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Spectrofluorimetric and Spectrophotometric Stability- Iwndicating Methods for the Analysis of Veralipride in Presence of Its Degradants and in Spiked Human Plasma

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Chinese Journal of Chemistry 2012年第1期30卷 183-189页

作者： Salama,Nahla Nour el Din Ahmed Salem,Maissa Yacoub abd el halim,lobna mohammed abdel Fattah,Laila EI-Sayed National Organization for Drug Control and Research(NODCAR) 6 Abu Hazem StreetPyramids AveP.O.Box 29GizaEgypt Analytical Chemistry Department Faculty of PharmacyCairo UniversityCairoEgypt Analytical Chemistry Department Faculty of PharmacyMisr University for Science and Technology6th of OctoberEgypt

Spectrofluorimetric and spectrophotometric stability-indicating methods were developed and validated for analysis of veralipride （Ver） in presence of its hydrolytic and oxidative degradants. The spectrofluorimetric method was based on direct measurement of the intrinsic fluorescence of Ver at 366 nm after excitation at 299 nm using sodium lauryl sulfate （SLS） as micelle enhancer. The fluorescence intensity plot was linear over the concentration range 1.0-10.0 ***-1. The high sensitivity of the method allowed its successful application to the analysis of Ver in spiked human plasma. Two other methods were developed. They are based on the oxidative coupling reac- tion of Vet with 3-methyl benzothiazolin-2-one hydrazone （MBTH） hydrochloride in presence of ceric ammonium sulphate in an acidic medium. The first method depends on spectrophotometric measurement of the stable green colored oxidative coupling product at 660 nm. The different experimental parameters affecting the reaction were optimized. Linearity range is 10.0--100.0 ~tgomL-1. The second method depends on a fluorescence quenching effect of Vet on the fluorescence of Ce3＋. The difference in fluorescence intensity was measured at 380 nm after excitation at 300 nm. This method is applicable over the concentration ranges 0.25-2.50 pg-mL-1. The methods were validated according to the ICH guidelines. They were successfully applied for the analysis of Ver in drug substance, drug product and in laboratory prepared mixtures containing different percentages of hydrolytic and oxidative degradants.

关键词： veralipride micelle-enhanced fluorescence MBTH validation stability fluorescence quenching Ce3+

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Solid Waste Management:A MADM Approach Using Fuzzy Parameterized Possibility Single-Valued Neutrosophic Hypersoft Expert Settings

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Computer Modeling in Engineering & Sciences 2025年第1期142卷 531-553页

作者： Tmader Alballa Muhammad Ihsan Atiqe Ur Rahman Noorah Ayed Alsorayea Hamiden abd el-Wahed Khalifa Department of Mathematics College of SciencesPrincess Nourah bint Abdulrahman UniversityRiyadh11671Saudi Arabia 2 Department of Mathematics University of Management and TechnologyLahore54000Pakistan Department of Mathematics College of ScienceQassim UniversityBuraydah51452Saudi Arabia

The dramatic rise in the number of people living in cities has made many environmental and social problems *** search for a productive method for disposing of solid waste is the most notable of these *** scholars have referred to it as a fuzzy multi-attribute or multi-criteria decision-making problem using various fuzzy set-like approaches because of the inclusion of criteria and anticipated *** goal of the current study is to use an innovative methodology to address the expected uncertainties in the problem of solid waste site *** characteristics(or sub-attributes)that decision-makers select and the degree of approximation they accept for various options can both be indicators of these *** tackle these problems,a novel mathematical structure known as the fuzzy parameterized possibility single valued neutrosophic hypersoft expert set(ρˆ-set),which is initially described,is integrated with a modified version of Sanchez’s *** this,an intelligent algorithm is *** steps of the suggested algorithm are explained with an example that explains *** compatibility of solid waste management sites and systems is discussed,and rankings are established along with detailed justifications for their *** study’s strengths lie in its application of fuzzy parameterization and possibility grading to effectively handle the uncertainties embodied in the parameters’nature and alternative approximations,*** uses specific mathematical formulations to compute the fuzzy parameterized degrees and possibility grades that are missing from the prior *** is simpler for the decisionmakers to look at each option separately because the decision is *** the computed results,it is discovered that they are consistent and dependable because of their preferred properties.

