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Highly defective dark TiO_(2) Modified with Pt: Effects of Precursor nature and Preparation Method on Photocatalytic Properties

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Transactions of Tianjin University 2024年第2期30卷 198-209页

作者： E.d.Fakhrutdinova O.A.Reutova T.A.Bugrova I.Yu.Ovsyuk l.S.Kibis O.A.Stonkus d.B.vasilchenko O.v.vodyankina v.A.Svetlychnyi national Research Tomsk State University TomskRussia 634050 novosibirsk State University NovosibirskRussia 630090 Boreskov Institute of Catalysis NovosibirskRussia 630090 nikolaev Institute of Inorganic Chemistry NovosibirskRussia 630090

The study focused on the modification with platinum of dark defective titania obtained via pulsed laser ablation. Both the method of Pt introduction and the nature of the Pt precursor were varied. All samples exhibited similar phase compositions, specific surface areas, and Pt contents. High-resolution transmission electron microscopy coupled with pulsed CO adsorption revealed increased dispersity when photoreduction and the hydroxonitrate complex (Me _(4) n) _(2) [Pt _(2) (OH) _(2) (nO _(3) ) _(8) ] were used. The sample featured a high content of single-atom species and subnano-sized Pt clusters. The X-ray photoelectron spectroscopy results showed that the photoreduction method facilitated the appearance of a larger number of Pt ^(2+) states, which appeared owing to the strong metal-support interaction (SMSI) eff ect of the transfer of electron density from the electron-saturated defects on the TiO _(2) surface to Pt ^(4+) . In the hydrogen evolution reaction, samples with a significant fraction of the Pt ^(2+) ionic component, capable of generating short-lived Pt^(0) single-atom sites under irradiation due to the SMSI eff ect, exhibited the highest photocatalytic activity. The 0.5Pt(C)/TiO_(2) -Ph sample exhibited the highest hydrogen yield with a quantum efficiency of 0.53, retaining its activity even after 8 h of operation.

关键词： dark(black)TiO_(2) Pulsed laser ablation Platinum reduction method Precursor type Photocatalysis Hydrogen evolution reaction

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Stability Analysis of dC Microgrid Clusters Based on Step-by-step System Matrix Building Algorithm

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Journal of Modern Power Systems and Clean Energy 2024年第3期12卷 900-912页

作者： K.Jithin n.Mayadevi R.Hari Kumar v.P.Mini the department of Electrical Engineering College of Engineering TrivandrumAPJ Abdul Kalam Technological University(APJAKTU)ThiruvananthapuramIndia

dC microgrids(dCMGs)are made up of a network of sources and loads that are connected by a number of power electronic converters(PECs).The increase in the number of these PECs instigates major concerns in system *** interconnecting the microgrids to form a cluster,the system stability must be *** paper proposes a novel stepby-step system matrix building(SMB)algorithm to update the system matrix of an existing dCMG cluster when a new microgrid is added to the cluster through a distribution *** stability of the individual dCMGs and the dCMG cluster is analyzed using the eigenvalue ***,the particle swarm optimization(PSO)algorithm is used to retune the controller gains if the newly formed cluster is not *** simulation of the dCMG cluster is carried out in MATlAB/Simulink environment to test the proposed *** results are also validated using the OP4510 real-time simulator(RTS).

关键词： Converter dC microgrid cluster eigenvalue interconnection particle swarm optimization system stability system matrix

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Greatly enhanced corrosion/wear resistances of epoxy coating for Mg alloy through a synergistic effect between functionalized graphene and insulated blocking layer

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Journal of Magnesium and Alloys 2024年第1期12卷 332-344页

作者： Z.Y.Xue X.J.li J.H.Chu M.M.li d.n.Zou l.B.Tong School of Metallurgical Engineering Xi’an University of Architecture and TechnologyXi’an 710055China State Key laboratory of Advanced design and Manufacturing for vehicle Body Hunan UniversityChangsha 410082China

