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燃料化学学报 2021年第10期49卷 1421-1434页

作者： ABOUL-eNeIN Ateyya A awadallah ahmed e eL-DeSOUKI Doaa S ABOUL-GHeIT Noha AK Process Development Division Egyptian Petroleum Research InstituteCairo 11727Egypt ePRI-Nanotechnology Center Egyptian Petroleum Research InstituteCairo 11727Egypt

通过催化热解农业废弃物甘蔗渣(SCB),采用两步工艺生产具有显著应用价值的碳纳米管(CNTs)。主要研究沸石催化剂(HZSM-5、HMOR和HY)、热解温度(450−700℃)和SCB/ZSM-5的比例(3−12)对SCB催化热解的影响,确定最佳工艺参数。随后,将第一步... 详细信息

通过催化热解农业废弃物甘蔗渣(SCB),采用两步工艺生产具有显著应用价值的碳纳米管(CNTs)。主要研究沸石催化剂(HZSM-5、HMOR和HY)、热解温度(450−700℃)和SCB/ZSM-5的比例(3−12)对SCB催化热解的影响,确定最佳工艺参数。随后,将第一步产生富含碳的热解产物用于第二步由Co-Mo/MgO催化生长CNTs。通过简单的两步工艺催化热解SCB生产CNTs。SCB的催化热解在半间歇式反应器(外径=4 cm,长度=90 cm)中进行,CNTs的生长在水平反应器(外径=2.5 cm,长度=100 cm)中进行。两个反应器通过玻璃管(直径0.6 cm,长度12 cm)连接并将热解产物从反应器I转移到反应器II。在半间歇式反应器中放入经过预处理的SCB和沸石催化剂,并以20℃/min加热到反应所需温度。随后,将0.5 g Co-Mo/MgO加入到水平反应器中作为CNTs的生长催化剂。在一个典型的实验中,将2 g沸石催化剂、24 g SCB放入半间歇式反应器,研究了不同种类沸石催化剂在500℃温度条件下对SCB热解的影响。接着,使用HZSM-5研究了不同温度(450−700℃)对SCB热解的影响。最后,研究了不同SCB/ZSM-5投料比例(SCB/ZSM-5=3、6、9、12)对SCB热解的影响。此外,水平反应器中的CNTs生长温度恒定为700℃。通过XRD、TPR和TPD进行催化剂表征。XRD谱图证实了催化剂存在MgO和Co_(3)O_(4),以及以小尺寸颗粒形式存在的CoMoO4和MgMoO4。使用XRD数据根据Scherrer方程计算45%Co-5%Mo/MgO催化剂的平均晶粒尺寸为25.8 nm。TPR分析表明,Co-Mo/MgO催化剂是由未反应的Co_(3)O_(4)以及混合氧化物组成。使用XRD数据,计算得到HZSM-5、HMOR和HY的平均晶粒尺寸分别为43、41和51 nm。NH3-TPD分析表明沸石催化剂存在大量的酸性位点。催化热解SCB结果表明,由HY和HZSM-5催化剂在500℃得到的挥发性产品(生物油和气体)的总收率值分别为34.4%和32.8%,而使用HMOR产生的这些挥发性产品的收率值最低(28.8%)。用HZSM-5催化热解SCB获得了最高的炭产量(23.1%)。然而,使用HMOR和HY热解催化剂产生的炭产量值较低,分别为15.8%和9.8%。使用TeM表征通过两步法生产的碳纳米管,并且测量了CNTs的外径。数据显示,用HZSM-5进行SCB热解产生了直径分布范围较宽的CNTs(10−56 nm),而用HMOR和HY热解催化剂则分别获得了直径较窄的CNTs(13−44 nm,12−28 nm)。拉曼光谱分析表明,使用HZSM-5作为SCB热解的催化剂可以生产最优的CNTs。研究了不同热解温度对CNTs产量的影响。结果显示,将热解温度从450℃提高到500℃,炭产率值从6.7%达到最佳值23.1%,接着增加温度至700℃,炭产量下降至16.7%。随后对不同温度下催化热解形成的炭产品进行TeM表征,结果显示,随着温度的升高炭产品中CNTs的比例下降,CNTs的直径范围变窄。拉曼光谱分析结果表明,在500和700℃形成的CNMs具有最少的缺陷。研究了投料比例对炭产品产量的影响,结果表明,SCB/ZSM-5的比例从3提高到12,生物油和气体的总产量从36.4%下降到32.8%,而生物炭的产量分别从63.6%增加到67.2%。根据催化剂的质量计算得到炭产量的最佳值是使用SCB/ZSM-5比例为6。使用TeM表征不同投料比例生产的炭产品,分析表征结果可得SCB/ZSM-5的比例为6,是形成具有良好质量的致密CNTs的最佳选择。并且不同投料比例的拉曼光谱显示,SCB/ZSM-5比例为6可以生产最优的CNTs。沸石类型(HZSM-5、HMOR和HY)、热解温度(450−700℃)和SCB/ZSM-5比例(3−12)影响CNTs和热解产物(气体、生物油和生物炭)的产量。实验结果表明,获得最高CNTs产量的条件为:热解温度为500℃、SCB/ZSM-5比例为6;获得最高生物油和气体总产量(40%)的条件为:热解温度为700℃、SCB/ZSM-5比例为12。TeM分析表明,使用HZSM-5催化剂在热解温度450℃只生成竹节状碳纳米管(BCNTs),而CNTs和碳纳米洋葱(CNO)是在较高温度热解温度(500−700℃)下产生的。使用SCB/ZSM-5的比例为6时,生成CNTs的直径分布范围最大(7−76 nm)。拉曼光谱分析表明,使用SCB/ZSM-5的比例为6时,形成的CNTs最优。该研究显示,在半间歇式反应器中催化热解SCB是生产CNTs的有效技术,通过对工艺和反应器的优化可以达到更好的效果。

