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Synthesis of ABA Type Block Copolymers of Poly(Ethylene Glycol)and Poly(Dodecyl Vinyl Ether)and Its Using as Surfactant in Emulsion Polymerization

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American Journal of Analytical Chemistry 2014年第1期5卷 39-44页

作者： Yesim Hepuzer Gursel Ayfer Sarac bahire filiz senkal Department of Chemistry Istanbul Technical UniversityIstanbulTurkey Department of Chemistry Yildiz Technical UniversityIstanbulTurkey

A poly(ethylene glycol) (PEG) based macroinitiator (MI) with terminal chloride atom at both ends was prepared by the reaction of PEG-400 with chloroacetyl chloride and used for the cationic polymerization of dodecyl vinyl ether (DVE) yielding ABA type block copolymer. The block copolymer was then used as the surfactant for the emulsion polymerization of vinyl acetate and styrene in the presence of potassium persulfate as an initiator. The effects of new polymeric emulsifier on the physicochemical properties of obtained latexes were investigated depending on surfactant percentage in homopolymerizations.

关键词： Cationic Polymerization Emulsion Polymerization Poly(Ethylene Glycol) Surfactants

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Emulsion Polymerization of Vinyl Acetate in the Presence of a New Cationic Surfactant

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American Journal of Analytical Chemistry 2014年第1期5卷 17-21页

作者： Ayfer Sarac bahire filiz senkal Murat Yıldırım Department of Chemistry Yildız Technical UniversityIstanbulTurkey Department of Chemistry Istanbul Technical UniversityIstanbulTurkey

In this study, the emulsion homopolymerization system containing vinyl acetate, potassium persulfate, a new cationic polymeric surfactant and water was studied by the applying semi-continuous emulsion polymerization process. The effects of new polymeric emulsifier on the physicochemical properties of obtained vinyl acetate latexes were investigated depending on vinyl acetate percentage in the polymerization recipe, and two thermal initiators in homopolymerization.

关键词： Emulsion Polymerization Lattices Cationic Surfactants Critic Micelle Concentration Viscosity

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Solid Phase Extraction and Determination of Nickel in Water Samples by Using Novel Thiol-Containing Sulfonamide Polymeric Resin and Atomic Absorption Spectrophotometer

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光谱学与光谱分析 2011年第8期31卷 2243-2248页

作者： Nagihan M Karaaslan B filiz senkal Cigdem Er Halim Avci Mehmet Yaman Firat University Science Fac.Dep.of Chemistry90-23119Elazig-Turkey Istanbul Technical University Science and Arts Fac.Dep.of ChemistryIstanbul-Turkey Kilis University Science and Arts Fac.Dep.of ChemistryKilis-Turkey

Interest in preconcentration techniques for the determination of metals at ultratrace levels still continues increasingly because of some disadvantages of flameless atomic absorption spectrometry as well as the high costs of other sensitive methods in compared to flame atomic absorption *** this study,thiol-containing sulfonamide resin was synthesized,characterized and applied as a new sorption material for solid phase extraction of nickel in drinking water *** preconcentration procedure,flame atomic absorption spectrometry was used for *** parameters were found to be pH=3.2,contact time=20 min and eluate volume=3 *** limit of detection was found to be 0.75 ng·*** synthesized resin exhibits the superiority in compared to the other adsorption reagents because of the fact that there is no necessity of any complexing reagent,high sorption capacity as well as the relatively fast extraction *** Ni concentrations in the studied 21 kind of water samples were found to be in the range of BDL-4.0 ng·mL-1.

关键词： Spectroscopy Extraction Nickel Preconcentration Atomic absorption

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