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Olefin Polymerization Behavior of Titanium(iv) Complexes with Fluorinated and Non-fluorinated Aliphatic Phenoxyimine Ligands

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Chinese Journal of Polymer science 2024年第1期42卷 52-62,I0007页

作者： vladislav A.Tuskaev Kasim F.Magomedov svetlana Ch.Gagieva Dmitry A.Kurmaev Yulia v.Nelyubina evgenii K.Golubev Maria D.evseeva viktor G.vasil'ev Galina G.Nikiforova Mikhail i.Buzin vyacheslav s.Bogdanov Boris M.Bulychev Department of Chemistry M.V.Lomonosov Moscow State UniversityMoscow 119992Russian Federation A.N.Nesmeyanov institute of Organoelement Compounds Russian Academy of SciencesMoscow119991Russian Federation Enikolopov institute of synthetic Polymer Materials Russian Academy of SciencesMoscow 117393Russian Federation

A series of Ti(Ⅳ) dichloride and dialkoxide com plexes with phenoxyimine ligands containing fluorinated and nonfluorinated aliphatic imine fragments have been *** molecular structures of complexes 1 and 4 were established by single-crystal X-ray diffraction *** complexes adopt a distorted octahedral coordination structure around the titanium atom and two oxygen atoms are situated in trans position while two nitrogen atoms and two outgoing ligands(Cl or iPrO) are situated in cis *** of activators(MMAO-12 and combinations Et_nAiCl_(3-n)+Bu_(2)Mg) and outgoing ligand(Cl or iPrO) nature on the catalytic activity and properties of the resulting polymers was *** Ti complexes,despite the nature of the outgoing ligands(Cl or iPrO) in the presence of Al/Mg activators,was found to display a high ethylene polymerization activity in the range 1600-3830 kg_(polymer)·mol_(Ti)^(-1)·h^(-1)·atm^(-1) with a viscosity average molecular weight(M_v) value in the range 1.1×10~6-7.1×10~6 Dalton(Da).The resulting UHMWPE can be processed by a solventless method into high-strength and high-modulus oriented *** rheological characteristics of a polymer melt have been *** absence of a cross-over point did not allow to compare the values of the molecular weight distribution of polymers obtained on fluorinated and non-fluorinated pre-catalysts,however,the estimation of the entanglement density is in good agreement with the mechanical characteristics of oriented film *** activation with methylalumoxane,the activity of the com plexes decreased very significantly;however,a polymer with a molecular weight of about 12 million Da was *** the process of ethylene/octene-1 copolymerization,fluorine-containing precatalysts showed a clear advantage over non-fluorinated analogues both in activity and in comonomer content.

关键词： Fi catalysts Titanium(iv) (Co)polymerization Al/Mg co-catalyst Ultra-high molecular weight polyethylene

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Elucidating elusive quaternary selenide EuCeCuse3:synthesis,crystal structure,properties and theoretical studies

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Journal of Rare Earths 2024年第1期42卷 163-171,I0006页

作者： Maxim v.Grigoriev Anna v.Ruseikina Maxim s.Molokeev vladimir A.Chernyshev aleksandr s.aleksandrovsky Alexander s.Krylov svetlana N.Krylova Nikolai P.shestakov Dmitriy A.velikanov Alexander A.Garmonov Alexey v.Matigorov evgeny A.Ostapchuk Thomas schleid Damir A.safin Laboratory of Theory and Optimization of Chemical and Technological Processes University of TyumenVolodarskogo Str.6625003TyumenRussian Federation Kirensky institute of Physics Federal Research Center KSC SB RASAkademgorodok 50 Bld.38660036KrasnoyarskRussian Federation Department of Physics Far Eastern State Transport UniversitySerysheva Str.47680021KrasnoyarskRussian Federation institute of Natural sciences and Mathematics Ural Federal University Named After the First President of Russia B.N.YeltsinMira Str.19620002EkaterinburgRussian Federation Department of Photonics and Laser Technology Siberian Federal UniversitySvobodnii Ave.79660079KrasnoyarskRussian Federation institute of Physics and Technology University of TyumenVolodarskogo Str.6625003 TyumenRussian Federation institute for inorganic Chemistry University of StuttgartPfaffenwaldring 55D-70569StuttgartGermany scientific and Educational and innovation Center for Chemical and Pharmaceutical Technologies Ural Federal University named after the First President of Russia B.N.YeltsinMira Str.19620002 EkaterinburgRussian Federation University of Tyumen Volodarskogo Str.6625003TyumenRussian Federation

