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Primary dendrite growth kinetics and rapid solidification mechanism of highly undercooled Ti-Al alloys

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Journal of Materials Science & Technology 2020年第5期40卷 47-53页

作者： z.c.Luo H.P.Wang Department of Applied Physics Northwestern Polytechnical UniversityXi’an 710072China

The rapid solidification processes of undercooled Ti-(47,50,54)at.%Al alloys were investigated by electromagnetic levitation(EML)method combined with a high-speed photoelectric *** maximum undercoolings of the three liquid alloys were 376 K,352 K and 316 K,*** processes corresponding to the primary dendrite growth and subsequent phase transition were recorded at various *** primary dendrite growth velocity V meets a double exponential relationship with the undercooling ***,a novel formula with physical meaning is proposed to explain that the more ordered liquid metal atoms accelerate the primary dendrite *** recalescences are found at all undercoolings for Ti-47 at.%Al alloy and at high undercoolings for Ti-50 at.%Al *** microstructures of solidified Ti-47 at.%Al alloys successively appear as coarse lamellar dendrites and finally evolve to refined parallel lamellar dendrites with the increasing *** T rises,the microstructures of solidified Ti-50 at.%Al alloys appear from coarse primary dendrites and interdendritic dendrites to refined lamellar *** the process from low undercooling to high undercooling,the primary phase of undercooled Ti-54 at.%Al alloys changes from r-Ti(r)to r-TiAl(r)and the microstructures of solidified alloys evolve from spherical primary dendrites and matrix phases to cellular dendrite ***,for the Ti-(47,50)at.%Al,the transformation temperature of metastable intermediateγphase decreases with the increase of ***,the microhardness of the three solidified alloys reaches the maximum when the undercoolings are 185 K,270 K and 316 K,respectively.

关键词： Electromagnetic levitation Rapid solidification Dendrite growth Microstructure Microhardness

Sulfide elimination by intermittent nitrate dosing in sewer sediments

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Journal of Environmental Sciences 2015年第1期27卷 259-265页

作者： Yanchen Liu chen wu Xiaohong zhou David z.zhu Hanchang Shi School of Environment Tsinghua University Department of civil and Environmental Engineering University of Alberta

The formation of hydrogen sulfide in biofilms and sediments in sewer systems can cause severe pipe corrosions and health hazards, and requires expensive programs for its prevention. The aim of this study is to propose a new control strategy and the optimal condition for sulfide elimination by intermittent nitrate dosing in sewer sediments. The study was carried out based on lab-scale experiments and batch tests using real sewer sediments. The intermittent nitrate dosing mode and the optimal control condition were investigated. The results indicated that the sulfide-intermittent-elimination strategy by nitrate dosing is advantageous for controlling sulfide accumulation in sewer sediment. The oxidation–reduction potential is a sensitive indicator parameter that can reflect the control effect and the minimum N/S（nitrate/sulfide）ratio with slight excess nitrate is necessary for optimal conditions of efficient sulfide control with lower carbon source loss. The optimal control condition is feasible for the sulfide elimination in sewer systems.

关键词： Sewer system Sulfide elimination Sediment Optimal condition Intermittent nitrate dosing

Y-Ba-cu-O mixed oxides for production of diphenols in liquid-solid phase

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chinese Journal of chemistry 1996年第6期14卷 516-524页

作者： Liu, cB zhao, z Yang, XG Ye, XK wu, Y cHINESE AcAD ScI CHANGCHUN INST APPL CHEMCHANGCHUN 130022JILINPEOPLES R CHINA

Superconductor mixed oxides were often used as catalysts at higher temperature in gas phase oxidations, and considered not suitable for lower temperature reactions in the liquid-solid phase; here the catalysis of YBa2cu3O7+/-x and Y2BacuO5+/-x in the phenol hydroxylation at lower temperature with H2O2 as oxygen donor was studied, and found that the superconductor YBa2cu3O7+/-x, has no catalytic activity for phenol hydroxylation, but Y2BacuO5+/-x does, even has better catalytic activity and stability than most previously reported ones. With the studies of catalysis of other simple metal oxides and perovskite-like mixed oxides, a radical substitution mechanism is proposed and the experimental facts are explained clearly, and draw a conclusion that the perovskite-like mixed oxides with (AO)(ABO(3)) and (AO)2(ABO(3)) structure have better catalytic activity than the simple perovskite oxides with (ABO(3))(3) structure alone, and (AO) structure unit is the key for the mixed oxides to have the phenol hydroxylation activity. No pollution of this process is very important for its further industrial application.

