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A Comparative Study of the Hydroxyl and Saponification Values of Polysorbate 60 in International Food Additive Specifications

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American Journal of Analytical Chemistry 2014年第3期5卷 199-204页

作者： Kazuaki Wakita Haruyoshi Kuwabara Noriko Furusho chiye tatebe Kyoko Sato Hiroshi Akiyama Division of Food Additives National Institute of Health Sciences Tokyo Japan Oleo & Specialty Chemicals Research Laboratory NOF Corporation Kawasaki-shi Japan Quality Assurance Department Gunma Complex Shin-Etsu Chemical Co. Ltd. Annaka-shi Japan

We investigated the hydroxyl and saponification values of 27 samples of Polysorbate 60 products that were commercially available worldwide. We observed that the values of most of the studied samples were not within the range established at the Joint FAO/WHO Expert Committee on Food Additives (JECFA), while they did agree with the specifications described in the USA, the EU and Japan. We believe that purities of the new commercial Polysorbate 60 samples are higher than those of the older products which were available when the JECFA specifications were discussed (around 1973). The present study suggests that the hydroxyl and saponification values of the current JECFA specifications for Polysorbate 60 should be re-evaluated.

关键词： Polysorbate 60 Polyoxyethylene Sorbitan Monostearate Hydroxyl Value Saponification Value Emulsifier Specification

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Extraction Method and Determination of Sudan I Present in Sunset Yellow FCF by Isocratic High-Performance Liquid Chromatography

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American Journal of Analytical Chemistry 2012年第8期3卷 570-575页

作者： chiye tatebe Takashi Ohtsuki Noriko Otsuki Hiroki Kubota Kyoko Sato Hiroshi Akiyama Yoko Kawamura National Institute of Health and Sciences 1-18-1 Setagaya-ku Kamiyoga Tokyo 158-8501 Japan

A method to extract and analyze Sudan I present in Sunset Yellow FCF (SYF) products was developed and validated. The method included the simple extraction of Sudan I from the SYF product using water, acetonitrile, and ethyl acetate and high-performance liquid chromatography (HPLC) analysis with isocratic elution using acetonitrile:water (7:3) with a photodiode array detector at 485 nm. This method was found to remove most of the excess SYF colorant and other impurities before injection to the HPLC instrument, making it easy to maintain precision control in routine laboratory tests for Sudan I in the SYF colorant. The detection limit of Sudan I in SYF products was 0.2 μg/g. A survey conducted to determine Sudan I in 13 commercial SYF samples from Japanese manufacturers from 1970 to 2010 showed that the levels of Sudan I ranged from 0.3 to 1.9 μg/g in products manufactured from 1970 to 1996 and were below the limit of detection in products manufactured after 2005.

关键词： Sudan I Sunset Yellow FCF HPLC

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