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The optimum conditions for methanol conversion to dimethyl ether over modified sulfated zirconia catalysts prepared by different methods

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燃料化学学报 2021年第1期49卷 63-71页

作者： Doaa S.el-DESOUKI Amina H.IBRAHIM Samira M.ABDelAZIM Noha A.K.ABOUL-GHEIT dalia R.ABDel-HAFIZAR Processes Development Department EPRICairo 11727Egypt Refining Department EPRICairo 11727Egypt

Sulfated zirconia(SZ)and two promoted 1% Mn/SZ catalysts which have been prepared via sol gel(Mn/SZ-S)and impregnation(Mn/SZ-I)methods were *** morphology of the catalysts was characterized by XRD,BET,NH3-TPD,ICP,SEM and FT-IR *** conversion of methanol to dimethyl ether and hydrocarbons was carried out in the temperature range of 120−300℃.The Mn/SZ-S showed the highest activity due to the high surface area with suitable *** optimum condition of Mn/SZ-S catalyst was investigated at 200℃ and LHSV of 0.02 h^−1 in a time range from 30 to 210 *** was found that the total conversion decreased from 80.18% to 53.26% at 210 *** reusability of this catalyst was studied at the optimum condition up till four cycles for 1 *** characterization of the reused catalyst showed a significant change in the structure and surface acidity due to the blockage of the surface acid sited by carbonaceous materials.

关键词： catalysts dehydration DME sulfate content sulfated zirconia

Effect of Treated Waste Water Irrigation on Plant Growth and Soil Properties in Gaza Strip, Palestine

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American Journal of Plant Sciences 2013年第9期4卷 1736-1743页

作者： Yasser el-nahhal Khalil Tubail Mohamad Safi Jamal Safi Environmental Protection and Research Institute Gaza Palestine

This study investigated the effect of treated wastewater (TWW) irrigation on growth of Chinese cabbage and corn and on soil properties in Gaza Strip, Palestine. Chinese cabbage and corn were planted in winter and summer seasons respectively in a sandy soil. The experimental design was a randomized complete block using 2 treatments with 4 replicates. Soil samples were collected from 0.0-120 cm depths from all plots and analyzed for pH, electric conductivity (EC) and nutrient contents. The plants were irrigated with either TWW or fresh water (FW) fortified with NPK, while control used drip irrigation system. The biomass (total fresh weight of the plants) was used as an indicator of the plant yields. Concentration of heavy metals on plant leaves was determined by Inductive Coupled Plasma Analyzer (ICP) and was taken as an indicator of plant quality. Biomass of Chinese cabbage and corn grown in plots irrigated with TWW was higher than those grown in plots irrigated with FW. These results indicate the ability of TWW supplying the necessary nutrients for plant growth. Heavy metal content in plant leaves in all treatments (TWW and FW) was nearly similar and below EPA standards, indicating high quality of plants. Soil analysis showed great changes in soil properties due to irrigation with TWW. The interesting outcome of this study is that TWW is an effective source for plant nutrients. It is encouraging to reuse TWW in agricultural system after full treatment.

关键词： TWW FW Corn Chinese Cabbage Heavy Metals

Selectivity of Acrylic Acid Radiation Grafted Non-Woven Polypropylene Sheets towards Some Heavy Metals Ions

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Open Journal of Polymer Chemistry 2012年第1期2卷 6-13页

作者： dalia el-Sayed Hegazy National Centre for Radiation Research and Technology Cairo Egypt

Graft polymerization has been considered as a general method for the modification of the physical and chemical properties of polymeric materials and of particular interest for synthesis of the hydrophilic membrane. In this study, hydrophilic carboxylic acid groups were introduced by radiation-induced grafting of acrylic acid (AAc) onto non-woven polypropylene fabric (NWPP). Different irradiation doses and (AAc) monomer concentrations were used to optimize grafting yield. Characterization and properties of the prepared graft copolymer were studied by employing X-ray Dif-fraction (XRD), Thermogravimetric Analysis (TGA), Scanning electron Microscope (SEM ), Fourier Transform Infrared Spectrometry (FTIR) and differential scanning calorimeter (DSC). The prepared grafted materials were used for removing some heavy metals ions. The results showed that the non-woven PP grafted with (AAc) has good affinity toward Cu, Ni and Co.

关键词： Radiation Grafting Acrylic Acid Characterization Removal of Heavy Metals

Influence of Biogas Production on Bioremediation of Animal Manures

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American Journal of Analytical Chemistry 2019年第1期10卷 1-8页

作者： Essam Ibrahim Hammad Mohamad R. Al-Agha Yasser el-nahhal Department of Environmental and Earth Sciences Faculty of Science The Islamic University Gaza Palestine

This study investigated the effect of biogas production on the removal hazardous waste properties. Biogas was produced from caw, chicken and mixed manure. Samples were taken before and after biogas production and tested for removal of total solid (TS), removal of chemical oxygen demand (COD), biological oxygen demand (BOD), and fecal coliform bacteria (FC). Results showed tremendous removal of the above mentioned parameters after biogas production. Chemical analysis of digestate indicates the advantages of using them as plant nutrients. Application of digestate in soil dramatically changed the chemical and physical properties of soil. It can be concluded that biogas production, is not only producing biogas but also removing waste parameters (TS, COD, BOD, FC) and producing plant nutrients.

