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Application of backflush and micro-flow techniques to the analysis of C5—C13.hydrocarbons in crude oils and its geochemical significance

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Progress in Natural Science:Materials International 2007年第11期17卷 1382-1387页

作者： Wang Peirong1,2. Zhao Hong2.3. Xu Guanjun1,4. Zhu Cuishan2.3. Xiao Tingrong4. Zhang Min2.3.and Zhang Bin1,4.1. Key Laboratory of Petroleum Geochemistry, china National Petroleum Corporation, beijing 100083. china 2. Geochemistry Department of Yangtze University, Jingzhou 4.4.2., china 3. Key Laboratory of Exploration Technologies for Oil and Gas Resources, Ministry of Education, Yangtze University, Jingzhou 4.4.2., china 4. Petroleum geology Central Laboratory, Research institute of Petroleum Exploration and Development, Petrochina, beijing 100083. china) Key Laboratory of Petroleum Geochemistry China National Petroleum Corporation Beijing 100083 China Geochemistry Department of Yangtze University Jingzhou 434023 China Key Laboratory of Exploration Technologies for Oil and Gas Resources Ministry of Education Yangtze University Jingzhou 434023 China Petroleum geology Central Laboratory Research Institute of Petroleum Exploration and Development PetroChina Beijing 100083 China

An Agilent 6890N GC equipped with both FID and Agilent 5975 MSD analyzer has been employed to analyze C5—C13.hydrocarbon fractions of crude oils. A technical combination of program temperature volatilizer injection, backflush and micro-flow controller afforded a fine separation of C5—C13.compounds on a PONA column with the heavy part of crude oils being cut off before entering the analytical column. Both GC-FID chromatogram and GC-MS mass chromatograms (MID and full scan) could be obtained at the same time. The retension time differences of nC6—nC13.alkanes between GC and TIC were in the range of 0.02.0.58 minutes. Totally 2.6 peaks have been assigned group compositions. Results on 8 typical oil samples from CNPC Key Laboratory Crude Oil Library showed that the characteristics of C6—C13.hydrocarbon group composition could be used in oil-oil correlation studies.

关键词： GC analysis GC/MS analysis backflush micro-flow controller light fraction in crude oil

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Some Recognitions on the Sedimentary-Tectonic Development of the Meso-Cenozoic Basins in Eastern china

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Acta Geologica Sinica(English Edition) 1988年第4期1卷 365-379页

作者： Liu Xun institute of geology, Chinese Academy of {2. {3., {4. CHINESE ACAD GEOL SCI INST GEOLBEIJINGPEOPLES R CHINA

Since Jurassic. intense and repeated tectonic movements have taken place in eastern china, of which theYanshanian movement is the most important. Thereby the development of the basins between the Jurassic andEogene in the studied areas may by divided into two different stages, i.e. the Yanshanian subcycle （J-K;） andthe North china subcycle （K;-E）. The basement and tectonic stress field of the basins played an obvious role in controlling thesedimentary-tectonic development of the basins. and down-faulted basins might form under different stressstates. Besides. the shearing stress also played an important part while the basins were forming in the notedareas.

关键词： Some Recognitions on the Sedimentary-Tectonic Development of the Meso-Cenozoic Basins in Eastern china

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A new method for spatio-temporal prediction of rainfall-induced landslide

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Science china Earth sciences 2006年第4期49卷 421-430页

作者： DING Jixin1,2. YANG Zhifa2. SHANG Yanjun2. ZHOU Shenghua1 & YIN Juntao3.1.{3. Non-ferrous Metals Resource geological Survey, {2. 100012.{3. 2. {4. of geology and Geophysics, Chinese Academy of sciences, Key Laboratory of Engineering Geomechanics, {2. 10002.,{3. 3. School of Geoscience & Environmental Engineering, Central South University, Changsha 4.0083.{3. 1. china Non-ferrous Metals Resource geological Survey Beijing 100012 China 2. institute of geology and Geophysics Chinese Academy of Sciences Key Laboratory of Engineering Geomechanics Beijing 100029 China 3. School of Geoscience & Environmental Engineering Central South University Changsha 410083 China

