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<sup>13</sup>C-NMR Data from Coumarins from Moraceae Family

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American Journal of Analytical Chemistry 2015年第11期6卷 851-866页

作者： Raphael F. Luz Ivo J. C. vieira Raimundo Braz-filho Vinicius F. Moreira Sector of Natural Products Chemistry Universidade Estadual do Norte Fluminense Darcy Ribeiro Campos dos Goytacazes Brazil Sector of Chemistry Instituto Federal Fluminense Campos dos Goytacazes Brazil

Species from Moraceae family stand out in popular medicine and phytotherapy, have been for example used as expectorants, bronchodilators, anthelmintics and treatment of skin diseases, such as vitiligo, due to the presence of compounds with proven biological activity, as the coumarins. Coumarins are lactones with 1,2-benzopyrone basic structure, and are widely distributed in the plant kingdom, both in free form, and in glycosylated form. This work reports a literature review, describing the data of 13C NMR from 53 coumarins isolated from the family Moraceae, and data comparison between genera who presented photochemical studies, in order to contribute to the chemotaxonomy of this family.

关键词： Moraceae Coumarin Furocoumarin Pyranocoumarin NMR Spectral Data

Preparation of Bi_(4)Ti_(3)O_(12)(BIT)Ceramics via a High-Energy Ball Milling Process Doped with Multi-Walled Carbon Nanotubes(MWNTs)

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Materials Sciences and Applications 2013年第9期4卷 549-555页

作者： Alexandre Goncalves Pinheiro Gilberto Dantas Saraiva Josué Mendes filho antonio Sergio Bezerra Sombra Faculdade de Educacao Ciencias e Letras do Sertao Central Universidade Estadual do CearáQuixadáBrazil Departamento de Fisica Universidade Federal do CearáFortalezaBrazil

We prepared the Nano-sized bismuth titanate Bi4Ti3O12 (BIT) powders, through a high-energy ball milling process from their oxides Bi2O3 and TiO2. This BIT phase can be formed after a milling process for 40 min. With an increasing milling time, this particle size of mixture is gradually reduced, thus, we have mostly an amorphous phase. The BIT ceramics were duly obtained by sintering the synthesized powders at temperatures ranging from 850°C to 1000°C. The BIT ceramics sintered at 1020°C for 1 h, exhibiting a density with 7.52 g/cm3 of a crystaline phase and a dielectric of K = 288.11 (100 Hz), as well as a dielectric loss of 0.05 (100 kHz). The High-energy ball milling process is a promising way to prepare BIT ceramics. After the preparation of the BIT, we doped it with the Multi-Walled Carbon Nanotubes which are properly obtained by a chemical vapour deposition (CVD), using nickel as a catalyst, as well as using acetilene at 720°C, and then proceeded with the dielectric and optical measurements.

关键词： Bi_(4)Ti_(3)O_(12) Ceramics Ferroelectric High-Energy Ball Milling Sintering Carbon Nanotubes MWNT

Sagittal abdominal diameter as a marker of visceral obesity in older primary care patients

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Journal of Geriatric Cardiology 2020年第5期17卷 279-283页

作者： Maria Auxiliadora Nogueira Saad antonio José Lagoeiro Jorge Diane Xavier deávila Wolney de Andrade Martins Márcia Maria Sales dos Santos Luciana Thurler Tedeschi Ismar Lima Cavalcanti Maria Luiza Garcia Rosa Rubens Antunes da Cruz filho Fluminense Federal University NiteróiRio de Janeiro StateBrazil