The poor corrosion and wear resistances of Mg alloys seriously limit their potential applications in various *** conventional epoxy coating easily forms many intrinsic defects during the solidification process,which cannot provide sufficient *** the current study,we design a double-layer epoxy composite coating on Mg alloy with enhanced anti-corrosion/wear properties,via the spin-assisted assembly *** outer layer is functionalized graphene(FG)in waterborne epoxy resin(WEP)and the inner layer is Ce-based conversion(Ce)*** FG sheets can be homogeneously dispersed within the epoxy matrix to fill the intrinsic defects and improve the barrier *** Ce film connects the outer layer with the substrate,showing the transition *** corrosion rate of Ce/WEP/FG composite coating is 2131 times lower than that of bare Mg alloy,and the wear rate is decreased by~90%.The improved corrosion resistance is attributed to the labyrinth effect(hindering the penetration of corrosive medium)and the obstruction of galvanic coupling *** synergistic effect derived from the FG sheet and blocking layer exhibits great potential in realizing the improvement of multi-functional integration,which will open up a new avenue for the development of novel composite protection coatings of Mg alloys.

关键词： Mg alloy Functionalized graphene Epoxy coating Corrosion/wear resistance Blocking layer

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Simultaneous removal of critical rare earth elements and chalcogen oxyanions by anaerobic granular sludge

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Rare Metals 2024年第9期43卷 4595-4611页

作者： Chiara Belloni Mohanakrishnan logan Stefano Papirio Piet n.l.lens University of Galway Galway H91 TK33Ireland department of Civil Architectural and Environmental EngineeringUniversity of Naples Federico II80125 NaplesItaly

Conventional mining of economically and strategically important critical rare earth elements(REEs)(such as neodymium,lanthanum and dysprosium),and chalcogens(such as selenium and tellurium)are associated with a huge economic and environmental ***,the need to recover REEs as well as chalcogens from different waste streams including wastewaters is becoming *** assays on synthetic chalcogen/REE-laden wastewater showed that the presence of REEs significantly improved the tellurite removal rate(>80%)and enhanced selenate removal by 66%±10%.Three 3.9 l continuous upflow anaerobic granular sludge bed(UASB)reactors were operated at a hydraulic retention time of 24 h and30℃.Selenate reduction was achieved with a removal efficiency of~98%with an influent p H of 4.0 for more than 28 *** effect of REEs on tellurite removal in the UASB bioreactor could not be clearly established since a soluble tellurium removal efficiency of more than 98%was observed already before the addition of REEs at elevated tellurite *** complete REE removal in both batch assays and UASB reactors at higher pH(7.0±0.5)was attributed to precipitation,whereas chalcogen oxyanions removal was due to microbial ***,at acidic p H,biosorption was responsible for REE's removal,and the Se-enriched sludge exhibited a superior REE's removal efficiency than the non-enriched and Te-enriched sludge.

关键词： Rare earth elements Selenium Tellurium Bioreduction Adsorption

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First results of turbulence investigation on Globus-M2 using radial correlation doppler reflectometry

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Plasma Science and Technology 2024年第10期26卷 49-55页

作者： A.POnOMAREnKO A.YASHIn v.GUSEv E.KISElEv G.KURSKIEv v.MInAEv Y.PETROv n.SAKHAROv P.SHCHEGOlEv E.TKACHEnKO n.ZHIlTSOv Peter the Great St.Petersburg Polytechnic University St.Petersburg 195251Russia Ioffe Institute St.Petersburg 194064Russia

The first results of investigation of the turbulence structure using doppler backscattering(dBS)on the Globus-M2 tokamak are presented.A one-channel dBS system with a variable probing frequency within the 18–26 GHz range was installed to investigate the edge plasma at normalized minor radiiρ=0.9–*** correlation doppler reflectometry was used to study the changes in turbulence eddies after the lH *** analysis was applied to the phase derivative of complex in-phase and quadrature(IQ)signals of the dBS diagnostic as it contains information about the poloidal plasma rotation *** l-mode,the radial correlation length l_(r)is estimated to be 3 cm and after transition to H-mode reduces to approximately 2 *** modelling in a linear local approximation using code GEnE indicates that the instability with positive growth rate at the normalized minor radiusρ=0.75 in l-mode and H-mode on Globus-M2 was the ion temperature gradient(ITG)mode.

