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Role of silicon in steels on galvanized coatings

Acta Metallurgica Sinica(English Letters) 2009年第2期22卷 138-145页

作者： chunshan che jintang lu gang kong qiaoyu xu College of Materials Science and Engineering South China University of Technology Guangzhou 510640 China

In this article, five kinds of silicon-containing steel sheets have been electrodeposited, and then immersed in a pure molten zinc bath at 450℃ for various periods of time. The results by scanning electron microscopy （SEM） show that the coating of the sample （0.09 wt pct Si） with iron-electrodeposited pretreatment eliminates the reactive zones which are found in the coating without iron-electrodeposited pretreatment. The galvanized sample （0.28 wt pct Si） with iron-electrodeposited pretreatment exhibits a compact and coherent coating. The coating of the sample （0.37 wt pct Si） with the iron-electrodeposited pretreatment experiences a transition from a compact and coherent coating to a reactive one. The energy dispersive spectrum （EDS） results reveal that for the galvanized samples with iron-electrodeposited pretreatment, excessive silicon accumulates on the surface of the substrate due to the low solubility of silicon in the Г, after the iron layer is depleted by the increasing growth of the Fe-Zn intermetallics. With the movement of the substrate/Г interface toward the substrate, silicon-enriched α-Fe peels off from the substrate and breaks into the particles. The particles move toward the δ layer through the Г layer because silicon-enriched α-Fe cannot be absorbed in the F layer. When the particles reach the δ/Г interface, they are dissolved in the δ laver, making the F laver thin or even vanish.

关键词： Zn coating Intermetallics Steel Electrodeposition Iron

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Influence of Ni-electrodeposited Pretreatment on Galvanized Coatings of Reactive Steels

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Journal of Wuhan University of Technology(Materials Science) 2007年第2期22卷 221-224页

作者：车淳山 College of Materials Science and Engineering South China University of Technology

Four types of steel sheets containing 0.04%, 0.09%, 0. 14% and 0.36% Si, respectively, were electrodeposited with a nickel layer of 3 tam in thickness and then galvanized in molten Zn at 450℃ for various periods of time. The formation and growth of intermetallic compound layers on the surface of the samples were investigated by SEM and EDS. The experimental results show that the method of Ni-electrodeposited pretreatment can distinctively restrain the over-growth of the galvanized coatings of reactive steels and get eligible coatings with a proper thickness, bright appearance and strong adherence. EDS results indicate that a series of Ni-Zn intermetallic compounds γ′, γ and δ, are first formed on the surface of the samples. With a prolonged immersion time, the F2-Fe-Zn-Ni and δ-Fe-Zn are formed accompanied by the gradual disappearance of γ′, γ and δ2 layer. After a longer immersion time, the lumpy ζ- Fe-Zn occurs between δ and liquid Zn and the F-Fe-Zn does between steel substrate and δ. Subsequently, ζ is in the form of a continuous and compact layer. The method of Ni-electrodeposited pretreatment changes the formation of Fe-Zn intermetallic compounds, which delay the growth of lumpy （and promote the growth of compact δ. Consequently, the abnormal growth of reactive steels is eliminated.

关键词： hot-dip galvanizing electrodepositing Ni reactive steel intermetallic compound

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