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Apatite phosphate doped by cobalt as hight efficient catalyst of multi-component synthesis of therapeutic spiropyrimidine compound

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Natural Products and Bioprospecting 2022年第1期12卷 567-572页

作者： abdallah rhihil Youness Aichi Mohamed Zahouily Saïd Sebti Mohamed El Guendouzi Laboratory of Chemistry Physics Materials and Catalysis(LCPMC) Faculty of Sciences Ben M’sik of CasablancaHassan II University of CasablancaCasablancaMorocco Financial Engineering Governance and Development LaboratoryNational School of Business and Management of CasablancaHassan II University of CasablancaCasablancaMorocco Laboratory of Materials Catalysis and Valorization of Natural ResourcesFaculty of Sciences and Technology of MohammediaHassan II University of CasablancaCasablancaMorocco

Spiropyrimidines vanquish a significant situation in the field of heterocyclic chemistry, they are broadly utilized as an antibacterial, an inhibitor of multidrug opposition, or an antiplatelet and antithrombotic drug. Phosphate, the principal Moroccan mineral wealth occupies a vital spot in the economic sector and its valuation is a goal continually looked for. Among the conceivable outcomes of valorization, its utilization in heterogeneous catalysis which thought about an exceptionally encouraging new way. In this context, the focus on the reaction of the synthesis of spiropy-rimidine, catalyzed by natural phosphate (NP) and by fluoroapatite (Fap), are used alone or doped by cobalt. These phosphate catalysts were characterized by XRD, IR and SEM, while the synthesized spiropyrimidine was identified by IR, GC-MS and NMR. The obtained yield with fluorapatite doped by cobalt (Co/Fap), at room temperature in ethanol is very high and shows a high impact performance induced by a synergistic effect compared to that of NP alone.

关键词： Spiropyrimidine Natural phosphate Co/Fap Heterogeneous catalysis Multicomponent reaction

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