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The Mechanism of Heating Rate on the Secondary Recrystallization Evolution in Grain Oriented Silicon Steel

Journal of Wuhan University of Technology(Materials Science) 2025年第1期 275-282页

作者：高倩 LI Jun WANG Xianhui cao Laifu GONG Jian LI Bo Central Iron and Steel Research Institute Group Shougang Zhixin Electromagnetic Material R&D (Beijing) Co. Ltd. Beijing Shougang Co. Ltd.

Grain-oriented silicon steels were prepared at different heating rates during high temperature annealing, in which the evolution of magnetic properties, grain orientations and precipitates were studied. To illustrate the Zener factor, the diameter and number density of precipitates of interrupted testing samples were statistically calculated. The effect of precipitate ripening on the Goss texture and magnetic property was investigated. Data indicated that the trend of Zener factor was similar under different heating rates, first increasing and then decreasing, and that the precipitate maturing was greatly inhibited as the heating rate increased. Secondary recrystallization was developed at the temperature of 1 010 ℃ when a heating rate of 5 ℃/h was used, resulting in Goss, Brass and {110} oriented grains growing abnormally and a magnetic induction intensity of 1.90T. Furthermore, increasing the heating rate to 20 ℃/h would inhibit the development of undesirable oriented grains and obtain a sharp Goss texture. However, when the heating rate was extremely fast, such as 40 ℃/h, poor secondary recrystallization was developed with many island grains, corresponding to a decrease in magnetic induction intensity to 1.87 T. At a suitable heating rate of 20 ℃/h, the sharpest Goss texture and the highest magnetic induction of 1.94 T with an onset secondary recrystallization temperature of 1 020 ℃ were found among the experimental variables in this study. The heating rate affected the initial temperature of secondary recrystallization by controlling the maturation of precipitates, leading to the deviation and dispersion of Goss texture, thereby reducing the magnetic properties.

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Progress in studying entanglement and steering from the macroscopic view

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Science China(Physics,Mechanics & Astronomy) 2021年第1期64卷 114-115页

作者： Ye cao School of Physics Beijing Institute of TechnologyBeijing 100081China

Magnons,the collective excitation of magnetically ordered materials,have attracted considerable interest for their low energy consumption,long coherence time and useful working frequency from gigahertz to ***,magnons can coherently interact with phonons,microwave and optical photons,as well as superconducting qubits,as schematically depicted in Figure 1,providing a novel platform to achieve hybrid quantum systems[1].Hybridizing distinct quantum systems with multitasking capabilities is critical in quantum information processing,because a single quantum system cannot keep pace with the fast development of quantum information and satisfy the requirement of building perfect quantum information networks[2].The emergying field cavity spintronics has inspired many interesting physics like nonreciprocal microwave propagation and energy level attraction,together with quite a few applications such as magnon sensors and magnon-photon transducers.

关键词： quantum microwave Figure

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Can patients with mild non-neoplastic lesions diagnosed at baseline screening be safely exempt from surveillance: evidence from multicenter community-based cohorts

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Science China Life Sciences 2025年第1期 263-271页

作者： Siyi He Zhiyi Zhang Guohui Song Zhenhai Wang Chunyun Dai Shipeng Yan Kun Jiang Bingbing Song He Li Maomao cao Dianqin Sun Fan Yang Xinxin Yan Shaoli Zhang Yi Teng Qianru Li Changfa Xia Wanqing Chen Office of Cancer Screening National Cancer Center/National Clinical Research Center for Cancer/Cancer HospitalChinese Academy of Medical Sciences and Peking Union Medical College Department of Gastroenterology Gansu Wuwei Tumor Hospital Cixian Cancer Institute Linzhou Cancer Hospital Center for Disease Control and Prevention of Sheyang County Department of Cancer Prevention and Control Hunan Cancer Hospital and The Affiliated Cancer Hospital of Xiangya School of MedicineCentral South University Luoshan Center for Disease Control and Prevention Office for Cancer Control and Research Affiliated Cancer Hospital of Harbin Medical University