geological condition and rainfall are two most principal conditions inducing landslides in the Chongqing region. By analyzing the forming conditions of rainfall-induced landslides, a new method for spatio-temporal prediction of rainfall-induced landslide is brought forward on the basis of grading and overlapping geological condition and rainfall factor in this paper. At first, semi-quantitative assessment and grading for the geological condition of a certain area or slope can be carried out with the multi-factor interactive matrix. Then the severity of rainfall in that area is grading according to the maximum daily rainfall and the total rainfall in a rainfall course. Finally, the “landslide probability judgement factor” can be worked out through grading and overlapping “geological condition influenc- ing factor” and “rainfall influencing factor”, by which the landslide can be graded into 4.grades, they are landslide extremely easily happening, landslide easily happening, landslide difficultly happening and landslide hardly ever happening respectively. More accurate spatio-temporal prediction of rain- fall-induced landslides can come true on the ground of detailed geological survey of some dangerous slopes in an area and more precise weather forecast. Finally, the reliability and feasibility of carrying out the spatio-temporal prediction of rainfall-induced landslides with the method of “two factors” grading and overlapping are validated by the example of Jipazi landslide.

关键词： rainfall-induced landslide, geological condition, rainfall, two factors, grading and overlapping, interactive matrix, spatio-temporal prediction.

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Digital image analysis of palaeoenvironmental records and applications

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Chinese Science Bulletin 2002年第23期47卷 1957-1963,2025-2026页

作者： SUN Donghuai1,2. LIU Yu2.& TAN Ming3.. South china Sea {3. of Oceanology, Chinese Academy of {2.. Guangzhou 5103.1, china 2. State Key Laboratory of Loess and Quaternary {4., Earth Environmental {3., Chinese Academy of {2., Xi’an 710075, china 3. {3. of {4. and Geophysics, Chinese Academy of {2., beijing 10002., china South china Sea institute of Oceanology Chinese Academy of Sciences Guangzhou China State Key Laboratory of Loess and Quaternary geology Earth Environmental Institute Chinese Academy of Sciences Xi’an China institute of geology and Geophysics Chinese Academy of Sciences Beijing China

Environmental change signals in geological or biological records are commonly reflected on their reflecting or transmitting images. These environmental signals can be extracted through digital image analysis. The analysis principle involves section line selection, color value reading and calculating environmental proxy index along the section lines, layer identification, auto-chronology and investigation of structure evolution of growth bands. On detailed illustrations of the image technique, this note provides image analyzing procedures of coral, tree-ring and stalagmite records. The environmental implications of the proxy index from image analysis are accordingly given through application demonstration of the image technique.

关键词： digital image environmental records.

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Mesozoic subduction-accretion zone in northeastern South china Sea inferred from geophysical interpretations

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Science china Earth sciences 2006年第5期49卷 471-482页

作者： ZHOU Di1, WANG Wanyin2. WANG Jialin3. PANG Xiong4. CAI Dongsheng5 & SUN Zhen1 1. Key Laboratory of Marginal Sea geology, South{2. Sea institute of Oceanology, Chinese Academy of sciences, Guang- zhou 5103.1,{2. 2. College of geological and Topographical Engineering, Chang’an University, Xi’an 710054.{2. 3. Key Laboratory of Marine geology, Tongji University, Shanghai 2.0092.{2. 4.{2. National Offshore Oil Co. Limited – Shenzhen Branch, Shenzhen 518067,{2. 5.{2. National Offshore Oil Co. Limited – Research Center, beijing 10002.,{2. 1. Key Laboratory of Marginal Sea geology South China Sea Institute of Oceanology Chinese Academy of Sciences Guangzhou 510301 China 2. College of geological and Topographical Engineering Chang’an University Xi’an 710054 China 3. Key Laboratory of Marine geology Tongji University Shanghai 200092 China 4. china National Offshore Oil Co. Limited — Shenzhen Branch Shenzhen 518067 China 5. china National Offshore Oil Co. Limited — Research Center Beijing 100027 China