关键词： tokamak turbulence doppler backscattering correlation reflectometry

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Sustainability assessment of solar drying systems:a comparative life-cycle analysis of phase-change material-based *** solar dryers

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Clean Energy 2024年第4期8卷 183-196页

作者： nakum divyangkumar Kirtika Sharma n.l.Panwar Gande Saichandhu department of Renewable Energy Engineering Maharana Pratap University of Agriculture and TechnologyUdaipur(Rajasthan)313001India Environmental Management Jawaharlal Nehru University TechnologyHyderabadIndia

Solar drying systems are becoming a popular alternative to traditional energy-based drying systems for agricultural products due to their effectiveness and reduced fuel *** the efficiency of solar drying systems has been thoroughly investigated,their sustainability has not been studied *** study aims to fill that gap by conducting a life-cycle assessment of two new solar drying systems built in Udaipur,Rajasthan,*** environmental implications of an innovative cylindrical solar-assisted drying system and a phase-change material-based solar drying system were evaluated using cradle-to-gate life-cycle *** study uses the ReCiPe 2016 endpoints(H)technique to calculate various aspects such as midpoint,endpoint,single score,normalization result,and network diagram for phase-change material-based solar drying and cylindrical solar-assisted *** show that phase-change material-based solar drying has an average of 40%more impact on the environment than cylindrical solar-assisted drying,with a high impact found in human non-carcinogenic toxicity,mainly due to the production of phase-change ma***,cylindrical solar-assisted drying system crossover phase-change material based solar drying in terms of its impact on human carcinogenic toxicity and fossil resource *** contribution to global warming of phase-change material-based solar drying is 13.7%more than that of cylindrical solar-assisted *** endpoint characterization indicates that phase-change material-based solar drying exceeds in terms of human health(40%)and ecosystem(37.04%),whereas cylindrical solar-assisted drying surpasses phase-change material-based solar drying in terms of impacts on resources,at 14%.The early drying in phase-change material-based solar drying makes up for its higher impact than that in cylindrical solar-assisted drying,which takes 3 hours longer to *** study offers guidance and methods for making the best choice of

关键词： solar drying cylindrical hybrid solar dryer PCM-based solar dryer life-cycle assessment ReCiPe method impact assessment

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等离子体技术制备具有亚微米颗粒结构的球化W-Cu伪合金微粉

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Transactions of nonferrous Metals Society of China 2024年第2期34卷 592-603页

作者： A.v.SAMOKHIn n.v.AlEKSEEv A.A.dOROFEEv A.A.FAdEEv M.A.SInAYSKIY I.d.ZAvERTIAEv Y.v.GRIGORIEv Institute of Metallurgy and Materials Science Russian Academy of SciencesMoscow 119334Leninsky prospect 49Russian Federal Scientific Research Center“Crystallography and Photonics” Russian Academy of SciencesMoscow 119334Leninsky prospect 59Russian

采用复杂多级方法研究并证实制备具有亚微米/纳米级内部结构的球形W-Cu复合微粉的可能性。首先,采用等离子体化学合成法制备具有核壳结构的W-Cu纳米粉末(W核及Cu壳)。然后,将W-Cu纳米粉末与蔗糖的水悬浮液进行喷雾干燥,形成25~63μm的微... 详细信息

采用复杂多级方法研究并证实制备具有亚微米/纳米级内部结构的球形W-Cu复合微粉的可能性。首先,采用等离子体化学合成法制备具有核壳结构的W-Cu纳米粉末(W核及Cu壳)。然后,将W-Cu纳米粉末与蔗糖的水悬浮液进行喷雾干燥,形成25~63μm的微粒,收率为50%。最后,用热等离子体射流处理由纳米粉末组成的微粒,形成致密的球形W-Cu颗粒。成品粉末的球化度为90%~95%,体积密度为8.1 g/cm^(3),流动性约为12 s/50 g,杂质中O、C和H的含量(质量分数)分别为0.7%、0.02%~0.2%和0.03%~0.05%。

关键词： W-Cu复合材料等离子体化学合成造粒等离子体球化纳米颗粒微粒微粉

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Experimental measurements of gamma-photon production and estimation of electron/positron production on the PETAl laser facility

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Matter and Radiation at Extremes 2024年第5期9卷 32-47页