Surveillance recommendations for gastric cancer（GC） in current guidelines focused on advanced precancerous lesions and were based on precise diagnosis of severity/extent of baseline lesions. We aimed to develop a less endoscopy-related equipment-dependent risk-stratification tool, and assessed whether mild-precursor-lesion patients can be safely exempt from surveillance. In the multicenter communitybased cohort, 75,051 participants receiving baseline endoscopy were enrolled during 2015–2017 and followed-up until 2021. Cumulative incidence rates（CIRs） of GC for precancerous-conditions were calculated by Kaplan-Meier method and compared by Log-rank tests. Mixedeffects Cox regression models were used to detect potential factors for progression towards GC. A risk score was calculated as counts of selected factors. An independent cohort, including 26,586 participants was used for external validation. During a median follow-up of 6.25 years, CIRs of GC were 0.302%, 0.436%, and 4.756% for normal group, non-neoplastic（atrophic gastritis/intestinal metaplasia） and neoplastic lesions（low-grade/high-grade dysplasia）, respectively(Ptrend<0.001). Four predictors, including male, ≥60 years, smoking, and limited vegetable consumption, were selected for risk-stratification. High-risk patients（≥3 risk factors） with non-neoplastic lesions showed higher GC risks（adjusted HR=7.73, 95%CI: 4.29–13.92）, and their four-year CIR reached the one-year CIR of neoplastic lesions. Further categorizing non-neoplastic lesions by histological grade, both patients with moderate-to-severe lesions（aHR=3.07, 95%CI: 1.67–5.64） and high-risk patients with mild lesions（aHR=7.29, 95%CI: 3.58–14.86） showed higher risks. Consistent trends were observed in validation cohort. High-risk mild-precursor-lesion patients should receive surveillance within 3–5 years after baseline screening. Our study provides evidence on supplementing current guideline recommendations.

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OBTAINING THE CRITICAL DRAW RATIO OF DRAW RESONANCE IN MELT SPINNING FOR POWER LAW POLYMER FLUIDS

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Chinese Journal of Polymer Science 2007年第5期25卷 501-507页

作者： Jinan cao Industrial Research Institute Swinburne Swinburne University of Technology P.O. Box 218 Hawthorn Victoria 3122 Australia

A direct difference method has been developed for Non-Newtonian power law fluids to solve the simultaneous non-linear partial differential equations of melt spinning, and to determine the critical draw ratio for draw resonance. The results show that for shear thin fluids, the logarithm of the critical draw ratio has a well defined linear relationship with the power index for isothermal and uniform tension melt spinning. When the power index approaches zero, the critical draw ratio points at unity, indicating no melt spinning can be processed stably for such fluids. For shear thick fluids, the critical draw ratio increases in a more rapid way with increasing the power index.

关键词： Draw resonance Melt spinning Power law fluid Numerical simulation.

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Application of Rare Earths in Thermal Barrier Coating Materials

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Journal of Materials Science & Technology 2007年第1期23卷 15-35页

作者： Xueqiang cao Key Lab of Rare Earth Chemistry and Physics Changchun Institute of Applied Chemistry Chinese Academy of Sciences.Changchun 130022 China

Rare earths are a series of minerals with special properties that make them essential for applications including miniaturized electronics, computer hard disks, display panels, missile guidance, pollution controlling catalysts, H2-storage and other advanced materials. The use of thermal barrier coatings （TBCs） has the potential to extend the working temperature and the life of a gas turbine by providing a layer of thermal insulation between the metallic substrate and the hot gas. Yttria （Y203）, as one of the most important rare earth oxides, has already been used in the typical TBC material YSZ （yttria stabilized zirconia）. In the development of the TBC materials, especially in the latest ten years, rare earths have been found to be more and more important. All the new candidates of TBC materials contain a large quantity of rare earths, such as R2Zr207 （R=La, Ce, Nd, Gd）, CeO2-YSZ, RMeAI11019 （R=La, Nd; Me=Mg, Ca, Sr） and LAP04. The concept of double-ceramic- layer coatings based on the rare earth materials and YSZ is effective for the improvement of the thermal shock life of TBCs at high temperature.

关键词： Rare earth Thermal barrier coatings Gas turbine

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Cathodic behavior of molten CaCl_2-cao and CaCl_2-NaCl-cao

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International Journal of Minerals,Metallurgy and Materials 2010年第6期17卷 791-794页

作者： Shu-lan Wang Wei Wang Shi-chao Li Shan-hui cao Department of Chemistry Northeastem University Shenyang 110004 China

The cathodic behavior of molten CaCl2, CaCl2-cao and equimolar CaCl2-NaCl-cao was studied by cyclic voltammograms and constant potential polarization at temperatures of 1123 to 1173 K on molybdenum and titanium electrodes. The diffusion coefficient of Ca2＋（cao） in molten CaCl2-cao was calculated from the linear relationship between the square root of scan rate and the peak current density. The deposition potentials and the potential temperature coefficient of cao in molten CaCl2-0.5mol%cao and CaCl2-NaCl-0.5mol%cao were also obtained from their cyclic voltammograms. The result shows that cao is more easily reduced than CaCl2. The addition of NaCl in molten CaCl2-cao induces the underpotential electrodeposition of cao.

