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Process optimization of reaction of acid leaching residue of asbestos tailing and sodium hydroxide aqueous solution

science china(Technological sciences) 2009年第1期52卷 204-209页

作者： du gaoxiang1,3. zheng shuilin2 & ding hao1 1 school of materials science and technology, china university of geosciences ({3.), beijing, 100083. china 2 school of Chemical and Environment Engineering, china university of Mining and technology ({3.), beijing 100083. china 3.Hebei Qinghe Refractory Group Co. Ltd., Xingtai 054804, china 1. school of materials science and {3. China University of Geosciences (Beijing) Beijing 100083 China 3. Hebei Qinghe Refractory Group Co. Ltd. Xingtai 054804 China 2. school of Chemical and Environment Engineering China University of Mining and Technology (Beijing) Beijing 100083 China

Silica is the major component of the acid leaching residue of asbestos tailing. The waterglass solution can be prepared by the reaction of the residue with sodium hydroxide aqueous solution. Compared to the high temperature reaction method, this process is environmental friendly and low cost. In this paper, the reaction process of the residue and the sodium hydroxide aqueous solution is optimized. The optimum reaction process parameters are as follows: the usage of sodium hydroxide is 26.4 g/100 g acid leaching residue, the reaction temperature is 90℃, the reaction time is 1 h, and the ratio of the liquid/solid is 2.0. The significance sequence of the process parameters to the alkali leaching reaction effect is the usage of sodium hydroxide > the ratio of the liquid/solid > the reaction time > the reaction temperature. The significance sequence to the leaching ratio of SiO2 is the ratio of the liquid/solid > the usage of sodium hydroxide > the reaction time > the reaction temperature. The significance sequence to the modulus of the sodium silicate is the ratio of the liquid/solid > the usage of sodium hydroxide > the reaction time > the reaction temperature. Under the optimum conditions, the leaching ratio of the SiO2 is 77.5%, and the modulus of the sodium silicate is 3.15. The XRD analysis result indicates that the major components of the alkali leaching residue are serpentine, talc, quartz and some albite.

关键词： asbestos tailing acid leaching residue sodium hydroxide process optimization

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Three-point bending fracture characteristics of bulk metallic glasses

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science china(Physics,Mechanics & Astronomy) 2010年第4期53卷 654-657页

作者： FAN ZhenJun, zheng ZhiYuan & JIAO ZengBao school of materials {3.s and technology, china university of geosciences, beijing 100083. china 1. school of materials sciences and {3. China University of Geosciences Beijing 100083 China

This paper presents the SEM micrographs for the three-point bending fracture surfaces of Zr-based, Ce-based and Mg-based bulk metallic glasses (BMGs), which show the dimple structures in the three kinds of BMGs. The shapes of the giant plastic deformation domain on the fracture surface are similar but the sizes are different. The fracture toughness KC and the dimple structure size of the Zr-based BMG are both the largest, and those of the Mg-based BMG are the smallest. The fracture toughness KC and the dimple structure size of the Ce-based BMG are between those of the Zr-based and the Mg-based BMG. Through analyzing the data of different fracture toughnesses of the BMGs, we find that the plastic zone width follows w = (KC/σY)2/(6π).

关键词： metallic glass fracture surface tree-point bending

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Compressive fracture characteristics of Zr-based bulk metallic glass

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science china(Physics,Mechanics & Astronomy) 2010年第5期53卷 823-827页

作者： FAN ZhenJun,zheng ZhiYuan & JIAO ZengBao school of materials {3.s and technology,china university of geosciences,beijing 100083.china 1. school of materials sciences and {3. China University of Geosciences Beijing 100083 China

The compressive fracture characteristics of Zr-based bulk metallic glass under uniaxial compression tests are *** zigzag rheological behavior is observed in the compression stress-strain curves of amorphous *** room temperature the uniaxial compression fracture takes place along the plane which is at a 45-degree angle to the direction of the compressive *** microstructure of a typical fracture pattern is the vein network.A unique,finger-like vein pattern is found to exist at the fracture surface of Zr-based bulk metallic glass.