关键词：碳纳米管 Co-Mo/MgO 热解甘蔗渣 ZSM-5沸石

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Study of scalar particles through the Klein–Gordon equation under rainbow gravity effects in Bonnor–Melvin-Lambda space-time

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Communications in Theoretical Physics 2024年第4期76卷 113-125页

作者： Faizuddin ahmed Abdelmalek Bouzenada Department of Physics University of Science&Technology MeghalayaRi-Bhoi793101India Laboratory of theoretical and applied Physics Echahid Cheikh Larbi Tebessi UniversityAlgeria

In our investigation,we explore the quantum dynamics of charge-free scalar particles through the Klein–Gordon equation within the framework of rainbow gravity,considering the Bonnor–Melvin-Lambda(BML)space-time *** BML solution is characterized by the magnetic field strength along the axis of the symmetry direction which is related to the cosmological constantΛand the topological parameterαof the *** behavior of charge-free scalar particles described by the Klein–Gordon equation is investigated,utilizing two sets of rainbow functions:(i)f(χ)=■,h(χ)=1 and(ii)f(χ)=1,h(χ)=1+βХ/*** 0e representing the particle's energy,ep is the Planck's energy,andβis the rainbow *** obtain the approximate analytical solutions for the scalar particles and conduct a thorough analysis of the obtained ***,we study the quantum dynamics of quantum oscillator fields within this BML space-time,employing the Klein–Gordon *** also,we choose the same sets of rainbow functions and obtain the approximate eigenvalue solution for the oscillator ***,we demonstrate that the relativistic approximate energy profiles of charge-free scalar particles and oscillator fields get influenced by the topology of the geometry and the cosmological ***,we show that the energy profiles of scalar particles receive modifications from the rainbow parameter and the quantum oscillator fields by both the rainbow parameter and the frequency of oscillation.

关键词： quantum fields in curved space-time relativistic wave equations solutions of wave equations bound-state special functions

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exact and heuristic formulae to compute the geodetic height from the ellipse equation

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Geodesy and Geodynamics 2024年第2期15卷 150-155页

作者： Mohamed eleiche ahmed Hamdi Mansi Construction Department Faculty of EngineeringEgyptian Russian UniversityCairoEgypt Istituto Nazionale di Geofisica e Vulcanologia Sezione di PisaPisaPlItaly

The conversion of the cartesian coordinates of a point to its geodetic equivalent coordinates in reference to the geodetic ellipsoid is one of the main challenges in *** ellipse equation in the meridian plane significantly influences the value of the geodetic *** research analyzes this influence and how it can contribute to their *** study investigates the mathematical relation between them and presents an exact formula relating to the geodetic height and the ellipse *** addition,a heuristic formula for the relation between the geodetic height and the ellipse equation is proposed,which is independent of the geodetic latitude and has a relative accuracy better than 99.9 %.The calculation is stable,and the cost is low.