关键词： Hypersoft expert set Sanchez’s method decision making optimization solid waste management possibility grade fuzzy parameterization

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Lanthanide amino acid Schiff base complexes:synthesis,spectroscopic characterization,physical properties and in vitro antimicrobial studies

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Journal of Rare Earths 2013年第7期31卷 715-721页

作者： Samir Alghool M.Sh.Zoromba Hanan F.abd el-halim Department of Chemistry Faculty of SciencePort Said UniversityPort Said 42521Egypt Department of Chemistry Faculty of PharmacyMisr International UniversityIsmailia RoadKm 28 CairoEgypt

Complexes of La （III）, Nd（III）, Gd（III）, Sm（III）, and Ce（IV） were synthesized with Schiff base [（3,5-di-tert-butyl-2-hy- droxybenzyl） amino] acetic acid （H3L）. The ligand and its complexes were synthesized and characterized based on the following analysis： elemental analyses, FAB-mass, molar conductance measurements, magnetic measurement, UV-visible, IR, and NMR spectral studies. The spectral data revealed that the ligand acted as a neutral tridentate coordinating to metal ion through ONO donor sequence. Thermal degradation studies of the ligand and its complexes showed that the previous lanthanide complexes were more thermally stable than the ligand itself. The Schiff base and its complexes were screened for their antibacterial （Escherichia coli, Staphylococcus aureus） and antifungal （Aspergillus flavus and Candida Albicans）.

关键词： lanthanide Schiffbase complexes physical properties biological activity rare earths

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Effect of different metal sulfate precursors on structural and catalytic performance of zirconia in dehydration of methanol to dimethyl ether

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燃料化学学报 2018年第1期46卷 67-74页

作者： abd el-Aziz A.Said Mohamed abd el-Aal Chemistry Department Faculty of ScienceAssiut University71516 AssiutEgypt

ZrO_2 was treated with 10% SO_4^(2-) from different metal sulfate precursors for methanol dehydration to dimethyl *** the samples exhibited tetragonal phase and no diffraction peaks corresponding to metal sulfates or metal oxides were *** FT-IR results revealed that there were different interactions between sulfate and ZrO_2,and this had a great effect on the surface area of the *** catalytic activity was measured over the catalysts in the temperature range of 100-300 ℃.The results revealed that sulfated zirconia with CuSO_4·5 H_2O and Al_2(SO_4)_3·16 H_2O showed the best catalytic *** maximum yield of DME ≈87% was obtained over CuSZ at a reaction temperature of 275 ℃.Moreover,the catalytic activity of the catalysts was correlated well with their surface acidity that measured by dehydration of isopropanol.

关键词： MSO 4/ZrO2 甲醇脱水 DME

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Capacity and Fairness Maximization-Based Resource Allocation for Downlink NOMA Networks

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Computers, Materials & Continua 2021年第10期69卷 521-537页

作者： mohammed abd-elnaby Department of Computer Engineering College of Computers and Information TechnologyTaif UniversityTaif21944Saudi Arabia

Non-orthogonal multiple access(NOMA)is one of the leading technologies for 5G *** pairing(UP)and power allocation(PA)are the key controlling mechanisms for the optimization of the performance of NOMA *** paper presents a novel UP and PA(UPPA)technique for capacity and fairness maximization in NOMA called(CFM-UPPA).The impact of the power allocation coefficient and the ratio between the channel gains of the paired users on the sum-rate capacity and the fairness in NOMA is firstly ***,based on this investigation,the PA and UP algorithms of the CFM-UPPA technique are *** power allocation coefficient of the proposed PA is formulated as an exponentially decaying function of the ratio between the channel gains of the paired users to maximize the capacity and the fairness,and its maximum value is adjusted to guarantee the successive interference cancellation(SIC)*** proposed UP is based on selecting the user that has the highest channel gain per subcarrier as the strong user to maximize the capacity and selecting the user that has the closest lower channel gain to the strong user’s channel gain as the weak user to improve the fairness and *** performance evaluation of the proposed CFM-UPPA technique in terms of capacity,fairness,and outage probability demonstrates that its performance significantly outperforms that of the orthogonal multiple access(OMA)system and that of the NOMA system with random ***,the simulation results demonstrate the efficiency of the proposed PA in improving the performance of other UP algorithms,such as the random UP algorithm.