We report on the novel heterometallic quaternary selenide EuCeCuse3,the fabrication of which has been a challenge until this *** structure of the reported selenide was elucidated from the powder X-ray diffraction data,which revealed the formation of EuCeCuse3with excellent yield(96.7%)accompanied with a minor fraction of Cese2(3.3%),and was best solved in orthorhombic space group Pnma with the BaLaCus3structural ***,the crystal structure of the title compound completes the row of the heterometallic quaternary selenides EuRECuse3(RE=La,Pr,Nd,sm,Eu,Gd,Tb,Dy,Ho,Er,Tm,Yb,Lu,Y),of which the cerium-based derivative exclusively belongs to the BaLaCus3structural *** distortion of the Cuse4polyhedron was compared for the whole series of EuRECuse3compounds using theτ4-descriptor for four coordinated ions,which revealed the highest degree of distortion for the Ce3+-containing selenide,followed by the La3+-based ***,the crystallographic and geometrical parameters of the reported selenide were discussed in comparison to the Ce3+-based sulfides srCeCus3and *** initio calculations of the crystal structure,a phonon spectrum and elastic constants for the crystal of EuCeCuse3were also *** types and wavenumbers of fundame ntal modes were determined and the involvement of ions participating in the phonon modes was *** experimental iR spectrum of the reported selenide was interpreted and found to be in agreement with the calculated *** experimental direct band gap of EuCeCuse3was measured to be 1.36 ev that is consistent with the concept of its origin due to interband transitions between orbitals emerging mainly from 4f(valence band)and 5d(conduction band)levels of the Eu2+*** dependence of the Young’s modulus on the direction demonstrates the anisotropy of the elastic properties,while the vickers hardness for EuCeCuse3was calculated to be 5.2 ***,the title compound is paramagnetic above 4 K.

关键词： Quaternary selenide synthesis Crystal structure Ab initio calculations Magnetic measurements spectroscopy

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Enhanced saturation magnetization in La^(3+) doped NiCo ferrites prepared by sol-gel auto-combustion method

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Journal of Rare Earths 2024年第8期42卷 1546-1554,I0005页

作者： Maddileti Jelli vidyasagar Thopudurthy Krishna Reddy C.v. Department of Physics Rayalaseema UniversityKurnoolA.P518007.Iindia Department of Physics Government PolytechnicRayachotiA.P516269India

Lanthanum doped nickel-cobalt nano ferrites with chemical formula Ni_(0.5)Co_(0.5)LaxFe_(2-x)O_(4)(x=0.05,0,10,0.15 and 0,20) were prepared using a simple sol-gel auto combustion *** basic structural properties were determined by X-ray diffraction method and the formation of single phased spinel ferrite was *** crystalline size decreased from 25 to 11 nm and lattice parameter a increases with increase of La *** surface morphology of these ferrites was observed by field-emission scanning electron microscopy(FEsEM) and agglomerated irregular grains are observed with increase of the rare earth element La ***-dispersive X-ray spectroscopy(EDX) result confirms the presence of the required *** Fourier transform infrared spectroscopy(FTiR) spectrum indicates the formation of the spinel ferrite structure with M-O *** direct band measurements from ultraviolet-visible spectroscopy(Uv-vis) spectroscopy indicate that the direct band gap decreases from 1.39 to 1.19 ev for x=0.05 to x=0.15,then increases to 1.28 ev for x=*** room temperature magnetic properties of these ferrites were studied by a vibrating sample magnetometer(vsM).The enhanced saturation magnetization of 49.73 emu/g is observed for x=0.10 and then saturation magnetizations are gradually decreased for x=0.15 and x=*** the remanent magnetization and coercivity also follow the same trend.