关键词： ellipse equation Geodetic height Heuristic geodetic height

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engineering nanomedicines for immunogenic eradication of cancer cells:Recent trends and synergistic approaches

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Acta Pharmaceutica Sinica B 2024年第6期14卷 2475-2504页

作者： ahmed O.elzoghby Omar Samir Hagar e.emam ahmed Soliman Riham M.Abdelgalil Yomna M.elmorshedy Kadria A.elkhodairy Mahmoud L.Nasr Division of engineering in Medicine and Division of Renal Medicine Department of MedicineBrigham and Women's HospitalHarvard Medical SchoolBoston 02115MAUSA Cancer Nanotechnology Research Laboratory(CNRL) Faculty of PharmacyAlexandria UniversityAlexandria 21521Egypt

Resistance to cancer immunotherapy is mainly attributed to poor tumor immunogenicity as well as the immunosuppressive tumor microenvironment(TMe)leading to failure of immune *** therapeutic strategies including chemotherapy,radiotherapy,photodynamic,photothermal,magnetic,chemodynamic,sonodynamic and oncolytic therapy,have been developed to induce immunogenic cell death(ICD)of cancer cells and thereby elicit immunogenicity and boost the antitumor immune ***,many challenges hamper the clinical application of ICD inducers resulting in modest immunogenic ***,we outline the current state of using nanomedicines for boosting ICD of cancer ***,synergistic approaches used in combination with ICD inducing nanomedicines for remodeling the TMe via targeting immune checkpoints,phagocytosis,macrophage polarization,tumor hypoxia,autophagy and stromal modulation to enhance immunogenicity of dying cancer cells were *** further highlight the emerging trends of using nanomaterials for triggering amplified ICD-mediated antitumor immune *** reticulum localized ICD,focused ultrasound hyperthermia,cell membrane camouflaged nanomedicines,amplified reactive oxygen species(ROS)generation,metallo-immunotherapy,ion modulators and engineered bacteria are among the most innovative *** challenges,merits and demerits of ICD inducer nanomedicines were also discussed with shedding light on the future role of this technology in improving the outcomes of cancer immunotherapy.

关键词： Immunogenic cell death Immunogenic eradication Nanomedicines Drug delivery Cancer immunotherapy Antitumor immunity T cells Tumor associated antigens Synergistic immune response

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Fuel cell stack design and modelling with a double-stage boost converter coupled to a single-phase inverter

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CLeAN eNeRGY 2024年第1期8卷 188-196页

作者： elnagi, Basem e. Ismaiel, ahmed M. Mansour, Hany S. e. Abd-Alwahab, M. N. Suez Canal Univ Fac Engn Elect Engn Dept Ismailia 41522 Egypt

A comprehensive proton-exchange membrane fuel cell stack model was developed and integrated with a two-stage DC/DC boost converter. It was directly coupled to a single-phase (two levels-four pulses) inverter without a transformer. The pulse-width modulation signal was used to independently regulate every converter phase. The converter was modelled using a MATLAB (R)/Simulink (R) environment and an appropriate voltage control method. The analysis features of the suggested circuit were created and, through established experiments, the simulation results were verified. A single-phase (two levels-four pulses) inverter control circuit was tested and it produced a pure sinusoidal waveform with voltage control. It matches the voltage of the network in terms of amplitude and frequency. A sinusoidal pulse-width modulation approach was performed using a single-phase (two levels-four pulses) pulse-width modulation inverter. The results demonstrated an enhancement in the standard of the output wave and tuned the dead time with a reduction of 63 mu s compared with 180 mu s in conventional techniques. A comprehensive model of a proton-exchange membrane fuel cell stack is integrated with a single-phase (two levels-four pulses) inverter without a transformer. Pulse-width modulation is used to independently regulate every converter phase. As a result, the dead time is reduced compared to conventional techniques. Graphical Abstract

关键词： PeM fuel cell pulse-width modulation single-phase inverter and double-stage DC/DC boost converter PeRFORMANCe SYSTeM

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Phytochemical analysis,antioxidant,acetylcholinesterase,andα-amylase inhibitors from Hippeastrum hybridum extract

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Journal of Traditional Chinese Medicine 2024年第3期44卷 496-504页

作者： Naila Sher Mushtaq ahmed Nadia Mushtaq Department of Biotechnology University of Science and Technology Bannu-KPK 28100Pakistan Department of Botany University of Science and Technology Bannu-KPK 28100Pakistan