关键词： 5G non-orthogonal multiple access user pairing power allocation capacity fairness

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Sum Rate Maximization-based Fair Power Allocation in Downlink NOMA Networks

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Computers, Materials & Continua 2022年第6期71卷 5099-5116页

作者： mohammed abd-elnaby Department of Computer Engineering College of Computers and Information TechnologyTaif UniversityTaif21944Saudi Arabia

Non-orthogonal multiple access(NOMA)has been seen as a promising technology for 5G *** performance optimization of NOMA systems depends on both power allocation(PA)and user pairing(UP).Most existing researches provide sub-optimal solutions with high computational complexity for PA problem and mainly focuses onmaximizing the sum rate(capacity)without considering the fairness ***,the joint optimization of PA and UP needs an exhaustive *** main contribution of this paper is the proposing of a novel capacity maximizationbased fair power allocation(CMFPA)with low-complexity in downlink *** investigation and analysis of the joint impact of signal to noise ratio(SNR)per subcarrier and the channel gains of the paired users on the performance of NOMA in terms of the capacity and the user fairness is ***,a closed-form equation for the power allocation coefficient of CMFPA as a function of SNR,and the channel gains of the paired users is *** addition,to jointly optimizeUP and PAinNOMA systems an efficient low-complexity UP(elCUP)method is proposed to be incorporated with the proposed CMFPA to compromise the proposed joint resource allocation(JRA).Simulation results demonstrate that the proposed CMFPA can improve the capacity and fairness performance of existing UP methods,such as conventional UP,and random UP ***,the simulation results show that the proposed JRA significantly outperforms the existing schemes and gives a near-optimal performance.

关键词： 5G NOMA UP PA capacity fairness

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Flexural Behavior of Cross-Connected Brick Masonry Infill Wall Panels Supported on Reinforced Concrete Beam Grids

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Journal of Shanghai Jiaotong university(Science) 2024年第5期29卷 889-899页

作者： BAYOUMI el-Said abd-Allah MAHMOUD Mahmoud Hassan ARIF mohammed Department of Civil Engineering College of EngineeringQassim UniversityBuraidah51452Saudi Arabia Engineering Expert at Ministry of Justice Cairo11516Egypt Department of Civil Engineering Faculty of EngineeringAl-Azhar UniversityCairo11651Egypt Department of Civil Engineering Aligarh Muslim UniversityAligarh202002India

This paper presents an experimental investigation on the flexural behavior of cross-connected brick masonry infill wall panels supported on reinforced concrete beam grids above and below the *** experimental program was comprised of six wall *** effect of change in lower beam stiffness relative to the wall and the geometry of the main walls were *** the results of the experimental tests,the increase in the depth of the lower beam grid reduces the deflection,resulting in an increase in the load carrying capacity of the ***,the stiffness of the main walls affects the deflection and the failure load of the cross walls.

关键词： brick masonry infill walls reinforced concrete beam grid main and cross walls stiffness deflection crack pattern failure load

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Fair subcarrier-power allocation scheme for multiuser multicarrier systems

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Journal of Central South University 2015年第8期22卷 3033-3041页

作者： mohammed abd-elnaby Germien G.Sedhom Nagy W.Messiha Xu Zhu Fathi E.abd el-Samie Faculty of electronic Engineering Menoufia University Deptartment of electrical Engineering and electronics University of Liverpool

The main objective of multiuser orthogonal frequency division multiple access(MU-OFDM) is to maximize the total system capacity in wireless communication systems. Thus, the problem in MU-OFDM system is the adaptive allocation of the resources(subcarriers, bits and power) to different users subject to several restrictions to maximize the total system capacity. In this work, a proposed subcarrier allocation algorithm was presented to assign the subcarriers with highest channel gain to the users. After the subcarrier allocation, subcarrier gain-based power allocation(SGPA) was employed for power and bit loading. The simulation results show that the proposed subcarrier-power allocation scheme can achieve high total system capacity and good fairness in allocating the resources to the users with slightly high computational complexity compared to the existing subcarrier allocation algorithms.

