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Interaction mechanism between BaZrO_(3)/Y_(2)O_(3) refractory and Ti_(2)Ni alloy melts

Journal of Iron and Steel Research International 2024年第6期31卷 1376-1388页

作者： Xiao Hou Guang-yao Chen Jian liu Ming-rui Lv Fei-hai Yu Qi-sheng Feng Rong-bin li Xiong-gang Lu chong-he li State Key Laboratory of Advanced Special Steel and Shanghai Key Laboratory of Advanced Ferromeallurgy and School of Materials Science and Engineering Shanghai UniversityShanghai 200072China Shanghai Special Casting Engineering Technology Research Center Shanghai 201605China Zhejiang Institute of Advanced Materials Shanghai UniversityJiashan 314100ZhejiangChina School of Materials Science and Engineering Shanghai DianJi UniversityShanghai 201306China

The titanium alloys with highly chemical activity require stable crucible refractories that can withstand the erosion of alloy *** phase composition and microstructure are crucial factors that affect the stability of the refractory *** effect of Y_(2)O_(3) on the composition and microstructure of BaZrO_(3) crucible was systematically investigated,and the improved mechanism of the stability of BaZrO_(3)/Y_(2)O_(3) crucible was clarified in comparison with the BaZrO_(3) *** results showed that the erosion layer thickness of the BaZrO_(3)/Y_(2)O_(3) crucible was only 63μm,which was far less than that in the BaZrO_(3) crucible(485μm),and the erosion layer in the BaZrO_(3)/Y_(2)O_(3) crucible also exhibited a higher density than that in the BaZrO_(3) *** the sintering,Y_(2)O_(3) could improve the densification of the BaZrO_(3) crucible due to the solid solution effect between Y_(2)O_(3) and ZrO_(2),which also caused the evaporation of BaO,resulting in the generation of a Y_(2)O_(3)(ZrO_(2))film on the surface of the ***,the Y_(2)O_(3)(ZrO_(2))had higher thermodynamic stability than Y_(2)O_(3),confirming that the BaZrO_(3)/Y_(2)O_(3) crucible with high density exhibited a superior erosion resistance to titanium *** dual-phase structure provides a strategy to design a long-life and stable refractory for melting titanium alloys.

关键词： Barium zirconate Yttrium oxide Dual-phase refractory Titanium alloy Interaction

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Multiple gaseous reduction of ilmenite: thermodynamic and experimental study

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Rare Metals 2015年第12期34卷 888-894页

作者： Wei Xiao Xiong-Gang Lu Xing-li Zou chong-he li Wei-Zhong Ding Shanghai Key Laboratory of Modern Metallurgy and Materials Processing Shanghai University

In this paper, the thermodynamics of the reduction of ilmenite using multiple gases (H2/CO) was calculated. It is found that the metallization rate of 20.1%–98.8%, H2 consumption rate of 43.0%–99.1%, and carbon deposition amount of 5.7×10?7?0.49mol can be obtained based on the conditions of hydrogen volume fraction of 10%–90% and temperature of 450–1200°C. Experimental study was also carried out using synthetic ilmenite as initial materials and reduced in a static bed reactor at 1100°C. The metallization rate reaches 97% when the multiple gas (70% H2/10% CO/20% Ar) flow rate is 120ml·min?1. A thermogravimetric analyzer was used to measure the variation of sample weight caused by the deposition of solid carbon. The amount of carbon deposited during experiments reaches its maximum while the original hydrogen volume content is 20%. The experimental results are well consistent with the thermodynamic analysis.