作者： F.Brun l.Ribotte G.Boutoux X.davoine P.E.Masson-laborde Y.Sentoku n.Iwata n.Blanchot d.Batani I.lantuéjoul l.lecherbourg B.Rosse C.Rousseaux B.vauzour d.Raffestin E.d’Humières X.Ribeyre Centre lasers Intenses et Applications UMR 5107Universitéde Bordeaux-CNRS-CEA33405 TalenceFrance CEA DAMCESTAF-33116 Le BarpFrance CEA DAMDIFF-91297 ArpajonFrance CEA LMCEUniversitéParis-Saclay91680 Bruyères-le-ChâtelFrance Institute of laser Engineering Osaka University2-6 YamadaokaSuitaOsaka 565-0871Japan

This article reports the first measurements of high-energy photons produced with the high-intensity PETawatt Aquitaine laser(PETAl)*** experiments were performed during the commissioning of the *** laser had an energy of about 400 J,an intensity of 8×10^(18)W cm^(−2),and a pulse duration of 660 fs(FWHM).It was shot at a 2 mm-thick solid tungsten *** high-energy photons were produced mainly from the bremsstrahlung process for relativistic electrons accelerated inside a plasma generated on the front side of the *** paper reports measurements of electrons,protons and *** electrons up to35 Mev with a few-Mev temperature were recorded by a spectrometer,called SESAME(SpectreÉlectronS Angulaire MoyenneÉnergie).K-and l-shells were clearly detected by a photon spectrometer called SPECTIX(Spectromètre PetalàCristal en TransmIssion pour le rayonnnement X).High-energy photons were diagnosed by CRACC-X(Cassette de RAdiographie Centre Chambre-rayonnement X),a bremsstrahlung *** cannon analysis is strongly dependent on the hypothesis adopted for the spectral *** shapes can exhibit similar reproductions of the experimental *** eliminate dependence on the shape hypothesis and to facilitate analysis of the data,simulations of the interaction were *** model the mechanisms involved,a simulation chain including hydrodynamic,particle-in-cell,and Monte Carlo simulations was *** simulations model the preplasma generated at the front of the target by the PETAl laser prepulse,the acceleration of electrons inside the plasma,the generation of Mev-range photons from these electrons,and the response of the detector impacted by the energetic photon *** this work enabled reproduction of the experimental *** high-energy photons produced have a large emission angle and an exponential distribution *** addition to the analysis of the photon spectra,positron production was also ***,if high

关键词： process positron hypothesis

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Output feedback adaptive super twisting sliding mode control for quadrotor UAvs

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Control Theory and Technology 2024年第1期22卷 92-105页

作者： Oscar Salas-Peña Jesus deleón-Morales Susana v.Gutiérrez-Martínez École Centrale de nantes-lS2n UMR 6004 CNRS44300NantesFrance Facultad de Ingeniería Mecánica y Eléctrica Universidad Autónoma de Nuevo León66451San Nicolás de Los GarzaMexico

In this paper, a sliding mode control with adaptive gain combined with a high-order sliding mode observer to solve the tracking problem for a quadrotor UAv is addressed, in presence of bounded external disturbances and parametric uncertainties. The high order sliding mode observer is designed for estimating the linear and angular speed in order to implement the proposed scheme. Furthermore, a lyapunov function is introduced to design the controller with the adaptation law, whereas an analysis of finite time convergence towards to zero is provided, where sufficient conditions are obtained. Regarding previous works from literature, one important advantage of proposed strategy is that the gains of control are parameterized in terms of only one adaptive parameter, which reduces the control effort by avoiding gain overestimation. numerical simulations for tracking control of the quadrotor are given to show the performance of proposed adaptive control–observer scheme.

关键词： Adaptive super twisting controller High-order sliding modes observer UAv

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Simple collective model for nuclear chiral mode

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Frontiers of physics 2024年第2期19卷 1-5页

作者： R.v.Jolos E.A.Kolganova d.R.Khamitova Joint Institute for nuclear Research 141980 DubnaMoscow regionRussia dubna State University 141982 DubnaMoscow RegionRussia

A simple semi-analytical collective model that takes into account the limitations of the variation interval of the collective variable is suggested to describe the chiral dynamics in triaxial odd−odd nuclei with a fixed particle−hole *** collective Hamiltonian is constructed with the potential energy obtained using the postulated ansatz for the wave function symmetric with respect to chiral *** diagonalizing the collective Hamiltonian the wave functions of the lowest states are obtained and the evolution of the energy splitting of the chiral doublets in transition from chiral vibration to chiral rotation regime is demonstrated.

关键词： collective model nuclear chiral

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