关键词： molten salts calcium oxide cyclic voltammetry polarization

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碳排放权交易制度的权利逻辑与规范进路

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河北大学学报（哲学社会科学版） 2025年第1期50卷 123-134页

作者：柯坚曹辰武汉大学环境法研究所湖北武汉430072

当下我国碳排放权交易制度体系正在经历着由政策引领向法治构建的转变。目前碳排放权交易制度行政立法中简单将“权利”与“配额”等同的做法,既无法体现碳排放权所兼具的公法、私法双重特征,也难以有效回应碳排放权交易市场的发展需求... 详细信息

当下我国碳排放权交易制度体系正在经历着由政策引领向法治构建的转变。目前碳排放权交易制度行政立法中简单将“权利”与“配额”等同的做法,既无法体现碳排放权所兼具的公法、私法双重特征,也难以有效回应碳排放权交易市场的发展需求以及完善碳排放权交易制度的规范构建。为此,需要构建以碳排放权交易市场为语境、以碳排放“权利”为逻辑主线的碳排放权交易制度,夯实其法治基础并明确其规范进路。从语境与语义出发,“碳排放权”的表述本身就意味着其私法的权利属性。在碳排放权交易制度的理论逻辑层面,双阶理论可以为碳排放权交易制度中“配额”到“权利”的过渡提供理论支撑;在其实践逻辑层面,碳排放权交易制度需要借助“权利”的确立为其交易市场的展开提供法治的基础。最后,考虑到碳排放权权利属性共识不足、碳排放权交易制度结构尚待稳定、权利基础呈现多元特征以及权利来源并非稳固不变等因素,策略上可以考虑暂时搁置碳排放权权属争议,以权益为抓手、以“权益表现—适用规范领域—法律保护方式”为主线,分步骤、分阶段推进碳排放权交易制度的规范构建。

关键词：碳排放权权益配额权利逻辑规范进路

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Constructing Pr-doped CoOOH catalytic sites for efficient electrooxidation of 5-hydroxymethylfurfural

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Journal of Energy Chemistry 2025年第1期 234-244页

作者： Botao Fan Hao Zhang Bang Gu Feng Qiu Qiue cao Wenhao Fang School of Chemical Science and Technology Yunnan University National Center for International Research on Photoelectric and Energy Materials School of Materials and Energy Yunnan University

Electrocatalytic conversion of renewable biomass is emerging as a promising route for sustainable chemical production;hence it urgently calls for developing efficient electrocatalysts with low potentials and high current ***,a Pr-doped Co（OH）2hexagonal sheet （Pr/Co=1/9,in mole） is synthesized by electrodeposition as highly performant catalyst for 5-hydroxymethylfurfural （HMF） oxidation reaction（HMFOR） to produce 2,5-furandicarboxylic acid （FDCA）.This novel and low-cost catalyst possesses a rather low onset potential of 1.05 V （***） and requires only 1.10 V （***） to reach a current density of 10 mA cm-2for HMFOR,significantly outperforming Co（OH）2benchmark (i.e.,210 mV higher to reach10 m A cm-2).The origin of Pr promotion effect as well as the evolution of CoOOH catalytic sites and HMFOR process has been deeply elucidated by physical characterizations,kinetic experiments,in situ electrochemical techniques,and theoretical *** unique Pr-ameliorated CoOOH active centers enable 100%conversion of HMF,99.6%selectivity of FDCA,and 99.7%Faraday efficiency,with a superior cycling durability toward *** can be one of the most outstanding results for Co-based HMFOR catalysts to date in the *** this work can help open up new horizons for constructing novel and efficient Co-based electrocatalysts by the utilization of lanthanide elements.