关键词： Multiple gases Hydrogen Thermodynamic analysis Direct reduction

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Phase transformation and reduction kinetics during the hydrogen reduction of ilmenite concentrate

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International Journal of Minerals,Metallurgy and Materials 2012年第5期19卷 384-390页

作者： Xin-guo Si Xiong-gang Lu Chuan-wei li chong-he li Wei-zhong Ding Shanghai Key Laboratory of Modern Metallurgy and Materials Processing Shanghai University Shanghai 200072 China hebei Iron and Steel Group Tangshan Steel Company Tangshan 063020 China

The reduction of ilmenite concentrate by hydrogen gas was investigated in the temperature range of 500 to 1200℃. The microstructure and phase transition of the reduction products were studied by X-ray diffraction （XRD）, scanning electron microscopy （SEM）, and optical microscopy （OM）. It was found that the weight loss and iron metallization rate increased with the increase of reduction temperature and reaction time. The iron metallization rate could reach 87.5% when the sample was reduced at 1150℃ for 80 min. The final phase constituents mainly consist of Fe, M305 solid solution phase （M=Mg, Ti, and Fe）, and few titanium oxide. Microstructure analysis shows that the surfaces of the reduction products have many holes and cracks and the reactions take place from the exterior of the grain to its interior. The kinetics of reduction indicates that the rate-controlling step is diffusion process control with the activation energy of 89 ***1-1.

关键词： ilmenite phase transformations kinetics hydrogen reduction metallization

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Effect of controlled rolling/controlled cooling parameters on microstructure and mechanical properties of the novel pipeline steel

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Advances in Manufacturing 2014年第3期2卷 265-274页

作者： Min Jiang li-Na Chen Jin he Guang-Yao Chen chong-he li Xiong-Gang Lu Shanghai Key Laboratory of Modern Metallurgy & Materials Processing Shanghai University Baoshan Iron & Steel Co. Ltd. Shanghai Special Casting Engineering Technology Research Center

The study of controlled rolling/controlled cooling process parameters which affect the microstructure and mechanical properties of a novel pipeline steel has been optimized by the orthogonal experiment with four factors and three levels in this paper. However, the parameters of thermo-mechanical control process （TMCP） optimized by the Gleeble-3500 hot simulator could not satisfy performance requirements of the X100 pipeline steel. In order to improve the performance of this steel, the influence of finish cooling temperature （FCT） on the microstructure and property is studied in detail. It is found that, as this steel is thermo-mechanically treated by this set of parameters （the start heating temperature, finish rolling temperature （FRT）, FCT and cooling rate of 1,180 ℃, 810 ℃, 350 ℃ and 35 ℃/s, respectively）, the micro- structures are mainly composed of granular bainite （GB） and acicular ferrite （AF）. The effective grain sizes are below 20 μm; the steel reaches the optimal balance between the strength and the toughness; the yield strength is 695 MPa; the tensile strength is 768 MPa; the elongation is 16.6 %; the impact energy is 262 J at room temperature. All indexes could meet the requirements of X100 pipeline steel.

关键词： Controlled rolling/controlled cooling Finishcooling temperature (FCT) Microstructure ~ Mechanicalproperties X100 pipeline steel

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Longitudinal vibration characteristics of a tapered pipe pile considering the vertical support of surrounding soil and construction disturbance

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Earthquake Engineering and Engineering Vibration 2024年第1期23卷 51-63页

作者： li Zhenya Pan Yunchao he Xianbin Lv chong Mohammad Towhid Key Laboratory of Ministry of Education for Geomechanics and Embankment Engineering Hohai UniversityNanjing 210098China Geotechnical Research Institute Hohai UniversityNanjing 210098China MOE Key Laboratory of Soft Soils and Geoenvironmental Engineering Zhejiang UniversityHangzhou 310058China

This research is concentrated on the longitudinal vibration of a tapered pipe pile considering the vertical support of the surrounding soil and construction ***,the pile-soil system is partitioned into finite segments in the vertical direction and the Voigt model is applied to simulate the vertical support of the surrounding soil acting on the pile *** surrounding soil is divided into finite ring-shaped zones in the radial direction to consider the construction ***,the shear complex stiffness at the pile-soil interface is derived by solving the dynamic equilibrium equation for the soil from the outermost to innermost *** displacement impedance at the top of an arbitrary pile segment is obtained by solving the dynamic equilibrium equation for the pile and is combined with the vertical support of the surrounding soil to derive the displacement impedance at the bottom of the upper adjacent ***,the displacement impedance at the pile head is obtained based on the impedance function transfer ***,the reliability of the proposed solution is verified,followed by a sensitivity analysis concerning the coupling effect of the pile parameters,construction disturbance and the vertical support of the surrounding soil on the displacement impedance of the pile.