关键词： Biogas Production Removal of COD BOD and/or TS

Enhancing Biogas Production: Influence of Mixing Cow and Chicken Manures

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Energy and Power Engineering 2018年第8期10卷 383-397页

作者： Essam Ibrahim Hammad Mohammad R. Al-Agha Yasser el-nahhal Department of Earth and Environment Faculty of Science The Islamic University of Gaza Gaza Palestine

The objectives of this study were to enhance the production of biogas through using a mixture of cow and chicken manure and to investigate the effect of digested manure on plant growth. Biogas digester consisted of a plastic polyethylene tank with a volume of 0.25 cubic meters. Cow and chicken manures were collected from certified animal and chicken farms. Mixture of manure was prepared by mixing 5 kg of chicken manure and 5 kg of cow manure together in 100 L plastic tank containing 90 L water free from chlorine. Percentage of manure in all cases was 10% (w/v). The manures were transferred to the digesters and kept in greenhouse to insure warm conditions (30°C - 39°C). Produced biogas was measured each two days and digestate samples were taken every two days for pH, EC, BOD, COD determination. Results showed increased biogas production and reached the highest quantity after 28 days and the amount of biogas produced from the mixture of cow and chicken manures was higher than the amount produced from each manure individually. Decreases in pH values were observed during biogas production followed by BOD, COD reduction. On the other hand, increases on EC values were observed. Application of digested manure in agriculture increased yield of lettuce by 75% comparing with the control sample. The study recommended using cow manure mixed with chicken manure to increase the production of biogas and to use the digested manure in agricultural.

关键词： Biogas Cow Manure Chicken Manure Digested Manure

Nemacur Residue Analysis in Soil Water and Cucumber Samples Collected from the Field in Gaza Strip, Palestine

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American Journal of Plant Sciences 2018年第3期9卷 517-530页

作者： Mohammed Ouda Alloh Said AL-Kurdi M. R. Alagha el-nahhal Yasser Department of Environment and Earth Sciences Faculty of Science The Islamic University Gaza Palestine

Application of Nemacur in Gaza strip increased rapidly as a potential alternative to the widely used soil sterilizing agent methyl bromide. Nemacur application may contaminate soil, water and plant systems due to its high solubility in water. The objective of this study was to determine Nemacur residues soil, water, and cucumber samples collected from a field plots applied Nemacur at different field rates (0.0, 0.5 F, 1 F, 2 F) where F is the recommended field rate of Nemacur (4 kg/Hectare). Nemacur residues were determined by chemo-assay and bioassay techniques. Results revealed that considerable Nemacur concentrations were found in cucumber fruits and plant leaves. Nemacur residues were higher in water samples collected from sandy soil (7.2 μg/L) than from clay soil (3.4 μg/L). Furthermore, Nemacur residues in sandy soil (0.23 μg/kg) were lower than those in clay soil (1.3 μg/kg). In addition, Nemacur concentration in top soil layer in clay soil was lower than other layers. Nemacur residues in cucumber fruits grown in sandy soil were lower than those in cucumber fruits grown in clay soil. Nemacur residues in cucumber fruits collected from the market were below detection limit of HPLC technique. Chemo-assay techniques determined lower concentration of Nemacur than bioassay techniques. It can be concludes that considerable concentrations of Nemacur were found in all tested samples. Comparing with maximum residues limits (MRLS). Nemacur concentrations in various environmental samples were less than the maximum residues limits.

关键词： Nemacur Fenamiphos Chemo-Assay Bioassay Soil

Impact of biomass in Egypt on climate change

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Natural Science 2013年第6期5卷 678-684页

作者： dalia Adel Nakhla Mohamed Galal Hassan Salah el Haggar Department of Mechanical Engineering School of Sciences and Engineering The American University in Cairo Cairo Egypt Department of Petroleum Engineering School of Sciences and Engineering The American University in Cairo Cairo Egypt Environmental Engineering PhD Program School of Sciences and Engineering The American University in Cairo Cairo Egypt

