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A review on graphite surface modification methods towards low carbon-containing refractories

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Journal of Iron and Steel Research International 2024年第6期31卷 1291-1303页

作者： Ting-ting Zhang Jun Ding bei-yue ma Zheng-long Liu Chao Yu Cheng-ji Deng The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan 430081HubeiChina School of Metallurgy Northeastern UniversityShenyang 110819LiaoningChina

The rapid development of iron and steel metallurgy technology has promoted the continuous innovation and iteration of carbon-containing refractories for clean steel *** meet the high-quality requirements for clean steel production and full exploit the performance advantages of carbon-containing refractories in dynamic smelting environment,it is necessary to explore the role of graphite and modified graphite in carbon-containing *** on this,graphite surface modification methods,including surfactants,surface oxidation,and surface coating,and their applications in carbon-containing refractories are *** advantages and disadvantages of each method are analyzed for practical ***,combined with the existing problems,the application prospect of improved graphite in carbon-containing refractories is discussed.

关键词： Graphite Carbon-containing refractory Clean steel Surface modification Service performance

Leaching behavior and microstructure of phosphorus in converter slag

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Journal of Iron and Steel Research International 2024年第7期31卷 1646-1660页

作者： Chao-gang Zhou Jin-yue Li Qing-gong Chen Yin-ye Yang Wei Gong Li-qun Ai Shu-huan Wang bei-yue ma College of Metallurgy and Energy North China University of Science and TechnologyTangshan 063210HebeiChina Key Laboratory for Ferrous Metallurgy and Resources Utilization of Ministry of Education Wuhan University of Science and TechnologyWuhan 430081HubeiChina College of materials Science and Engineering Guizhou Minzu UniversityGuiyang 550025GuizhouChina School of materials and Architectural Engineering Guizhou Normal UniversityGuiyang 550025GuizhouChina School of Metallurgy Northeastern UniversityShenyang 110819LiaoningChina

Converter slag is a by-product of the steelmaking process and contains a large amount of Ca,Fe,P and other *** the phosphorus in the converter slag can be effectively extracted,the resulting phosphorus can be used as a phosphate *** in converter slag is mainly enriched in 2CaO·SiO_(2)-3CaO·P_(2)O_(5)(C_(2)S-C_(3)P)solid solution and is easily dissolved in ***,acid leaching method was used to dissolve the solid solution to extract phosphorus in converter slag,so as to realize the recycling of phosphorus resources in converter *** leaching behavior of three actual converter slags from different steel mills in acid leaching solutions composed of citric acid,sodium hydroxide,hydrochloric acid and deionized water was studied by X-ray diffraction,scanning electron microscopy combined with energy dispersive spectrometry,Fourier transform infrared spectroscopy and Raman spectroscopy to reveal the change in object image structure as well as SiO_(4) and PO_(4) tetrahedron before and after acid *** results show that only a small amount of phosphorus in converter slag with too low basicity is enriched in C_(2)S-C_(3)P solid solution,resulting in poor leaching *** the converter slag has a high basicity,the removal effect of phosphorus is 70.64%-81.88%.In addition,when the basicity of converter slag is roughly the same,the dephosphorization effect of slag with high FeO content is relatively *** acid leaching will cause depolymerization behavior of SiO_(4) and PO_(4) tetrahedron,so that the mole fraction of Q0(Si)(asymmetric stretching vibration of Si-O bond in SiO_(4) tetrahedron with bridge oxygen number of 0)and NBO/Si(non-bridging oxygen in silicate tetrahedra)will ***-containing solids can be obtained from the solution after acid leaching through static precipitation,and the solids have the potential to make phosphate fertilizers.

关键词： Dephosphorization converter slag Acid leaching Phosphorus Solid solution Slag structure

Corrosion resistance of BN-ZrO_(2)ceramics with different additives by molten steel

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Journal of Iron and Steel Research International 2022年第7期29卷 1101-1109页

作者： Fan Qian Hua-long Li Wen-gang Yang Hai-rong Guo Guo-qi Liu Hong-xia Li bei-yue ma State Key Laboratory of Advanced Refractories Sinosteel Luoyang Institute of Refractories Research Co.Ltd.Luoyang 471039HenanChina Institute of Research of Iron and Steel ShasteelZhangjiagang 215625JiangsuChina School of Metallurgy Northeastern UniversityShenyang 110819LiaoningChina

BN–ZrO_(2)ceramics with different additives such as SiC,Al_(2)O_(3) and MgAl_(2)O_(4) were fabricated by hot pressing sintering process to study sintering properties and corrosion resistance by the rotary immersion molten steel *** results showed that SiC,Al_(2)O_(3) and MgAl_(2)O_(4) can improve the sintering properties of BN–ZrO_(2)ceramics;especially,the introduction of SiC can significantly improve the hardness of the material;thus,the above compounds will help to improve the wear resistance of BN–ZrO_(2)*** exposed oxide layer is in contact with molten steel and forms liquid phase after BN oxidation and B_(2)O_(3) volatilization,additives can significantly affect the properties of liquid phase,and m-ZrO_(2)grains are sintered and grown by dissolution–precipitation mechanism by liquid ***,Al_(2)O_(3) and MgAl_(2)O_(4) are more conducive to the formation of working layer with solid skeleton,which determines the corrosion resistance of BN–ZrO_(2)ceramics.