OBJeCTIVe:To investigate the effects of Hippeastrum hybridum(HH)as a free radical scavenger,and an inhibitor of the two enzymes i-e Alpha-amylase(α-amylase)and acetylcholinesterase(AChe).MeTHODS:In this study,HH plant was preliminary analyzed for phytochemical screening and then tested for its antioxidant,anti-α-amylase,and anti-AChe efficiency via standard ***:Phytochemical analysis shows the existence of different compounds;while Coumarins and quinones were *** total phenolic,flavonoid,and tannins content were found to be(78.52±0.69)mg GAe/g,(2.01±0.04)mg RUe/g,and(58.12±0.23)mg TAe/g of plant extract respectively.28.02%±0.02%alkaloid and 2.02%±0.05%saponins were present in the HH *** HH extract showed the anti-oxidant property with IC50(50%inhibition)of(151.01±0.13)(HH),(79.01±0.04)(Ascorbic acid)for ferric reducing,(91.48±0.13)(HH),(48.02±0.11)(Ascorbic acid)against Ammonium molybdenum,(156.02±0.31)(HH),(52.38±0.21)(Ascorbic acid)against DPPH,136.01±0.21(HH),52.02±0.31(Ascorbic acid)against H_(2)O_(2),and 154.12±0.03(HH),(40.05±0.15)(Ascorbic acid)μg/mL against ABTS *** analysis indicated that HH caused a competitive type of inhibition ofα-amylase(V_(max)remained constant and Km increases from 10.65 to84.37%)while Glucophage caused the un-competitive type of inhibition i-e both Km and V_(max)decreased from40.49 to 69.15%and 38.86 to 69.61%*** K_(i),(inhibition constant);K_(I),(dissociation constant),K_(m),(Michaelis-Menten constant),and IC50 were found to be62,364,68.1,and 38.08±0.22 for HH and 12,101.05,195,34.01±0.21 for ***,HH causes an anon-competitive type of inhibition of AChe i-e Km remains constant while V_(max)decreases from 60.5%to74.1%.The calculated K_(i),K_(I),K_(m),and IC50 were found to be 32,36.2,0.05,and 18.117±***:From the current results,it is concluded that HH extract contains bioactive compounds,and could be a good alternative to controlling oxidant

关键词： Hippeastrum hybridum phytochemicals antioxidant alpha-amylase acetylcholinesterase

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A review on edge analytics:Issues,challenges,opportunities,promises,future directions,and applications

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Digital Communications and Networks 2024年第3期10卷 783-804页

作者： Sabuzima Nayak Ripon Patgiri Lilapati Waikhom Arif ahmed National Institute of Technology Silchar India ericsson Sweden

edge technology aims to bring cloud resources(specifically,the computation,storage,and network)to the closed proximity of the edge devices,i.e.,smart devices where the data are produced and *** computing and application in edge devices lead to emerging of two new concepts in edge technology:edge computing and edge *** analytics uses some techniques or algorithms to analyse the data generated by the edge *** the emerging of edge analytics,the edge devices have become a complete ***,edge analytics is unable to provide full support to the analytic *** edge devices cannot execute advanced and sophisticated analytic algorithms following various constraints such as limited power supply,small memory size,limited resources,*** article aims to provide a detailed discussion on edge *** key contributions of the paper are as follows-a clear explanation to distinguish between the three concepts of edge technology:edge devices,edge computing,and edge analytics,along with their *** addition,the article discusses the implementation of edge analytics to solve many problems and applications in various areas such as retail,agriculture,industry,and ***,the research papers of the state-of-the-art edge analytics are rigorously reviewed in this article to explore the existing issues,emerging challenges,research opportunities and their directions,and applications.

关键词： edge analytics edge computing edge devices Big data Sensor Artificial intelligence Machine learning Smart technology Healthcare

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Intelligent Fractional-Order Controller for SMeS Systems in Renewable energy-Based Microgrid

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Computer Modeling in engineering & Sciences 2024年第8期140卷 1807-1830页

作者： Aadel M.Alatwi Abualkasim Bakeer Sherif A.Zaid Ibrahem e.Atawi Hani Albalawi ahmed M.Kassem electrical engineering Department Faculty of EngineeringUniversity of TabukTabuk47913Saudi Arabia Industrial Innovation and Robotic Center(IIRC) University of TabukTabuk47731Saudi Arabia Department of electrical engineering Faculty of EngineeringAswan UniversityAswan81542Egypt Renewable energy and environmental Technology Centre University of TabukTabuk47913Saudi Arabia electrical engineering Department Faculty of EngineeringSohag UniversitySohag82524Egypt