关键词： bulk metallic glass fracture surface compressive fracture

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CXCL13.shapes tumor immune microenvironment in ovarian cancer with homologous recombination deficiency

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Genes & Diseases 2024年第5期11卷 48-50页

作者： Yue ding zheng Ye Bo ding Songwei Feng Furong {3. Xuejiao Ma Xiaoxuan Wang Yang Shen Department of Obstetrics and Gynaecology Zhongda HospitalSchool of MedicineSoutheast UniversityNanjingJiangsu 210008China State Key Laboratory of Bioelectronics School of Biological Science and Medical EngineeringSoutheast UniversityNanjingJiangsu 210096China State Key Laboratory of Translational Medicine and Innovative Drug Development Jiangsu Simcere Diagnostics Co.Ltd.NanjingJiangsu 210042China

Recently,immune checkpoint inhibitors(ICIs)and poly(ADP-ribose)polymerase inhibitors(PARPi)have played a pivotal role in prolonging the recurrence-free survival of patients with ovarian cancer(OC).1,2 Although PARPi have revolutionized the treatment of OC,the absence of reliable predictive biomarkers limits the broad application of ICIs for patients with homologous recombination(HR)deficiency(HRD).3.CXC-chemokine ligand 13.CXCL13.is a cytokine constitutively secreted in the stromal cells of the B-cell region of secondary lymphoid tissue.4 It exclusively binds to the chemokine receptor CXCR5,which is abundantly expressed in subsets of mature circulating B lymphocytes,follicular helper T cells,and skin-derived dendritic cells,and governs the migration of these cells into secondary lymphoid organs in response to the CXCL13.gradient.5 In this study,we aimed to elucidate the role of CXCL13.in shaping the tumor immune microenvironment(TIME)in HR-deficient OC and to explore its relationship with the cGAS-STING signaling pathway.

关键词： CXCL13 cancer organs

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The Self-assembling and Application of Inorganic Anti-bacterial Material Made of Natural Nanoporous Carrier

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Journal of Wuhan university of technology(materials {3.) 2008年第6期23卷 771-774页

作者：孙春宝 school of Civil and Environmental Engineering University of Science and Technology Beijing

The inorganic antimicrobial material was inhibited to the microbes with the added metal ion,*** primary wet product carrying 5%-10% zinc ion was generated under the following conditions：temperature was 95 ℃,solution zinc concentration was 1.2-2.0 mol/L,and the ratio of Zn solution to zeolite weight was 5：*** final stable product was manufactured after baking in an oven for 1-3.h at the temperature of 500-900 ℃.The baked material was tested for its disinfection effectiveness and coloring effect when mixed with paint *** on the final batch of tests,the zinc content of this anti-microbial product was further optimized.

关键词： inorganic antimicrobial nanoporous material antibacterial coating zeolite self-assembling

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Force Parameter Model of 3.Roll Mills for Continuous Cold Rolling Wires

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International Journal of Minerals,Metallurgy and materials 1999年第4期13卷 292-295页

作者： Baolong zheng1 Li Sun2 Ruichen An2 Jin Wang1 Weichang Zhu1(l Material science and Engineering school, {3. of science and technology beijing, beijing 100083. china2 Tangshan iron and Steel Co. Ltd., Tangshan 063.00, china) Material science and Engineering school University of Science and Technology Beijing Beijing 100083 China Tangshan Iron and Steel Co. Ltd. Tangshan 063000 China

Based on experimental data, the mathematical model of rolling force parameters of 3.roll mills was studied. The structure ofthe model was theoretically set up and the coefficients were determined by static analysis of the data. The torque in continuous rollingwas measured, and the characteristics and efficiency of 3.roll mills are investigated.

关键词： 3.roll mill force mathematical model cold rolling wire

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Synthesis of vertically aligned carbon nanotube arrays on silicon substrates

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science china(Technological sciences) 2004年第5期47卷 616-624页

作者： zheng Ruiting1, CHENG Guoan1, PENG Yibin1, 2, Zhao Yong1, 3. LIU Huaping1 & LIANG Changlin1 1. Key Laboratory of Radiation Beam technology and {3. Modification of Ministry of Education, Department of {3. science and Engineering, beijing Normal university, beijing 100875, china 2. school of science, Civil Aviation university of china, Tianjin 3.03.0, china 3. Department of Physics, Nanchang university, Nanchang 3.0047, china Correspondence should be addressed to zheng Ruiting 1. Key Laboratory of Radiation Beam technology and materials Modification of Ministry of Education Department of Materials Science and Engineering Beijing Normal University 100875 Beijing China 2. school of science Civil Aviation University of China 300300 Tianjin China 3. Department of Physics Nanchang University 330047 Nanchang China

The growth of well-aligned carbon nanotube (CNT) arrays using a heat chemical vapor deposition system on silicon substrates is reported. The growth properties of CNT arrays are studied as a function of synthesis conditions. It is found that 750°C and 10 nm Fe film are suitable conditions for the growth of well-aligned CNT arrays. CNT arrays with a uniform diameter, thick tube wall and firm cohesion to the Si substrate can be grown for C2H2 concentration of 27%. Based on the experiment, the processes of improving the alignment of CNT arrays and cohesion between CNT arrays and Si substrates are discussed.