关键词： superconductor mixed oxides phenol hydroxylation radical substitution

On a general theory for compressing process and aeroacoustics:linear analysis

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Acta Mechanica Sinica 2010年第3期26卷 355-364页

作者： E .Mao Y. P. Shi J. z. wu State Key Laboratory for Turbulence and complex Systems College of Engineering Peking University 100871 Beijing China University of Tennessee Space Institute Tullahoma TN 37388 USA

Of the three mutually coupled fundamental processes （shearing, compressing, and thermal） in a general fluid motion, only the general formulation for the compress- ing process and a subprocess of it, the subject of aeroacous- tics, as well as their physical coupling with shearing and thermal processes, have so far not reached a consensus. This situation has caused difficulties for various in-depth complex multiprocess flow diagnosis, optimal configuration design, and flow/noise control. As the first step toward the desired formulation in fully nonlinear regime, this paper employs the operator factorization method to revisit the analytic linear theories of the fundamental processes and their decomposi- tion, especially the further splitting of compressing process into acoustic and entropy modes, developed in 1940s-1980s. The flow treated here is small disturbances of a compressible, viscous, and heat-conducting polytropic gas in an unbounded domain with arbitrary source of mass, external body force, and heat addition. Previous results are thereby revised and extended to a complete and unified theory. The theory pro- vides a necessary basis and valuable guidance for developing corresponding nonlinear theory by clarifying certain basic issues, such as the proper choice of characteristic variables of compressing process and the feature of their governing equations.

关键词： Longitudinal (compressing) processTransversal (shearing) process Acoustic mode Entropy mode Aeroacoustics

Measurement and Prediction of Insertion Force for the Mosquito Fascicle Penetrating into Human Skin

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Journal of Bionic Engineering 2009年第2期6卷 143-152页

作者： X Q Kong c W wu State Key Laboratory of Structural Analysis for Industrial Equipment Department of Engineering MechanicsDalian University of Technology

Mosquitoes are exceptional in their ability to pierce into human skin with a natural ultimate painless microneedle, named fascicle. Here the structure of the Aedes albopictus mosquito fascicle is obtained using a Scanning Electron Microscope (SEM), and the whole process of the fascicle inserting into human skin is observed using a high-speed video imaging technique. Direct measurements of the insertion force for mosquito fascicle to penetrate into human skin are reported. Results show that the mosquito uses a very low force (average 18 μN) to penetrate into the skin. This force is at least three orders of magnitude smaller than the reported lowest insertion force for an artificial microneedle with an ultra sharp tip to insert into the human skin. In order to understand the piercing mechanism of mosquito fascicle tip into human multilayer skin tissue, a numerical simulation is conducted to analyze the insertion process using a nonlinear finite element method. A good agreement occurs between the numerical results and the experimental measurements.

关键词： biomimetic microneedle mosquito fascicle mechanics penetration

Exergy analysis of R1234ze（z） as high temperature heat pump working fluid with multi-stage compression

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Frontiers in Energy 2017年第4期11卷 493-502页

作者： Bin HU Di wu L.W. WANG R.z. WANG Institute of Refrigeration and cryogenics Shanghai Jiao Tong University Shanghai 200240 China

In this paper, the simulation approach and exergy analysis of multi-stage compression high tempera- ture heat pump （HTHP） systems with R1234ze（z） working fluid are conducted. Both the single-stage and multi-stage compression cycles are analyzed to compare the system performance with 120℃ pressurized hot water supply based upon waste heat recovery. The exergy destruction ratios of each component for different stage compression systems are compared. The results show that the exergy loss ratios of the compressor are bigger than that of the evaporator and the condenser for the single-stage compres- sion system. The multi-stage compression system has better energy and exergy etticiencies with the increase of compression stage number. compared with the single- stage compression system, the coefficient of performance （cOP） improvements of the two-stage and three-stage compression system are 9.1% and 14.6%, respectively. When the waste heat source temperature is 60℃, the exergy efficiencies increase about 6.9% and 11.8% for the two-stage and three-stage compression system respec- tively.