关键词： multiuser orthogonal frequency division multiple access (MU-OFDM) subcarrier-allocation power allocation fairness capacity

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Analysis of BrainMRI: AI-Assisted Healthcare Framework for the Smart Cities

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Intelligent Automation & Soft Computing 2023年第2期35卷 1843-1856页

作者： Walid el-Shafai Randa Ali Ahmed Sedik Taha el-Sayed Taha mohammed abd-elnaby Fathi E.abd el-Samie Department electronics and electrical Communications Engineering Faculty of Electronic EngineeringMenoufia UniversityMenoufia32952Egypt Department of ROBOTICS and Intelligent Machines Faculty of Artificial IntelligenceKafrelsheikh UniversityKafrelsheikhEgypt Department of Computer Engineering College of Computers and Information TechnologyTaif UniversityTaif21944Saudi Arabia

The use of intelligent machines to work and react like humans is vital in emerging smart ***-aided analysis of complex and huge MRI(Mag-netic Resonance Imaging)scans is very important in healthcare *** AI(Artiﬁcial Intelligence)driven healthcare applications,tumor detection is one of the contemporary researchﬁelds that have become attractive to *** are several modalities of imaging performed on the brain for the pur-pose of tumor *** paper offers a deep learning approach for detecting brain tumors from MR(Magnetic Resonance)images based on changes in the division of the training and testing data and the structure of the CNN(Convolu-tional Neural Network)*** proposed approach is carried out on a brain tumor dataset from the National Centre of Image-Guided Therapy,including about 4700 MRI images of ten brain tumor cases with both normal and abnormal *** dataset is divided into test,and train subsets with a ratio of the training set to the validation set of 70:*** main contribution of this paper is introdu-cing an optimum deep learning structure of CNN *** simulation results are obtained for 50 epochs in the training *** simulation results reveal that the optimum CNN architecture consists of four layers.

关键词： Healthcare smart cities clinical automation CNN machine learning brain tumor medical diagnosis

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Cancelable Speaker Identification System Based on Optical-Like Encryption Algorithms

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Computer Systems Science & Engineering 2022年第10期43卷 87-102页

作者： Safaa el-Gazar Walid el-Shafai Ghada el-Banby Hesham F.A.Hamed Gerges M.Salama mohammed abd-elnaby Fathi E.abd el-Samie Department of electrical Engineering Faculty of EngineeringEgyptian-Russian UniversityCairoEgypt Department of electronics and electrical Communications Engineering Faculty of Electronic EngineeringMenoufia UniversityMenouf32952Egypt Security Engineering Laboratory Department of Computer SciencePrince Sultan UniversityRiyadh11586Saudi Arabia Department of Industrial electronics and Control Engineering Faculty of Electronic EngineeringMenoufia UniversityMenouf32952Egypt Department of Computer Engineering College of Computers and Information TechnologyTaif UniversityTaif21944Saudi Arabia Department of Information Technology College of Computer and Information SciencesPrincess Nourah Bint Abdulrahman UniversityRiyadh84428Saudi Arabia

Biometric authentication is a rapidly growing trend that is gaining increasing attention in the last *** achieves safe access to systems using biometrics instead of the traditional *** utilization of a biometric in its original format makes it usable only ***,a cancelable biometric template should be used,so that it can be replaced when it is *** biometrics aims to enhance the security and privacy of biometric *** encryption is an efficient technique to be used in order to generate cancelable biometric *** this paper,a highly-secure encryption algorithm is proposed to ensure secure biometric data in verification *** considered biometric in this paper is the speech *** speech signal is transformed into its ***,the spectrogram is encrypted using two cascaded optical encryption *** first algorithm is the Optical Scanning Holography(OSH)for its efficiency as an encryption *** OSH encrypted spectrogram is encrypted using Double Random Phase Encoding(DRPE)by implementing two Random Phase Masks(RPMs).After the two cascaded optical encryption algorithms,the cancelable template is *** verification is implemented through correlation estimation between enrolled and test templates in their encrypted *** the correlation value is larger than a threshold value,the user is *** threshold value can be determined from the genuine and imposter correlation distribution curves as the midpoint between the two *** implementation of optical encryption is adopted using its software rather than the optical *** efficiency of the proposed cancelable biometric algorithm is illustrated by the simulation *** can improve the biometric data security without deteriorating the recognition *** results give close-to-zero This values for the Equal Error Rate(EER)and close-to-one values for the Area under Receiver Operator Charact

关键词： Cancelable biometrics spectrogram OSH DRPE EER AROC

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