关键词： tapered pipe pile longitudinal vibration vertical support of the surrounding soil construction disturbance displacement impedance

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Nanoconfinement-induced water molecules and hydrogen molecules transport behaviors in ball-in-ball structure photocatalysts to improve hydrogen evolution

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Nano Research 2024年第5期17卷 3752-3760页

作者： Ben chong Baorong Xu he li Honghui Ou Guidong Yang XJTU-Oxford Joint International Research Laboratory of Catalysis School of Chemical Engineering and TechnologyXi’an Jiaotong UniversityXi’an 710049China

The diffusion,adsorption/desorption behaviors of water molecules and hydrogen molecules are of great importance in heterogeneous photocatalytic hydrogen *** the study of structure-property-performance relationships,nanoconfined space provides an ideal platform to promote mass diffusion and transfer due to their extraordinary properties that are different from the bulk ***,we designed and prepared a nanoconfined CdS@SiO_(2)-NH_(2) nanoreactor,whose shell is composed of amino-functionalized silica nanochannels,and encapsulates spherical CdS as a photocatalyst *** and simulated results reveal that the amino-functionalized nanochannels promote water molecules’and hydrogen molecules’directional diffusion and *** molecules are enriched in the nanocavity between the core and the shell,and promote the interfacial photocatalytic *** a result,the maximized water enrichment and minimized hydrogen-occupied active sites enable photocatalyst with optimized mass transfer kinetics and localization electron distribution on the CdS surface,leading to superior hydrogen production performance with activity as high as 37.1 mmol·g^(-1)·h^(-1).

关键词： nanochannels photocatalytic hydrogen evolution mass transfer amino-functionalized CdS

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On the electric behaviour of conductive grease inside the contact zone

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Friction 2024年第4期12卷 683-697页

作者： Yuxin ZHOU Jinjie liU Xinming li he chong Bo HAN Qinghua BAI SKF(Shanghai)Automotive Technologies Co. Ltd.Shanghai 201814China School of Mechanical and Automotive Engineering Qingdao University of TechnologyQingdao 266250China

Conductive grease has been considered as a potential solution in addressing electric erosion issue inside motor *** the conductive grease performance,especially the electric and tribological behaviour is crucial for its *** paper combines bulk grease characterization and contact film study considering both electrical and tribological loading *** results show that the electric performance for the selected conductive grease sample is electric field dependent,including both frequency and voltage *** film impedance inside the contact area is closely related to the external electric field,running condition,and lubrication *** following film impedance calculation tells that not only bulk grease electric parameters,but the contact parameter,lubricant film contour and lubrication condition should be considered when performing the overall bearing electrical modelling.

关键词： Electric erosion lubricant conductivity grease film impedance

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Direct observation of oxygen vacancy formation and migration over ceria surface by in situ environmental transmission electron microscopy

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Journal of Rare Earths 2024年第4期42卷 676-682页

作者： Dawei Pang Wei li Ningqiang Zhang Hong he Shengcheng Mao Yanhui Chen liwei Cao chong li Ang li Xiaodong Han Beijing Key Laboratory of Solid Microstructure and Properties Department of Materials and ManufacturingBeijing University of TechnologyBeijing 100124China Beijing Key Laboratory for Green Catalysis and Separation The Faculty of Environment and LifeBeijing University of TechnologyBeijing10124China International Joint Research Laboratory for Quantum Functional Materials of henan School of Physics and MicroelectronicsZhengzhou UniversityZhengzhou450001China