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深板层角膜移植与穿透性角膜移植治疗基质角膜营养不良预后的比较

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中国组织工程研究 2025年第8期29卷 1626-1633页

作者：静如意陈颖欣曹蕾北部战区总医院辽宁省沈阳市110000

背景:基质角膜营养不良的传统手术治疗方式为穿透性角膜移植,近年来越来越多的医生开始考虑使用深板层角膜移植治疗基质角膜营养不良。目前国内对比穿透性角膜移植和深板层角膜移植治疗基质角膜营养不良的研究少有报道。目的:比较深板... 详细信息

背景:基质角膜营养不良的传统手术治疗方式为穿透性角膜移植,近年来越来越多的医生开始考虑使用深板层角膜移植治疗基质角膜营养不良。目前国内对比穿透性角膜移植和深板层角膜移植治疗基质角膜营养不良的研究少有报道。目的:比较深板层角膜移植和穿透性角膜移植治疗基质角膜营养不良的疗效。方法:选择2000年1月至2018年1月北部战区总医院收治的基质角膜营养不良患者57例(57眼),男18例,女39例,平均年龄(52.9±20.0)岁,按照手术治疗方式分为深板层角膜移植组(n=21)、穿性角膜移植组(n=36),术后随访观察最佳矫正视力、角膜内皮细胞密度、角膜植片透明度、术中及术后并发症、原病复发情况。结果与结论:①两组患者术后1,3,6,12个月的视力均高于术前(P0.05);随着术后时间的延长,两组患者角膜内皮细胞密度逐渐降低,穿透性角膜移植组患者术后6,12个月的角膜内皮细胞密度年丢失率均高于深板层角膜移植组(P0.05);②深板层角膜移植组有6例出现并发症,穿透性角膜移植组有14例出现并发症,57例患者术后12个月内均无复发,两组患者术后5年的复发率比较差异无显著性意义(P>0.05),穿透性角膜移植组和深板层角膜移植组术后5年的移植物存活率分别为83%和86%,组间比较差异无显著性意义(P>0.05);③结果表明,基质角膜营养不良的治疗可考虑使用深板层角膜移植替代一部分穿透性角膜移植。

关键词：穿透性角膜移植深板层角膜移植基质角膜营养不良最佳矫正视力角膜植片透明度角膜内皮细胞密度并发症复发

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有限元分析冠状动脉新型刻痕球囊的安全性及有效性

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中国组织工程研究 2025年第10期29卷 2083-2090页

作者：曹政郑晓新蒋学俊武汉大学人民医院心内科武汉大学心血管病研究所心血管病湖北省重点实验室湖北省武汉市430060

背景:目前临床上使用的冠状动脉介入预扩张球囊主要是传统的高压球囊、乳突球囊等,它们在病变血管中可能会出现滑脱进而擦伤血管的情况。目的:评估新型旋刻球囊在血管扩张中的安全性及有效性。方法:(1)有限元分析:通过采集相关人体组织... 详细信息

背景:目前临床上使用的冠状动脉介入预扩张球囊主要是传统的高压球囊、乳突球囊等,它们在病变血管中可能会出现滑脱进而擦伤血管的情况。目的:评估新型旋刻球囊在血管扩张中的安全性及有效性。方法:(1)有限元分析:通过采集相关人体组织数据建立血管三维有限元模型,随后建立乳突球囊植入血管三维有限元模型与旋刻球囊植入血管三维有限元模型,分析不同充气压下球囊扩张时的血管应力、血管位移、球囊应力、球囊位移。(2)动物实验:将8只新西兰大耳兔随机分成2组,在髂动脉中分别植入乳突球囊与旋刻球囊进行扩张,每组4只。球囊撤出后取材,苏木精-伊红染色与透射电镜观察血管损伤情况。结果与结论:(1)有限元分析:两种球囊的弹力性质无明显差异,在相同充气压下,乳突球囊组血管应力、血管位移、球囊应力、球囊位移均远远大于旋刻球囊组,并且各指标的均匀性优于旋刻球囊组;随着充气压的增加,乳突球囊组血管应力、血管位移、球囊应力、球囊位移增加幅度远远大于旋刻球囊组。(2)动物实验:苏木精-伊红染色与透射电镜观察显示,旋刻球囊扩张造成的血管损伤只局限在内膜,而乳突球囊扩张造成的血管损伤比较严重,内膜、中膜损伤严重,部分节段可以看到血肿形成,血管周围的炎性细胞较多,局部可见有巨噬细胞堆积。(3)结果表明:相较于乳突球囊扩张,旋刻球囊扩张造成血管闭塞以及夹层的风险较小,但有一定出现球囊弯曲的概率。

关键词：冠状动脉粥样硬化预扩张新型扩张球囊血管损伤有限元分析旋刻球囊

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