关键词： carbon nanotubes, vertically aligned, silicon substrate, chemical vapor deposition.

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Secondary Hardening, Austenite Grain Coarsening and Surface Decarburization Phenomenon in Nb-Bearing Spring Steel

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Journal of Iron and Steel Research International 2012年第3期19卷 47-51,61页

作者： ZHANG Chao-lei, LIU Ya-zheng, ZHOU Le-yu, JIANG Chao ({3. of materials science and Engineering, university of science and technology beijing, beijing 100083. china) school of materials science and Engineering University of Science and Technology Beijing Beijing 100083 China

The secondary hardening, the austenite grain coarsening and the surface decarburization phenomenon of Nb-bearing spring steel were investigated, and the effects of niobium on tempered microstructure was studied using scanning electron microscope. The results show that the micro-addition of niobium increases the tempering resistance and produces secondary hardening. The effect of niobium on the size and distribution of cementite particles is one of the primary reasons to increase the hardness after tempering. The grain-coarsening temperature of the spring steel is raised 150 ~C due to Nb-addition. Furthermore, both the secondary hardening and the austenite grain coarsening phenomenon congruously demonstrate niobium begins observably dissolving above 1 100 ℃ in the spring steel. Be- sides, niobium microalloying is an effective and economy means to decrease the decarburization sensitivity of the spring steels.

关键词： spring steel! microalloyingl secondary hardening grain coarsening surface decarburization

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Generation and controlling of the dispersive wave by femtosecond pulses propagating in the normal dispersion regimes of the birefringent photonic crystal fiber

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science china(Physics,Mechanics & Astronomy) 2010年第4期53卷 643-648页

作者： LI ShuGuang1,2, zheng Yi1, YIN GuoBing2, ZHANG Lei2, ZHOU GuiYao2 & HOU LanTian2 1 school of science,{3. Jiaotong university,{3. 100044, china 2 Key Laboratory of Metastable materials science and technology, College of science, Yanshan university, Qinhuangdao 066004, china 1. school of science Beijing Jiaotong University Beijing 100044 China2. Key Laboratory of Metastable Materials Science and Technology College of Science Yanshan University Qinhuangdao 066004 China

This paper studies the generation of the dispersive wave (DW) in the normal dispersion regimes of the birefringent photonic crystal fiber (BPCF) fabricated in this work. The remarkable blue-shifted radiation is found to be generated when 3. fs pulses are input in the normal dispersion regime of the BPCF for the first time. The characteristics of the blue-shifted DW strongly depend on the polarization of the input pulse. As a result, two peaks appear in the blue-shifted region of the spectrum when the input pulses polarize along the slow axis of the BPCF. With the increase of the center wavelength of the initial input pulse, the difference between the wavelengths of the two peaks widens. The peak location in the spectrum can be explained by the phase matching condition between the DW and the input pulse. In addition, when the input polarization is set to an angle of 45° with respect to the principal axes of the BPCF, the cross-phase modulation and coherent coupling between two orthogonally polarized modes would result in pulse trapping in the BPCF. Accordingly, the DW shift toward short wavelength is restrained. The DW generation in the normal-dispersion regimes of BPCF can be controlled by the phase matching condition and polarization of the input pulse.

关键词： birefringent photonic crystal fiber normal dispersion dispersive wave pulse trapping

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Development on Technique of Tube Reducing in Double 3.Roll Dies

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International Journal of Minerals,Metallurgy and materials 2000年第1期14卷 55-57页

作者： Baolong zheng Li Sun Ruichen An , Lianshi Li Material science and Engineering school, {3. of science and technology beijing, beijing 100083. china No. 1 Steel Rolling Factory, Tangshan Iron and Steel Corporation, Tangshan 063.00, china Material science and Engineering school University of Science and Technology Beijing Beijing 100083 China No.1 Steel Rolling Factory Tangshan Iron and Steel Corporation Tangshan 063000 China

Based on the experiments, a new technique of reducing tube with two linked 3.roll roller dies was developed. The external friction conditions, velocity and the non-uniform deformation of metal were distinctly improved, and the friction between metal and tool was decreased. Corrosion strip layers and photo-elastic coatings methods were adopted in the experiment for measuring residual stress, and the residual stresses in the drawn tube with 3.roll dies are reduced.

关键词： reducing tube roller dies drawing deformation

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