A segment of Mesozoic subduction-accretion zone was inferred across thenortheastern South china Sea at approximately NE4.0 orientation. Basic evidence includes thefollowing: A belt of peek gross horizontal Bouguer gravity gradient (PGHGBA) is comparable in sizeand intensity to that of the Manila subduction-accretion zone. A belt of high positive magneticanomalies appears to the north and sub-parallel to the PGHGBA, representing the volcanic arcassociated to the subduction zone. The PGHGBA crosses obliquely both Cenozoic structures and presentseafloor topography, indicating a pre-Cenozoic age. The segment is offset left-laterally byNW-running strike-slip faults, in concord with the Mesozoic stress field of South china. Inaddition, the existence of the subduction zone is supported by wide-angle seismic data obtained indifferent years by different institutions. At approximate localities, a north-dipping ramp of Mohosurface is indicated by records of ocean-bottom seismometers, and a strong reflector about 8 kmbeneath the Moho reflector is indicated by both OBS and long-cable seismic records. Theidentification of a segment of Mesozoic subduction zone in NE South china Sea fills nicely the gapof the Great Late Mesozoic Circum SE Asia Subduction-acrretion Zone, which extended from Sumatra,Java, SE Kalimantan to N Palawan, and from Taiwan, Ryukyu to SW Japan.

关键词： Mesozoic, subduction zone, SE Asia, NE South china Sea, geophysics.

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SHRIMP zircon U-Pb age and Nd isotopic study on the Nyainqêntanglha Group in Tibet

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Science china Earth sciences 2005年第9期48卷 1377-1386页

作者： HU Daogong1, WU Zhenhan1, JIANG Wan1, SHI Yuruo2. YE Peisheng1 & LIU Qisheng1 1. institute of Geomechanics, Chinese Academy of geological {2., beijing 100081,{4. 2. institute of geology, Chinese Academy of geological {2., beijing SHRIMP Centre, beijing 10003.,{4. 1. institute of Geomechanics Chinese Academy of Geological Sciences 100081 Beijing China 2. institute of geology Chinese Academy of Geological Sciences Beijing SHRIMP Centre 100037 Beijing China

The Nyainqêntanglha Group is traditionally viewed as the oldest metamorphic basement in the Lhasa block, but its formation age and tectonic setting remain debate. Zircons extracted from the metamorphic sequence of volcanics and intrusions of the Nyainqêntanglha Group, 10 km west of Nam Co in northern Lhasa block, have been investigated by cathodolu- minescence (CL), backscattered (BSE) and dated by ion microprobe (SHRIMP). We conclude that the U-Pb age of 787±9 Ma of zircons from the trondhjemite imposes a constraint on maxi- mum protolith age, and minimum formation age of the Nyainqêntanglha Group is constrained by U-Pb age of 74.±8 Ma of zircons from the granite. The formation age of the Nyainqêntanglha Group is consistent with sedimentary age of Greater Himalayan rocks, showing that they devel- oped coevally in an arc-basin tectonic setting of Neoproterozoic active continental margin along the northern margin of the India shield. The inherited zircons from the tholetiite and granite give older 2.7Pb/2.6Pb ages from 94. to 1766 Ma. The positive εNd( t ) value indicates that the mafic rocks were derived from the depleted mantle, but contaminated by the older continental crustal material. Integrated Nd model age and U-Pb age data provide excellent evidence for the exis- tence of Mesoproterozoic basement in the Lhasa block during Neoproterozoic time.

关键词： Nyainqêntanglha Group, SHRIMP dating, Nd isotope, Neoproterozoic, Tibet.

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Principles and methods of quantitative analysis on b-axis disorder in 2.: 1 dioctahedral phyllosilicate

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Chinese Science Bulletin 1997年第22期42卷 1908-1912页

作者： WANG Ling and ZHANG Zhenyu1. Changsha institute of Geotectonics, Chinese Academy of sciences, Changsha {2.0013.{3. 2. institute of {{2., Chinese Academy of sciences, beijing 10002.,{3. Changsha institute of Geotectonics Chinese Academy of Sciences Changsha China institute of geology Chinese Academy of Sciences Beijing China

IN XRD patterns of clay minerals, a phenomenon that strong peaks often have (00l) and(hkl) (k=3.) indices and show symmetric figures can be seen commonly, while a minorityof reflection peaks (hkl) (k≠3.) are comparat... 详细信息

关键词： b-axis disorder pyrophvllile 2 phyllosilicate clay minerals dioctahedral minerals orientating structure of hy-droxyls crystal structure analysis DTA-TG.