An autonomous microgrid that runs on renewable energy sources is presented in this *** has a supercon-ducting magnetic energy storage(SMeS)device,wind energy-producing devices,and an energy storage ***,because such microgrids are nonlinear and the energy they create varies with time,controlling and managing the energy inside them is a difficult ***-order proportional integral(FOPI)controller is recommended for the current research to enhance a standalone microgrid’s energy management and *** suggested dedicated control for the SMeS comprises two loops:the outer loop,which uses the FOPI to regulate the DC-link voltage,and the inner loop,responsible for regulating the SMeS current,is constructed using the intelligent FOPI(iFOPI).The FOPI+iFOPI parameters are best developed using the dandelion optimizer(DO)approach to achieve the optimum *** suggested FOPI+iFOPI controller’s performance is contrasted with a conventional PI controller for variations in wind speed and microgrid *** optimal FOPI+iFOPI controller manages the voltage and frequency of the *** behavior of the microgrid as a reaction to step changes in load and wind speed was measured using the proposed *** simulations were used to evaluate the recommended system’s *** results of the simulations showed that throughout all interruptions,the recommended microgrid provided the load with AC power with a constant amplitude and *** addition,the required load demand was accurately ***,the microgrid functioned incredibly well despite SMeS and varying wind *** obtained under identical conditions were compared with and without the best FOPI+iFOPI *** utilizing the optimal FOPI+iFOPI controller with SMeS,it was found that the microgrid performed better than the microgrid without SMeS.

关键词： Fractional-order proportional integral(FOPI) intelligent controller renewable energy resources superconducting magnetic energy storage optimization

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Kaoline-based catalyst for a high stability desulfurization of sour heavy naphtha in a three-phase oscillatory baffled reactor

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Particuology 2024年第1期84卷 249-260页

作者： Hassan M.Hmood Saba A.Gheni Safaa M.R.ahmed Mudheher M.Ali Hamid Yonis Saleh Mohammed H.Mohammed Awad e.Mohammed Marwan A.Mahomood Hiba R.Mohammed ahmed A.Hassan Adam Harvey North Refineries Company Ministry of OilIraq Chemical engineering Department Tikrit UniversityIraq Ministry of Oil Iraq AL-Hawija Technical Institute Northern Technical UniversityMoselIraq School of engineering Newcastle UniversityUK

To meet the rapidly increasing demand for energy and the dramatic depletion of conventional crude oil,it is imperative to utilize sour *** no coke being produced,oxidative desulfurization(ODS)of naphtha lowers its sulfur content and average molecular *** this article,we outline a method for heavy naphtha non-extractive ODS using a very stable *** technique involves the use of a solid catalyst with oxygen gas as the *** necessitated relatively high mixing intensities;hence a three-phase Oscillatory Baffled Reactor(OBR)was *** catalyst was based on the zeolite ZSM-5,prepared from natural kaolin by a series of delamination and activation steps and impregnated with Fe.A TiO2 nanolayer was applied,using the sol-gel method,to prevent rapid *** reactor performance was evaluated to minimize the sulfur content in the naphtha *** to the protective coating,the sulfur conversion stabilized at 90%.The results of this work establish the use of natural clay-based catalysts in a continuous,three-phase ODS,particularly with regard to proving long-term *** also showed that modest ODS can be achieved using an environmentally friendly oxidant,at mild operating conditions,whilst maintaining stability.

关键词： Natural kaoline Desulfurization Three-phase Oscillatory baffled reactor

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Higgs inflation model with non-minimal coupling in hybrid Palatini approach

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Chinese Physics C 2024年第4期48卷 193-201页

作者： Brahim Asfour Aatifa Bargach ahmed errahmani Taoufik Ouali Laboratory of Physics of Matter and Radiation University of Mohammed firstBP 717OujdaMorocco

In this paper,we propose a hybrid metric Palatini approach in which the Palatini scalar curvature is non minimally coupled to the scalar *** derive einstein’s field equations,i.e.,the equations of motion of the scalar ***,the background and perturbative parameters are obtained by means of Friedmann equations in the slow roll *** analysis of cosmological perturbations allowed us to obtain the main inflationary parameters,e.g.,the scalar spectral index and tensor to scalar ratio *** this perspective,as an application of our analysis,we consider the Higgs field with quartic potential,which plays the inflaton role,and show that predictions of Higgs hybrid inflation are in good agreement with recent observational data[***.641,61(2020)].

关键词： non-minimal coupling hybrid metric Palatini Higgs inflation

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