Background Longevity,combined with a higher prevalence of obesity,particularly visceral obesity,has been associated with an increased risk of cardiovascular *** resistance(IR)is an important link between visceral obesity and cardiovascular *** important association has been found between sagittal abdominal diameter,visceral obesity and *** objective of this study is to evaluate sagittal abdominal diameter as a marker of visceral obesity and correlate it with IR in older primary health care *** A cross-sectional study was performed with 389 patients over 60 years of age(70.6±6.9),of whom 74%were *** clinical,anthropometric and metabolic profiles were assessed and their fasting serum insulin level was used to calculate the homeostasis model assessment insulin resistance(HOMA-IR).Sagittal abdominal diameter was measured in the supine position at the midpoint between the iliac crest and the last rib with abdominal *** Sagittal abdominal diameter was significantly correlated with anthropometric measures of general and visceral obesity and with HOMA-IR in both *** was no change in the association between sagittal abdominal diameter and HOMA-IR after adjusting for age,sex,diabetes and *** It is feasible to use sagittal abdominal diameter in older primary care patients as a tool to evaluate visceral obesity,which is an indicator of cardiovascular risk.

关键词： Cardiovascular risk Insulin resistance Primary health care Sagittal abdominal diameter

Preparation of High Purity Neodymium Oxide from Brazilian Monazite by Ion Exchange

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Journal of Energy and Power Engineering 2015年第7期9卷 616-621页

作者： Carlos Alberto da Silva Queiroz Jose antonio Seneda Walter dos Reis Pedreira filho IPEN/CNEN-SP (Instituto de Pesquisas Energeticas e Nucleares/Comissao Nacional de Eneergia Nuclear-Sao Paulo) Cidade Universitaria Sao Paulo 05508-000. Brazil Fundacao Jorge Duprat Figueiredo de Seguranca e Medicina do Trabalho-FUNDACENTRO Sao Paulo 05409-002 Brazil

A simple and economical chemical process for obtaining high purity neodymium oxide is discussed. The raw material in the form of RE （rare earth） carbonates is produced industrially in Brazil from monazite. Using this concentrate as the feed material, ion exchange with a strong cationic resin, commonly used for water treatment, and without the use of retention ions was used for the fractionating of the REE （rare earth elements）. The eluent was ammonium salt of EDTA （ethylenediaminetetraacetic acid） at pH 4.0. The complex of EDTA-neodymium was transformed into neodymium oxides via oxalate precipitation. We produced 99.9% pure Nd203 in yields greater than or equal to 80%. Molecular absorption spectrophotometry was used to monitor the neodymium content during the process and sector field inductively coupled plasma mass spectrometry was used to certify the purity of the neodymium oxides. The typical neodymium oxides obtained contained the followings contaminants in micrograms per gram： Sc （4.09）; Y （0.39）; La （0.78）; Ce （5.62）; Pr （4.56）; Sm （11.10）; Eu （1.10）; Gd （14.30）; Tb （29.3）; Dy （4.15）; Ho （8.39）; Er （13.80）; Tm （0.23）; Yb （2.29）; Lu （0.39）. High purity neodymium oxides obtained from this procedure replaced the imported product used in research and development work on rare earth at IPEN/CNEN-SP （Instituto de Pesquisas Energeticas e Nucleares/Comissfio Nacional de Eneergia Nuclear-Sao Paulo）.

关键词： Neodymium oxide elemental rare earths separation rare earths.

Puerto Madero and Porto Maravilha： The Transformation Process of Port Areas into Tourist Zones

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Journal of Civil Engineering and Architecture 2017年第10期11卷 915-920页

作者： antonio Colchete filho Frederico Braida Lucia Maria Sa Antunes Costa Juliana Varejao Giese Graduate Program in Built Environment Federal University of Ju& de Fora Ju& de Fora 36036-900 Brazil Graduate Program in Urbanism Federal University of Rio de Janeiro Rio de Janeiro 21941-901 Brazil

Transformations in the use of urban space in contemporary cities have common features and projects in the global era take similar themes, such as requalifications of port areas and waterfronts. The main objective of this paper is to revisit the process of urban transformation and valorization of the port areas of Buenos Aires, Argentina, and Rio de Janeiro, Brazil, completed in 1990 and 2015, respectively. It recapitulates their historical processes from decay to recovery as tourist zones, following the implementation of the ＂Strategic Plan of Antiguo Puerto Madero＂, from 1990, in Buenos Aires, and of ＂Urban Operation Porto Maravilha＂, from 2009, in Rio de Janeiro. While planning and strategies differ as they sought distinct locations in different times, they were similar in attracting massive investment from the real estate market. Therefore, consequences of the projects for the cities and the local population are a more important issue than formal results achieved.

