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Three-dimensional crystal plasticity and HR-EBSD analysis of the local stress-strain fields induced during twin propagation and thickening in magnesium alloys

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Journal of Magnesium and Alloys 2023年第2期11卷 657-670页

作者： Filip Siska daria drozdenko Kristian Mathis Jan Cizek Tingting Guo Matthew Barnett Institute of Physics of Materials The Czech Academy of SciencesZizkova 513/22Brno 61662Czech Republic Department of Physics of Materials Faculty of Mathematics and PhysicsCharles UniversityKe Karlovu 5Prague 12116Czech Republic Institute of Plasma Physics The Czech Academy of SciencesZa Slovankou 1782/3Prague 18200Czech Republic Institute for Frontier Materials Deakin UniversityGeelongVictoria 3216Australia

Present work focuses on analysis of the stress and strain fields inside and around the individual {10–12} twin in magnesium alloy. The 3D crystal plasticity model represents twin as an ellipsoidal inclusion surrounded by the matrix. Five different twin thicknesses and three different lateral twin lengths are used for stress/strain analysis. The simulations are complemented with experimental observations using high-resolution electron backscattered diffraction. The simulations and experiments show a similar distribution of the shear stress and the spatial activity of individual slip systems(basal, prismatic, pyramidal). Plasticity induced inside the twin is dominantly caused by the prismatic dislocations slip and does not influence twin back stress which is identical to pure elastic twin. The twin with larger lateral dimension requires lower equilibrium stress which suggests anisotropic twin propagation and increased thickness of such twins. The lateral twin propagation is mostly influenced by prismatic and pyramidal slip in the twin vicinity. The twin thickness can reach a maximal level that is driven by the critical resolved shear stress values for dislocation slip with the significant influence of basal slip.

关键词： Magnesium alloy Twinning FEM Crystal plasticity HR-EBSD

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Hot deformation of Mg-Y-Zn alloy with a low content of the LPSO phase studied by in-situ synchrotron radiation diffraction

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Journal of Magnesium and Alloys 2020年第1期8卷 199-209页

作者： Klaudia Horváth Fekete daria drozdenko Jan Capek Kristián Máthis Domonkos Tolnai Andreas Stark Gerardo Garcés Patrik Dobron Department of Physics of Materials Faculty of Mathematics and PhysicsCharles UniversityKe Karlovu 512116 PragueCzech Republic Nuclear Physics Institute of the CAS 25068ˇRežCzech Republic Magnesium Research Center Kumamoto University2-39-1 Kurokami Chuo-ku860-8555 KumamotoJapan Laboratory for Neutron Scattering and Imaging Paul Scherrer InstituteVilligen PSI5232Switzerland Institute of Materials Science Helmholtz-Zentrum GeesthachtMax-Planck Str.1GeesthachtD21502Germany Department of Physical Metallurgy CENIM-CSICAvenida Gregorio del Amo 8E-28040 MadridSpain

The compressive deformation behavior of the extruded WZ42(Mg98.5Y1Zn0.5 in at.%)magnesium alloy containing a low amount of long-period stacking ordered(LPSO)phase was studied by in-situ synchrotron radiation diffraction *** were conducted at temperatures between room temperature and 350℃.Detailed microstructure investigation was provided by scanning electron microscopy,particularly the backscattered electron imaging and electron backscatter diffraction *** results show that twinning lost its dominance and kinking of the LPSO phase became more pronounced with increasing deformation *** cracks of the LPSO phase and no debonding r at the interface between the LPSO phase and the Mg matrix were observed at temperatures above 200℃.At 350℃,the LPSO phase lost its strengthening effect and the deformation of the alloy was mainly realized by the dynamic recrystallization of the Mg matrix.

关键词： Magnesium alloy LPSO phase Kinking High temperature Synchrotron radiation diffraction

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In-situ study of the microstructure evolution during tension of a Mg-Y-Zn-Al alloy processed by rapidly solidified ribbon consolidation technique

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Journal of Magnesium and Alloys 2024年第5期12卷 2024-2040页

作者： Jeno Gubicza Kristián Máthis Péter Nagy Péter Jenei Zoltán Hegedus Andrea Farkas Jozef Vesely Shin-ichi Inoue daria drozdenko Yoshihito Kawamura Department of Materials Physics Faculty of ScienceEotvos Loránd UniversityPázmány P.sétány 1/ABudapest H-1117Hungary Department of Physics of Materials Faculty of Mathematics and PhysicsCharles UniversityKe Karlovu 512116 Praha 2Czech Republic Deutsches Elektronen-Synchrotron DESY Notkestr.85Hamburg 22603Germany Magnesium Research Center Kumamoto University2-39-1 KurokamiChuo-kuKumamoto 860-8555Japan

Mg-Y-Zn-Al alloys processed by rapidly solidified ribbon consolidation(RSRC)technique exhibit an exceptional mechanical performance indicating promising application *** material has a bimodal microstructure consisting of fine recrystallized and coarse non-recrystallized grains with solute-rich stacking faults forming cluster arranged layers(CALs)and nanoplates(CANaPs),or complete long period stacking ordered(LPSO)*** order to reveal the deformation mechanisms,in-situ synchrotron X-ray diffraction line profile analysis was employed for a detailed study of the dislocation arrangement created during tension in Mg-0.9%Zn-2.05%Y-0.15%Al(at%)*** uncovering the effect of the initial microstructure on the mechanical performance,additional samples were obtained by annealing of the as-consolidated specimen at 300 and 400℃ for 2 *** heat treatment at 300℃ had no significant effect on the initial microstructure,its evolution during tension and,thus,the overall deformation behavior under tensile *** the other hand,annealing at 400℃ resulted in a significant increase of the recrystallized grains fraction and a decrease of the dislocation density,leading to only minor degradation of the mechanical *** maximum dislocation density at the failure of the samples corresponding to the plastic strain of 10-25% was estimated to be about 16-20×10^(14)m^(-2).The diffraction profile analysis indicated that most dislocations formed during tension were of non-basal and pyramidal types,what was also in agreement with the Schmid factor values revealed independently from orientation *** was also shown that the dislocation-induced Taylor hardening was much lower below the plastic strain of 3% than above this value,which was explained by a model of the interaction between prismatic dislocations and CANaPs/LPSO plates.

关键词： Mg-Zn-Y-Al alloy Long period stacking ordered(LPSO)phase Cluster arranged nanoplates(CANaPs) Annealing Tension Dislocation density Hardening

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