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Journal of Management Analytics 2024年第1期11卷 45-61页

作者： Jun Ye Shigui du Rui Yong School of Civil and Environmental Engineering Ningbo UniversityNingboPeople’s Republic of China

Motivated based on the trigonometric t-norm and t-conorm,the aims of this article are to present the trigonometric t-norm and t-conorm operational laws of SvNNs and then to propose the SvNN trigonometric weighted average and geometric aggregation operators for the modelling of a multiple criteria decision making(MCDM)technique in an inconsistent and indeterminate *** realize the aims,this paper first proposes the trigonometric t-norm and t-conorm operational laws of SvNNs,which contain the hybrid operations of the tangent and arctangent functions and the cotangent and inverse cotangent functions,and presents the SvNN trigonometric weighted average and geometric operators and their ***,an MCDM technique is proposed in view of the presented two aggregation operators in the circumstance of *** the end,an actual case of the choice issue of slope treatment schemes is provided to indicate the practicability and effectivity of the proposed MCDM technique.

关键词： Single-valued neutrosophic number trigonometric t-norm and t-conorm trigonometric weighted aggregation operator decision making