关键词： Urban design waterfront renewal Puerto Madero Buenos Aires Porto Maravilha Rio de Janeiro.

2-D DOA Estimation in a Cuboid Array Based on Metaheuristic Algorithms and Maximum Likelihood

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International Journal of Communications, Network and System Sciences 2020年第8期13卷 121-137页

作者： Gilberto Lopes filho Ana Cláudia Barbosa Rezende Lucas Fiorini Cruz Flávio Henrique Teles vieira Rodrigo Pinto Lemos Universidade Federal de Goiás (UFG) Goiánia Brazil

This paper proposes to apply the genetic algorithm and the firefly algorithm to enhance the estimation of the direction of arrival (DOA) angle of electromagnetic signals of a smart antenna array. This estimation is essential for beamforming, where the antenna array radiating pattern is steered to provide faster and reliable data transmission with increased coverage. This work proposes using metaheuristics to improve a maximum likelihood DOA estimator for an antenna array arranged in a uniform cuboidal geometry. The DOA estimation performance of the proposed algorithm was compared to that of MUSIC on different two dimensions scenarios. The metaheuristic algorithms present better performance than the well-known MUSIC algorithm.

关键词： Metaheuristic Algorithms Genetic Algorithm Firefly Algorithm DOA Estimation Maximum Likelihood

Alternative Control of Alternaria Brown Spot in Tangerine

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Agricultural Sciences 2020年第12期11卷 1217-1231页

作者： antonio Manoel Da Silva filho Élida Barbosa Corrêa Alisson Queiroz Moura Juan Manuel Anda Rocabado Phytopathology Laboratory of the State University from Paraiba (UEPB) Lagoa Seca Brazil Department of Agricultural Engineering Federal University of Campina Grande (DEAG/UFCG) Campina Grande Brazil Center University Araras Dr. Edmundo Ulson Araras Brazil Laboratory of Electronic Microscopy Federal University of the Rec&#244 ncavo of Bahia (UFRB) Cruz das Almas Brazil

Alternaria brown spot is considered the main disease of tangerines in the State of Paraiba. The objective of work was to evaluate vegetal tinctures from bitter melon (Momordica charantia) and guava (Psidium guajava) leaves, as an alternative control for Alternaria brown spot in tangerine. The effects of vegetal tinctures were tested in leaves and fruits (detached) of tangerine “Dancy” inoculated with tangerine pathotype of Alternaria alternata. The effect of tinctures on mycelium growth and spore germination of the pathogen was tested. Tinctures at 20% concentration promoted reduction of disease severity. A reduction of 80% in the diameter of leaf lesions was observed for bitter melon tinctures and 75.3% for guava tinctures. In fruits, the reduction was 48.4% (bitter melon tinctures) and 43.3% (guava tinctures). Guava tinctures, starting at a concentration of 5%, inhibited 100% of mycelium growth of tangerine pathotype of A. alternata, while the use of bitter melon tinctures inhibited 100% of mycelium growth starting at a concentration of 10%. The greater sensitivity to tinctures observed when these were added to the culture medium when compared to inoculation in leaves and fruits may be explained due to the higher exposition of the pathogen to the active principle when the vegetal tinctures were added to the culture medium, than when tinctures were sprayed over the vegetal surface in fruits and leaves. The number of germinated spores decreases 76.7% and 82% when using tinctures from guava and bitter melon (20%). Tinctures from bitter melon and guava are potential tools for alternative management of the Alternaria brown spot in tangerine “Dancy”.