关键词： multi-stage compression high temperatureheat pump heat recovery exergy destruction,R1234ze(z) working fluid

ELEcTROcHEMIcAL NOISE ANALYSIS OF THE INFLUENcE OF THE zn^(2+)IONS cONcENTRATION ON zINc ELEcTROPLATING

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Acta Metallurgica Sinica(English Letters) 2005年第2期18卷 137-144页

作者： z.zhang c.S.wu Q.Y.cai F.H.cao J.Q.zhang Departmentofchemistry ZhejiangUniversityHangzhou310027China Departmentofchemistry ZhejiangUniversityHangzhou310027China／／StateKeyLaboratoryforCorrosionandProtectionInstituteofMetalResearchTheChineseAcademyofSciencesShenyang110016China

The influence of the concentration of zn2+ ions on zinc electroplating process was investigated by means of electrochemical noise (EN) and cyclic voltammetry methods in conjunction with the scanning electron microscopy (SEM) technique. It was found that the EN generated during the electroplating of dentritic or large polymeric zinc deposit has large potential oscillation amplitude and positive potential drift while the compact zinc deposit possesses small noise amplitude and little potential drift. With the change of rate determining step from diffusion-control through mixed-control to activation-control, the maximum relative energy obtained from wavelet analysis defined from the region with larger scales to those with smaller scales, and the EDP (relative energy distribution plot) can be us, as 'fingerprints' of EN to characterize the electroplating process and the deposit structure. The results also showed that electrochemical noise technique can give more information about the electrodeposit structure than other normal electrochemical measurements, such as linear potential sweep method and cyclic voltammetry technique.

关键词： zinc electroplating zinc ions concentration electrochemical noise electrodeposit structure

Revealing the high-frequency attenuation mechanism of polyurea-matrix composites

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Acta Mechanica Sinica 2020年第1期36卷 130-142页

作者： J.cheng z.L.Liu c.c.Luo T.Li z.J.Li Y.Kang z.zhuang Applied Mechanics Laboratory School of Aerospace EngineeringTsinghua UniversityBeijing100084China Key Laboratory of Advanced Materials of Ministry of Education Department of Chemical EngineeringTsinghua UniversityBeijing100084China School of Materials Science and Engineering Tsinghua UniversityBeijing100084China

In this paper,a method for analyzing the high-frequency attenuation property of polyurea-matrix composites is developed by combining experimental,computational and theoretical ***,the ultrasonic experimental platform is established by solving the difficulties of high-frequency ultrasonic testing as high-frequency signal distortion,insufficient driving voltage and sampling rate failure,to study the dynamic mechanical properties(1-5 MHz)of pure polyurea and polyurea-matrix ***,the influences of composite parameters including the size and volume fraction of inclusions on wave attenuation performance under different frequencies are obtained and further verified by numerical ***,the contribution of inclusions to the wave attenuation performance is also theoretically *** is found that the increase of inclusion volume fraction and inclusion diameter will increase the attenuation coefficient of the *** the attenuation of composites with the inclusions of a 150-μm diameter and 30%as volume fraction can be 82%higher than pure *** amplifying attenuation effect of inclusions is mainly attributed to the scattering effect,which is verified by comparing numerical and theoretical results.

关键词： Polyurea Viscoelastic Dynamic mechanical properties Ultrasound

A betatron tune measurement system based on bunch-by-bunch transverse feedback at the Duke storage ring

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chinese Physics c 2013年第7期37卷 76-82页

作者：徐卫 W. z. wu 李京祎何多慧 Y. K. wu National Synchrotron Radiation Laboratory (NSRL) University of Science and Technology of China FEL Laboratory TUNL and Department of Physics Duke University

To combat electron beam instabilities, a digital bunch-by-bunch transverse feedback （TFB） system has been developed for the Duke storage ring. While it is capable of suppressing transverse beam instabilities for multibunch operation, the TFB system has not been needed for typical operation of the Duke storage ring. To explore the great potential of this system, we have developed beam diagnostic techniques using the TFB, in particular, the TFB based tune measurement techniques. The tune measurement technique allows us to conduct fast chromaticity measurements, compared with the existing chromaticity measurement system using a network analyzer. This new tune measurement system also enables us to measure the bunch tune for multibunch operation of the Duke storage ring. With the TFB based tune measurement system, we have studied the tune stability of the electron beam in the Duke storage ring. This tune system has also been used to calibrate the tune knob for the Duke storage ring.

关键词： transverse feedback tune chromaticity