关键词： Ferrites sol-gel auto combustion La doping Magnetic properties Rare earths

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Exploring the electromagnetic shielding behavior of lanthanum doped calcium nanoferrites

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Journal of Rare Earths 2024年第11期42卷 2128-2136页

作者： E.Ahilandeswari K.sakthipandi R.Rajesh Kanna G.Rajkumar B.Ganesh Babu s.Arunmetha Aslam Hossain P.sakthivel v.Rajendran M.srinidhi Raghavan Department of Physics SRM TRP Engineering College Department of Electronics and Communication Engineering M. Kumarasamy College of Engineering Department of Physics Easwari Engineering College Department of Mechanical Engineering SRM TRP Engineering College Centre for Advanced Energy studies Department of Electronics and Communication EngineeringKoneru Lakshmaiah Education Foundation smart Materials Research institute Southern Federal University Centre for Materials science Department of PhysicsScience and HumanitiesFaculty of EngineeringKarpagam Academy of Higher Education Centre for Nanotechnology Academy of Maritime Education and Training (Deemed to be University) Department of Chemistry and Centre for Nano-Materials and Displays B.M.S. College of Engineering

The present study focuses on the synthesis and characterization of lanthanum(La3+)-doped calcium nanoferrites(CaLaxFe2-xO4:x=0.025,0.050,0.075 and 0.100) using the sonochemical *** techniques were employed to analyze the effect of La3+infusion,Raman spectroscopy confirms the presence of active A1g,T2gand Egmodes in the CaLaxFe2-xO4nanoferrite,indicating the formation of an active ferrite *** introduction of La3+doping results in a significant increase in the band gap energy,rendering the nanoferrites insulating（3.23-3,57 ev）.At higher frequencies,the impedance studies reveal minimal losses and better AC conductivity,pointing to improved dielectric *** higher frequencies,the Q-factor of La-doped calcium nanoferrites shows lower electromagnetic *** M-H curve exhibits ferromagnetic behavior,with La3+-doped calcium nano ferrites displaying a saturation magnetization ranging from 12.72 to 18.10 emu/*** incorporation of La3+also induces enhanced electrical polarization,leading to notable dielectric loss and increased absorption of electromagnetic ***,these CaLaxFe2-xO4nanoferrites demonstrate potential as effective microwave absorbers across a wide frequency range,with significant shielding absorption observed at 8.8-9.1 GHz.

关键词： Dielectric Magnetism Microwave absorption Nanoferrites Rare earths structural properties

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synthesis,structure and magnetic properties of sm_(1.2)Ho_(0.8)Fe_(17)Hx(X=0;4.4)

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Journal of Rare Earths 2021年第9期39卷 1089-1094页

作者： s.v.veselova M.A.Paukov i.s.Tereshina v.N.verbetsky K.v.Zakharov D.i.Gorbunov A.N.vasiPev Faculty of Physics M.V.Lomonosov Moscow State UniversityMoscow 119991Russia Nuclear Fuel Cycle Department.Centrum vyzkumu Rez Hlavni 130Husinec-Rez 25068.Czech Republic immanuel Kant Baltic Federal University Kaliningrad 236004Russia Faculty of Mathematics and Physics Charles UniversityPrague 12116Czech Republic Hochfeld-Magnetlabor Dresden(HLD-EMFL) Helmholtz-Zentrum Dresden-RossendorfDresden 07328Germany f National Research South Ural State UniversityChelyabinsk 454080Russia