关键词： Alternaria alternata f. sp. citri Momordica charantia Psidium guajava Vegetal Extracts Vegetal Tinctures

Numerical Simulation of the Shell-and-Tube Heat Exchanger:Influence of the Lower Flows and the Baffles on a Fluid Dynamics

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Advances in Chemical Engineering and Science 2017年第4期7卷 349-361页

作者： Sebastiao Josédos Santos filho Josedite Saraiva de Souza antonio Gilson Barbosa de Lima Departament of Mechanical Engineering UNINASSAUCampina GrandeBrazil Departament of Mechanical Engineering Federal University of Campina GrandeCampina GrandeBrazil

This project proposes the numerical reproduction development of the water flow in a shell-and-tube heat exchanger 2:1 according to the CLASS C TEMA standard (for moderate operation conditions, with commercial application). With baffles in aluminum and copper tube for the cold fluid flow, the shell is in acrylic, and with thermal analysis efficiencies with regard to the presence or not of the baffles, that is to analyze the efficiency with only, the tubes and the shell and soon after the analysis with tubes and baffles. Heat exchangers are widely used equipment on an industrial and commercial scale, the application of these equipments on an industrial scale represents innovative processing solutions reflecting the processes efficiency, producing significant savings and lower cost, supporting the business success, and consequently offering opportunities, social responsibility, which are the pillars of sustainability. For the development of this work the methodology was used to calculate effectiveness, following the design parameters and contour conditions, it was analyzed the fluids behavior in the shell and the tube, through computational fluid dynamics (CFD) using the software ANSYS CFX 15.0. The results were compared with Excel generated worksheets calculated using the existing equations and correlations.

关键词： Heat Exchanger CFD Baffles ANSYS CFX

Historical Evolution of the Trophic and Limnological Relationships in the Itaipu Reservoir:Top-Down and Bottom-Up Effects upon Fish Production

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Advances in Bioscience and Biotechnology 2015年第6期6卷 390-407页

作者： Rinaldo antonio Ribeiro filho Miguel Petrere Junior Angelo antonio Agostinho Simone Friderigi Benassi Julia Myriam de Almeida Pereira Edson Kiyoshi Okada Curso de Engenharia de Pesca Universidade Estadual Paulista(Unesp)RegistroBrazil Programa de Pos Graduacao em Diversidade Bilogica e Conservacao Universidade Federal de Sao Carlos(UFSCar)SorocabaBrazil Programa de Pos Graduacao em Sustentabilidade em Ecossistemas Marinhos e Costeiros UNISANTASantosBrazil Departamento de Biologia Nucleo de Pesquisas em LimnologiaIctiologia e AquiculturaUniversidade Estadual de MaringaParanaBrazil Divisao de Reservatorio(MARR.CD) Itaipu BinacionalFoz do IguaçuBrazil

Many experimental studies have contributed to the development of the theory of trophic chains in lacustrine habitats. They have revealed the important role played by fish, a subject that has been mostly ignored by limnological studies for the past few decades. Most of these studies were developed in Europe and in the United States. The general applicability of this theory has not yet been tested in subtropical and tropical habitats. In spite of controversies, the bottom-up: top-down trophic cascade hypotheses are the most adopted conceptual models. In this context, we examined if these hypotheses may be corroborated by data from the subtropical Itaipu Reservoir. A negative effect was verified between water transparency and total suspended solids. The detritivorous fish exerted a controlling effect on chlorophyll-a concentrations. Bottom-up effects were detected in four trophic levels, and top-down was detected in just one trophic level. The limnological variates influenced the chlorophyll-a concentration, which indicated that the lnTKN plus the effect of the quarter and the reservoir zone (and their interaction) were important.

关键词： Reservoir Trophic Cascade Top-Down Bottom-Up Limnology Biotic Community