关键词： Thin strip continuous casting Side-dam Hot-pressing sintering BN–ZrO_(2)ceramic

Recent progress in synthesis of composite powders and their applications in low-carbon refractories

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Journal of Iron and Steel Research International 2022年第7期29卷 1041-1051页

作者： Ji-yuan Luo Xin-ming Ren Xiao-chuan Chong Dong-hai Ding bei-yue ma Guo-qing Xiao Jing-kun Yu College of materials Science and Engineering Xi’an University of Architecture and TechnologyXi’an 710055ShaanxiChina School of Metallurgy Northeastern UniversityShenyang 110819LiaoningChina

The development of low-carbon refractories is of great significance,but it is limited by the deteriorated properties that resulted from the decreased graphite *** composite powders has proved to be effective in improving the properties of low-carbon *** recent progress in the synthesis of composite powders including modified graphite,nanocarbon-containing composite powders,oxide/non-oxide and non-oxide composite powders and their applications in low-carbon refractories were reviewed,and the future development of composite powder technology was prospected.

关键词： Composite powder Modified graphite Nanocarbon-containing composite powder Oxide/non-oxide Non-oxide Low-carbon refractory

Characterization and mechanism of dissolution behavior of Al_(2)O_(3)/MgO oxides in molten slags

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Journal of Iron and Steel Research International 2022年第11期29卷 1711-1722页

作者： Yan-zhu Huo Hua-zhi Gu Ao Huang bei-yue ma Liu-gang Chen Guang-qiang Li Ya-wei Li The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan 430081HubeiChina School of Metallurgy Northeastern UniversityShenyang 110819LiaoningChina Henan Key Laboratory of High Temperature Functional Ceramics Zhengzhou UniversityZhengzhou 450001HenanChina

Al_(2)O_(3)-and MgO-based oxides are among the most common oxides in the steelmaking *** exist as the main components of refractories,inclusions,or ***_(2)O_(3)-and MgO-based oxides interact with molten slags continuously during the steel smelting process,which may lead to the dissolution and absorption of the oxides by molten slags,or reactions between oxides and molten slags to form intermediate *** the dissolution behavior of Al_(2)O_(3)-and MgO-based oxides in molten slags is important for prolonging the service life of refractories and removing inclusions in molten ***,Al_(2)O_(3)-and MgO-based oxides are considered,and the test methods,dissolution mechanisms,and influencing factors are comprehensively introduced,which can provide a foundation for refractories wear and high-quality steel smelting.

关键词： Al_(2)O_(3)/MgO oxide Slag corrosion Refractory wear Inclusion Dissolution mechanism

Enhanced oxidation resistance of low-carbon MgO-C refractories with ternary carbides:a review

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Journal of Iron and Steel Research International 2022年第7期29卷 1052-1062页

作者： Chao Yu Bo Dong Yu-feng Chen bei-yue ma Jun Ding Cheng-ji Deng Hong-xi Zhu Jing-hui Di The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan 430081HubeiChina School of Metallurgy Northeastern UniversityShenyang 110819LiaoningChina

The demand for low-carbon MgO–C refractories is ever growing to meet the development of advanced steelmaking technologies and efficient energy ***,to improve the oxidation resistance and inhibit the weakness of low-carbon MgO–C refractories,antioxidants are *** application of ternary carbides that focused on improving the oxidation performance of MgO–C refractories has been explored,and the ternary carbides including Al_(4)O_(4)C,Al8B_(4)C_(7),Al_(4)SiC_(4),Ti_(2)AlC,Ti_(3)AlC_(2),and Ti_(3)SiC_(2)have been proved *** crystal structure,physical properties,oxidation behavior,and synthesis of these ternary carbides were summarized,and their oxidation mechanism in assisting antioxidation of MgO–C refractories was *** addition,the potential aspects related to the usage and development of ternary carbides in low-carbon MgO–C refractories were proposed.