intermetallic compounds based on rare-earth metals and iron are by far the most promising materials for permanent mag *** this work,the multicomponent compound sm_(1.2)Ho_(0.8)Fe_(17)was prepared by in duction *** hydride sm_(1.2)Ho_(0.8)Fe_(17)H_(4.4)with a high hydrogen content was obtained by direct hydrogenation of the intermetallic *** rhombohedral Th2Zn17-type of structure(space group R3^(-)m)is inhere nt to parent compound and hydride as *** effect of hydrogenation on the magneric properties of sm_(1.2)Ho_(0.8)Fe_(17)was *** temperature of the hydride sm_(1.2)Ho_(0.8)-Fe_(17)H_(4.4)is higher than that of parent compound by△Tc=138 *** hydrogen embedded in sm_(1.2)Ho_(0.8)Fe_(17)crystal lattice in creases the saturation magnetization(σs)at T=300 K,but does not significantly affect%at T=4.2 *** ferrimagnetic structure is retained in magnetic fields up to 58 T in the parent compound,while,in the hydride,there is a spin-reorie ntatio n phase transitio n observed at 55 *** is found that the parameter of the in tersublattice exchange interaction decreases significantly in the hydride sm_(1.2)Ho_(0.8)Fe_(17)Hg_(4.4)(and in the nitride sm_(1.2)Ho_(0.8)Fe_(17)N_(2.4))which is associated with boosting of the unit-cell volume and distances between magnetic ions.

关键词： intermetallic compound Hydride Crystal structure Magnetization Magnetic phase transition Exchange interaction

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specificity of electrophysical and gas-sensitive properties of nanocomposite ZnO–TiO_(2) films formed by solid-phase pyrolysis

ChemPhysMater

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ChemPhysMater 2024年第3期3卷 314-319页

作者： victor v.Petrov Maria G.volkova Alexsandra P.ivanishcheva Gleb v.Tolstyak Ekaterina M.Bayanb institute of Nanotechnologies Electronicsand Equipment EngineeringSouthern Federal UniversityTaganrog 347922Russia Faculty of Chemistry Southern Federal UniversityRostov-on-Don 344090Russia

ZnO–TiO_(2) thin films containing 0.5 mol%,1.0 mol%,and 5.0 mol%ZnO were synthesized by oxidative solidphase *** materials contained anatase and rutile phases with particle size of 6–13 nm,as confirmed using X-ray phase analysis and scanning electron *** a certain number of ZnO crystallites appeared in the TiO_(2) film structure in the temperature range of room temperature to 220℃,a two-level response of the film resistance was observed,differing by approximately 10%,as obtained by electrophysical *** two-level response correlates with the formation of two donor energy levels of 0.28 and 0.33 ev in the band structure of the ZnO–TiO_(2) *** donor level with a higher activation energy corresponded to the Ti vacancy(v−Ti),and that with a lower activation energy corresponded to the Zn vacancy(v−Zn).Two levels of gas-sensitive properties were noted for 0.5ZnO–TiO_(2),1ZnO–TiO_(2),and 5ZnO–TiO_(2) under the influence of 50 ppm NO_(2) at 250℃.such two-level responses can be ascribed to the pinning of the Fermi level on ZnO and TiO_(2) *** mechanism of the beak-shaped and two-level responses of sensors based on composite nanomaterials when exposed to various gases was elucidated.

关键词： Thin film ZnO TiO_(2) Nanocomposites Pyrolysis Gas sensors

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silicene on non-metallic substrates： Recent theoretical and experimental advances

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Nano Research 2018年第3期11卷 1169-1182页

作者： Emilio scalise Kostantina iordanidou valeri v. Afanas'ev Andre stesmans Michel Houssa Max-Planck-lnstitut fur Eisenforschung Max-Planck Straβe 1 D-40237 Dusseldorf Germany Department of Physics and Astronomy University of Leuven Celestijnenlaan 200D B-3001 Leuven Belgium

silicene, the silicon counterpart of graphene, has been successfully grown on metallic substrates such as Ag（111）, ZrB2（0001）, and ir（111） surfaces. However, characterization of its electronic structure is hampered by the metallic substrate. in addition, potential applications of silicene in nanoelectronic devices will require its growth on or integration with semiconducting and insulating substrates. We herein present a review of recent theoretical works regarding the interaction of silicene with non-metallic templates, distinguishing between the weak van-der-Waals-like interactions of silicene with, for example, layered metal （di）chalcogenides, and the stronger covalent bonding between silicene and, for example, Zns surfaces. We then present a methodology to effectively compare the stability of diverse silicene structures using thermodynamics and molecular dynamics density functional theory calculations. Recent experimental results on the growth of silicene on Mos2 are also reported and compared to the theoretical predictions.