Egypt is one of the most vulnerable countries to climate change due to the expected detrimental impacts on coastal zones, agriculture, water security as well as indirect social and health impacts. Egypt is responsible for 0.57% of the global greenhouse gas (GHG) emissions. Although Egypt is a non-annex I country not requiring any specific emission reduction or limitation targets under the Kyoto protocol, its National plans have included mitigation measures to reduce its greenhouse gases. The main sectors contributing to climate change in Egypt are energy, industry, agriculture and waste. Waste, on the other hand, has been accumulating in the streets of Egypt and along its water banks causing considerable air, soil and water pollution and indirect detrimental health impacts. However, this waste which is composed of organic municipal waste, agricultural residues, agro-industrial waste, animal manure and sewage sludge are valuable biomass resources. Utilizing the waste resources of Egypt especially the biomass or the organic component of this waste will not only solve some of the pressing economic needs of Egypt such as animal fodder, fertilizer and fuel but will also alleviate environmental burdens through decreasing air pollution and greenhouse gas emissions in the sector of waste as well as those of energy, industry and agriculture. This paper quantifies the biomass resources in Egypt generated from different waste resources. Then it demonstrates the efforts that Egypt made to contribute to global greenhouse gas emissions reductions through the Kyoto Protocol’s clean development mechanism (CDM). The projects in the waste sector already established in Egypt and approved as CDM projects are listed, which are related to waste management facilities and those which are waste to energy projects. Finally, a list of mitigation projects as proposed by the Egyptian government to decrease GHGs as related to the waste sector are enumerated.

关键词： Waste Climate Change Biomass Egypt

Development of Analytical Method for the Detection of Nemacur Residues in Cucumber Fruits

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American Journal of Analytical Chemistry 2018年第1期9卷 64-76页

作者： Said Al-Kurdi Mohammed O. Alloh Mohammed R. Al-Agha Yasser el-nahhal Department of Earth and Environmental Sciences Faculty of Science The Islamic University Gaza Palestine

Application of Nemacur (Fenamiphos) for pest control may contaminate soil, water and plant with harmful residues and pose threats to human life. This study developed an easy method for the determination of Nemacur residues in cucumber fruits collected from the central markets and from the farm. The method is based on extracting the active ingredients of Nemacur from the commercial formulation and used as a standard material to calibrate the HPLC to determine Nemacur residues in cucumber fruits collected from the central market. Results showed that more than 70% of the active ingredient was extracted from the commercial formulations. Standardization of HPLC with extracted materials showed strong positive association between concentration and peak area relationship. Bioassay investigation showed high mortality of tested organism (fish). Statistical analysis of mortality % between the commercial formulation and those of the extracted ingredient showed no significant differences. These results demonstrated the effectiveness of extracted Nemacur to calibrate HPLC and in bioassay test. Nemacur residues in Cucumber fruits collected from the market were below the detection limit of HPLC, recovery % of Nemacur from control group of cucumber was above 80%. It can be concluded that the method is easily developed and validated by bioassay and chemo-assay.

关键词： Nemacur Fenamiphos Analytical Method HPLC

Bougainvillea spectabilis flowers extract protects against the rotenone-induced toxicity

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Asian Pacific Journal of Tropical Medicine 2017年第5期10卷 457-466页

作者： Omar M.E.Abdel-Salam Eman R.Youness Nadia A.Ahmed Sayed A.el-Toumy Ahmed M.A.Souleman Nermeen Shaffie dalia M.Abouelfadl Department of Toxicology and Narcotics National Research CentreCairoEgypt Department of Medical Biochemistry National Research CentreCairoEgypt Department of Chemistry of Tannins National Research CentreCairoEgypt Department of Phytochemistry and Plant Systematic National Research CentreCairoEgypt Department of Pathology National Research CentreCairoEgypt

Objective:To investigate the effect of two extracts of Bougainvillea spectabilis(B. spectabilis) flowers with yellow and pink/purple on brain oxidative stress and neuronal damage caused in rats by systemic rotenone injection. Methods:Rotenone 1.5 mg/kg was given three times per week alone or in combination with B. spectabilis flowers extracts(25 mg or 50 mg) via the subcutaneous route for 2 weeks. Brain concentrations of the lipid peroxidation marker malondialdehyde(MDA),reduced glutathione,nitric oxide(nitrite),the pro-inflammatory cytokine interleukin-1beta(Il-1β) as well as butyrylcholinesterase,and paraoxonase-1(PON-1) activities,were determined. Histopathology and caspase-3 immunohistochemistry were also performed. Results:Rotenone resulted in significant increases of brain MDA(the product of lipid peroxidation),and nitric oxide content along with decreased brain reduced glutathione. There were also marked and significant inhibition of brain PON-1 and BCh E activities and increased Il-1β in brain of rotenone-treated rats. B. spectabilis flowers extract itself resulted in brain oxidative stress increasing both lipid peroxidation and nitrite content whilst inhibiting PON-1 activity. The yellow flowers extract inhibited BCh E activity and increased brain Il-1β. When given to rotenone-treated rats,B. spectabilis extracts,however,decreased lipid peroxidation while their low administered doses increased brain GSH. Brain nitrite decreased by the pink extract but showed further increase by the yellow extract. Either extract,however,caused further inhibition of PON-1 activity while the yellow extract resulted in further inhibition of BChE activity. Histopathological studies indicated that both extracts protected against brain,liver and kidney damage caused by the toxicant. Conclusions:These data indicate that B. spectabilis flowers extracts exert protective effect against the toxic effects of rotenone on brain,liver and kidney. B. spectabilis flowers extracts decreased

关键词： Bougainvillea spectabilis Flowers Extract Rotenone Oxidative stress Parkinson’s disease