The extremely high structural tolerance of ceria to oxygen vacancies(Ov)has made it a desirable catalytic material for the hydrocarbon oxidation to chemicals and pharmaceuticals and the reduction of gaseous *** is proposed that the formation and diffusion of Ov originate from its outstanding reduction ***,the formation and diffusion process of Ov over the surface of ceria at the atomic level is still ***,the structural and valence evolution of CeO_(2)(111)surfaces in reductive,oxidative and vacuum environments from room temperature up to 700℃was studied with in situ aberration-corrected environmental transmission electron microscopy(ETEM)*** is found to form under a high vacuum at elevated temperatures;however,the surface can recover to the initial state through the adsorption of oxygen atoms in an oxygen-contained ***,in hydrogen environment,the step-CeO_(2)(111)surface is not stable at elevated temperatures;thus,the steps tend to be eliminated with increasing *** with first-principles density function calculations(DFT),it is proposed that O-terminated surfaces would develop in a hypoxic environment due to the dynamic diffusion of Ov from the outer surface to the ***,in a reductive environment,H2 facilitates the formation and diffusion of Ov while Ce-terminated surfaces *** results reveal dynamic atomic-scale interplay between the nanoceria surface and gas,thereby providing fundamental insights into the Ov-dependent reaction of nano-CeO_(2) during catalytic processes.

关键词： Ceria Direct observation In situ ETEM Oxygen vacancy Density function calculations Rareearths

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Calculation of phase equilibria in Al-Fe-Mn ternary system involving three new ternary intermetallic compounds

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Advances in Manufacturing 2018年第2期6卷 247-257页

作者： Lu-Hai Zhou Zhu L Shu-Sen Wang Ren-Min Hu Shi-Hua Wang Zi-Wei Qin Xiong-Gang Lu chong-he li State Key Laboratory of Advanced Special Steel & Shanghai Key Laboratory of Advanced Ferrometallurgy & School of Materials Science and Engineering Shanghai University Shanghai University Shanghai 200072 People's Republic of China Shanghai Special Casting Engineering Technology Research Center Shanghai 201605 People's Republic of China Baosteel Special Steel Co. Ltd. Shanghai 200940 People's Republic of China

In this study, the Al-Fe-Mn ternary system is reassessed by the CALPHAD method. Three new ternary intermetallic compounds are initially described and a rea- sonable and self-consistent set of thermodynamic parameters are established to describe this system. The 973 K, 1 073K, 1 173K, 1 273K, 1 373K, and 1 473K isothermal sections and the 1 073 K, 1 013 K, 968 K and 913 K isothermal sections at the AI corner as well as the liquidus projection at the Al corner are calculated. It is shown that the calculated results are in good agreement with almost all of the experimental results previously reported.

关键词： Al-Fe-Mn - CALPHAD Phase equilibria Isothermal sections

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Accelerating lithium-sulfur battery reaction kinetics and inducing 3D deposition of li_(2)S using interactions between Fe_(3)Se_(4)and lithium polysulfides

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Journal of Energy Chemistry 2024年第8期95卷 540-553,I0012页

作者： Yihan lin liheng li Longjie Tan Yongliang li Xiangzhong Ren Peixin Zhang Chuanxin he lingna Sun College of Chemistry and Environmental Engineering Shenzhen UniversityShenzhen 518060GuangdongChina

Although lithium-sulfur batteries(LSBs)exhibit high theoretical energy density,their practical application is hindered by poor conductivity of the sulfur cathode,the shuttle effect,and the irreversible deposition of li_(2)*** address these issues,a novel composite,using electrospinning technology,consisting of Fe_(3)Se_(4)and porous nitrogen-doped carbon nanofibers was designed for the interlayer of *** porous carbon nanofiber structure facilitates the transport of ions and electrons,while the Fe_(3)Se_(4)material adsorbs lithium polysulfides(liPSs)and accelerates its catalytic conversion ***,the Fe_(3)Se_(4)material interacts with soluble liPSs to generate a new polysulfide intermediate,li_(x)FeS_(y)complex,which changes the electrochemical reaction pathway and facilitates the three-dimensional deposition of li_(2)S,enhancing the reversibility of *** designed LSB demonstrates a high specific capacity of1529.6 mA h g^(-1)in the first cycle at 0.2 *** rate performance is also excellent,maintaining an ultra-high specific capacity of 779.7 mA h g^(-1)at a high rate of 8 *** investigation explores the mechanism of the interaction between the interlayer and liPSs,and provides a new strategy to regulate the reaction kinetics and li_(2)S deposition in LSBs.

关键词： lithium-sulfur batteries Polysulfide intermediates li_(2)S electrodeposition Interlayers Electrostatic spinning Adsorption Catalysis

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