关键词： silicene non-metallic substrates chalcogenide Mos2 layered compounds

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study of the process e^+e^- →π^+π^-π~0π~0 at energies s～(1/2)<1 Gev

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Chinese Physics C 2010年第6期34卷 680-685页

作者： M.N.Achasov K.i.Beloborodov A.v.Berdyugin A.A.Botov v.B.Golubev T.v.Dimova v.P.Druzhinin L.v.Kardapoltsev A.G.Kharlamov D.P.Kovrizhin i.A.Koop A.A.Korol s.v.Koshuba A.E.Obrazovsky E.v.Pakhtusova D.A.shtol s.i.serednyakov Z.K.silagadze A.N.skrinsky Yu.A.Tikhonov Yu.M.shatunov A.v.vasil'ev Budker institute of Nuclear Physics Russian Academy of Sciences Novosibirsk state University

in an experiment with the spherical Neutral Detector at vEPP-2M collider the cross section of the process e^＋e^- →π^＋π^-π^0π^0 was measured. At energies √s 〈 920 Mev this cross section was measured for the first time. The energy dependence of the cross section is well discribed by the vector dominance model with contributions from p, p＇, p＂ mesons. The decay probability ρ→π^＋π^-π^0π^0 was found to be Bρ = （1.60±0.74±0.18） × 10^-5. The upper limit for the decay ω→π^＋π^-π^0π^0 was improved by two orders of magnitude compared to the previous measurements and is Bω 〈 2 × 10^-4 at 90% confidence level.

关键词： vEPP-2M spherical neutral detector meson decay

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Rare earth-doped mixed Ni-Cu-Zn ferrites as an effective photocatalytic agent for active degradation of Rhodamine B dye

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Journal of Rare Earths 2024年第3期42卷 488-496,I0003页

作者： swapnil A.Jadhav sandeep B.somvanshi sudarshan s.Gawali Kranti Zakde K.M.Jadhav Department of Physics Dr.Babasaheb Ambedkar Marathwada UniversityAurangabad431004MaharashtraIndia school of Materials Engineering Purdue UniversityWest Lafayette 47906USA University Department of Basic and Applied sciences MGM UniversityAurangabad431003MaharashtraIndia

in this study, a series of Gd^(3+)-doped mixed Ni-Cu-Zn ferrites with composition of Zn_(0.5)Ni_(0.3)Cu_(0.2)Fe_(2-x)Gd_(x)O_(4)(x = 0, 0.025, 0.05, 0.075, 0.1) was prepared using self-ignition sol-gel method. The prepared nanoparticles with an average size ranging from 22 to 26 nm show a single-phase cubic structure belonging to the spinel matrix. A rise in the Gd^(3+)concentration leads to an increase in crystallite size and lattice parameter. in Fourier transform infrared spectra, two main absorption bands belonging to the spinel structure are observed. The high-frequency bands(v_(1)) represent the tetrahedral complex, while the lowfrequency bands(v_(2)) signify the octahedral complex. The optical bandgap of the nanoferrites is found within the range of 2.91 to 2.41 ev, depending on their size. The magnetic characteristics of the material,such as saturation magnetization and coercivity are significantly altered with the concentration of Gd^(3+)in the solution. Using Rhodamine B(RhB) as a model organic pollutant, an in-depth investigation of the photocatalytic activity of the compounds was carried out. The present outcomes show that adding an adequate amount of Gd^(3+)significantly enhances the number of hydroxyl radicals produced by the ferrite,in turn, increasing the photocatalytic activity of the material. Mechanism elucidated by scavenger studies reveals that ·OH and holes are the primary reactive radicals responsible for the degradation *** photocatalysts show an insignificant performance loss in five consecutive cycles. Thus, it is concluded that these photocatalysts are highly suitable for the remediation of dye-contaminated wastewater.