关键词： Low-carbon MgO–C refractory Ternary carbide maX phase Oxidation mechanism Oxidation resistance

Influence of pre-synthesized Al_(2)O_(3)-SiC composite powder from clay on properties of low-carbon MgO-C refractories

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Journal of Iron and Steel Research International 2022年第7期29卷 1080-1088页

作者： bei-yue ma Xin-ming Ren Zhi Gao Fan Qian Zhao-yang Liu Guo-qi Liu Jing-kun Yu Gao-feng Fu Key Laboratory for Ecological Metallurgy of Multimetallic Mineral(Ministry of Education) Shenyang 110819LiaoningChina School of Metallurgy Northeastern UniversityShenyang 110819LiaoningChina State Key Laboratory of Advance Refractories Sinosteel Luoyang Institute of Refractories Research Co.Ltd.Luoyang 471039HenanChina

To improve the properties of low-carbonization of MgO–C refractories,the introduction of composite additives is an effective ***_(2)O_(3)–SiC composite powder was prepared from clay using electromagnetic induction heating and carbon embedded ***,the Al_(2)O_(3)–SiC composite powder synthesized by electromagnetic induction heating at 600 A was added into low-carbon MgO–C refractories(4 wt.%)to improve their *** results showed that when the addition amount of Al_(2)O_(3)–SiC composite powder is within the range of 2.5–5.0 wt.%,the properties of low-carbon MgO–C samples were significantly improved,e.g.,the apparent porosity of 7.58%–8.04%,the bulk density of 2.98–2.99 g cm-3,the cold compressive strength of 55.72–57.93 MPa,the residual strength after three air quenching at 1100°C of 74.86%–78.04%,and the decarburized layer depth after oxidized at 1400°C for 2 h of 14.03–14.87 ***,the idea for the rapid synthesis of Al_(2)O_(3)–SiC composite powder provides an alternative low-carbon MgO–C refractories performance optimization strategy.

关键词： MgO–C refractory Electromagnetic induction heating Al_(2)O_(3)–SiC composite powder Oxidation

Comparison study of slag corrosion resistance of MgO–MgAl_(2)O_(4),MgO–CaO and MgO–C refractories under electromagnetic field

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Journal of Iron and Steel Research International 2021年第1期28卷 38-45页

作者： Xin‑ming Ren bei‑yue ma Shi‑ming Li Hong‑xia Li Guo‑qi Liu Wen‑gang Yang Fan Qian Shi‑xian Zhao Jing‑kun Yu Key Laboratory for Ecological Metallurgy of Multimetallic Mineral(Ministry of Education) School of MetallurgyNortheastern UniversityShenyang 110819LiaoningChina State Key Laboratory of Advance Refractories Sinosteel Luoyang Institute of Refractories Research Co.Ltd.Luoyang 471039HenanChina

To illuminate the corrosion behavior of MgO-based refractories under electromagnetic field(EMF),herein,the slag corrosion and penetration resistance of MgO–MgAl_(2)O_(4),MgO–CaO,and MgO–C refractories were investigated using the rotary immersion slag resistance test at 1873 K for 1 *** results showed that the order of the good slag resistance of as-tested refractories was MgO–C>MgO–CaO>MgO–MgAl_(2)O_(4).The EMF accelerated the corrosion and penetration of slag to the refractories,which caused the molten slag to be easier into the refractories by natural convection and marangoni *** addition,the MgO–C refractories did not show an overwhelming advantage in slag resistance because EMF impeded the formation of the dense protection ***,in view of the present results,the MgO–C refractories are still the most promising slag line material for refining furnace among MgO–MgAl_(2)O_(4),MgO–CaO,and MgO–C refractories.

关键词： MgO-based refractory Corrosion Basic slag Electromagnetic field

Physics based circuit compatible model for hybrid antiferroelectric random access memory

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Science China(Information Sciences) 2025年第1期68卷 396-397页

作者： Qiuxia WU yue PENG Wenwu XIAO Wenxuan ma Shuo ZHANG Litao SUN Chunfu ZHANG Xiaohua ma yue HAO School of Microelectronics Xidian University Xi'an Uni IC Semiconductors

Since the discovery of HfO2-based ferroelectric （FE） materials in 2011,considerable advancements have been made in material preparation,mechanism research,and device realization [1].Consequently,these materials are now regarded as leading candidates for embedded non-volatile memory（eNVM）.Beyond eNVM applications,recent studies have demonstrated that memory devices with antiferroelectric（AFE） films can achieve high response speeds,low latency,and reduced power consumption while maintaining excellent endurance characteristics [2,3].Additionally,the typical double hysteresis loops and multiple non-overlapping polarization current peaks of AFE films offer a novel approach to designing multistate ***,in order to further promote the application of high storage density AFE,an AFRAM electronic design automation （EDA） model must be developed,and it has yet to be proposed.

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