关键词： Gd^(3+)substitution spinel ferrite structural properties Magnetic properties Photocatalysis Rare earths

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integrated adsorption and photocatalytic removal of methylene blue dye from aqueous solution by hierarchical Nb_(2)O_(5)@PAN/PvDF/ANO composite nanofibers

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Nano Materials science 2024年第1期6卷 96-105页

作者： Aditya Rianjanu Kurniawan Deny Pratama Marpaung Elisabeth Kartini Arum Melati Rizky Aflaha Yudha Gusti Wibowo i Putu Mahendra Nursidik Yulianto Januar Widakdo Kuwat Triyana Hutomo suryo Wasisto Tarmizi Taher Department of Materials Engineering Institut Teknologi SumateraTerusan RyacuduWay HuiJati AgungLampung Selatan35365Indonesia Center for Green and sustainable Materials Institut Teknologi SumateraTerusan RyacuduWay HuiJati AgungLampung Selatan35365Indonesia Department of Environmental Engineering Institut Teknologi SumateraTerusan RyacuduWay HuiJati AgungLampung Selatan35365Indonesia Department of Physics Faculty of Mathematics and Natural SciencesUniversitas Gadjah MadaSekip Utara PO Box BLS 21Yogyakarta55281Indonesia Department of Mining Engineering Institut Teknologi SumateraTerusan RyacuduWay HuiJati AgungLampung Selatan35365Indonesia Department of Chemistry Institut Teknologi SumateraTerusan RyacuduWay HuiJati AgungLampung Selatan35365Indonesia Research Center for Photonics National Research and Innovation Agency(BRIN)Kawasan Puspitek SerpongTangerang Selatan15314Indonesia Department of Physics Faculty of Mathematics and Natural SciencesUniversitas IndonesiaDepok16424Indonesia PT Nanosense instrument indonesia UmbulharjoYogyakarta55167Indonesia Department of Chemical Engineering Faculty of EngineeringUniversitas Gadjah MadaJl Grafika No.2Yogyakarta55281Indonesia

This work presents the development of hierarchical niobium pentoxide(Nb_(2)O_(5))-based composite nanofiber membranes for integrated adsorption and photocatalytic degradation of methylene blue(MB)pollutants from aqueous *** Nb_(2)O_(5) nanorods were vertically grown using a hydrothermal process on a base electrospun nanofibrous membrane made of polyacrylonitrile/polyvinylidene fluoride/ammonium niobate(v)oxalate hydrate(Nb_(2)O_(5)@PAN/PvDF/ANO).They were characterized using field-emission scanning electron microscopy(FE-sEM),X-ray diffraction(XRD)analysis,and Fourier transform infrared(FTiR)*** composite nanofibers possessed a narrow optical bandgap energy of 3.31 ev and demonstrated an MB degradation efficiency of 96%after 480 min contact *** pseudo-first-order kinetic study was also conducted,in which Nb_(2)O_(5)@PAN/PvDF/ANO nanofibers have kinetic constant values of 1.29×10^(-2) min^(-1) and 0.30×10^(-2) min^(-1) for adsorption and photocatalytic degradation of MB aqueous solutions,*** values are 17.7 and 7.8 times greater than those of PAN/PvDF/ANO nanofibers without Nb_(2)O_(5) *** their outstanding photocatalytic performance,the developed membrane materials exhibit advantageous characteristics in recycling,which subsequently widen their practical use in environmental remediation applications.

关键词： Hierarchical nanostructure Composite nanofiber Niobium pentoxide Dye degradation synergetic adsorption and photocatalysis

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