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Relationships between bacterial-algal proliferating and mass extinction in the Late Devonian Frasnian-Famennian transition:Enlightening from carbon isotopes and molecular fossils

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Science china Earth sciences 2005年第10期48卷 1656-1665页

作者： GONG Yiming1,2. XU Ran1, TANG Zhongdao1, SI Yuanlan3.& LI Baohua4.1. Faculty of Earth Science and State Key Laboratory of geological Processes and Mineral Resources,{2. University of Geosciences, Wuhan 4.0074.{2. 2. {4. of Resources & Environments, Henan Polytechnic University, Jiaozuo 4.4.03.{2. 3. Department of Computer Science, South-Central University for Nationalities, Wuhan 4.0074.{2. 4. Laboratory of Marine geology, Tongji University, Shanghai 2.0092.{2. Faculty of Earth Science and State Key Laboratory of geological Processes and Mineral Resources china University of Geo{2. Wuhan china institute of Resources & Environments Henan Polytechnic University Jiaozuo china Department of Computer Science South-Central University for Nationalities Wuhan china Laboratory of Marine geology Tongji University Shanghai china

Studies show positive shifts of inorganic and organic carbon isotope values (δ 13.carb and δ 13.kerogen) from +0.4. (‰ V-PDB) to +3.54.(‰ V-PDB) and from ?2..3. (‰ V-PDB) to ?2.0}14.(‰ V-PDB), respectively, B* (Ba* = Ba/ (Al2.3.X 15%)) values from 0.015 to 0.14., TOC values from 0.02. to 0.2.%, V/Cr values from 0.3.to 2.0, Sr/Ba values from 3.2. to 4..50 in the Late Devonian Frasnian Upper rhenana zone to the top linguiformis zone of the Yangdi sec-tion deposited in carbonate slope facies of Guilin, Guangxi, South china, which indicates that biomass, productivity, organic carbon burial and salinity increase and that oxygenation near the boundary between sediments and waters decreases from the Late Devonian Frasnian Upper rhenana zone to the top linguiformis zone. Abundance of molecular fossils increases and normal alkanes, isoprenoid hydrocarbon, terpanes and steranes are dominated from the Late Devonian Frasnian to the bottom of Famennian, which shows that the predecessors of molecular fossils of the Frasnian-Famennian (F-F) transition are dominated by marine phytoplankton, zooplankton and benthic bacteria with no photosynthesis. Therefore, it is considered that the F-F transitional mass extinction with a multistage, selection and global synchronizing was caused by bacte-rial-algal proliferating, continuing deterioration of the shallow marine ecoenvironment of the mid-dle-lower latitudes. A simple cause and effect chain can be expressed as: appearance of seed plants and multi-storied forests → enhanced chemical and biochemical weathering and pe-dogenesis → wide development of soils → increasing riverine nutrient fluxes in epicontinental sea → from superoligotrophic to eutrophic in epicontinental sea → proliferating of marine phyto-plankton and zooplankton → frequent red tide and anoxia → mass extinction of shallow marine organisms in the middle-lower latitudes. It is worth notice that the factor drawdown of atmos-pheric Pco2. climatic cooling and sea level falling c

关键词： mass extinction, bacteria-algae, carbon isotopes, molecular fossils, biodiversity, Late Devonian, Guangxi, South china.

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Timing and history of marine hydrocarbon accumulation in Tarim craton

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Chinese Science Bulletin 2002年第S1期47卷 120-127页

作者： ZHAO Jingzhou~(1,2. & LI Qiming~3.1. Department of Petroleum geology, Xi’an Petroleum institute, Xi’an 710065,{2. 2. Research institute of Petroleum Exploration and Development, Petro{4., beijing 100083.{2. 3. Tarim Oilfield Company, Kuerle, Xinjiang 84.000,{2. Xian Petr Inst Dept Petr Geol Xian 710065 Peoples R China Petrochina Res Inst Petr Explorat & Dev Beijing 100083 Peoples R China Tarim Oilfield Co Xinjiang 841000 Peoples R China

Based on the analyses of hydrocarbon inclu-sions, K-Ar dating of authigenic illites and oil/gas-watercontact retrospection as well as other methods, the marineprimary reservoirs in the cratonic region of the Tarim Basinare found to have been formed in the late Caledonian toearly Hercynian, late Hercynian, and Himalayan, and oil andgas adjusted and redistributed in the Yanshanian (Jurassic toCretaceous) and Himalayan (Tertiary). The analyses alsoshow that the remaining primary oil accumulations aremostly formed in the late Hercynian, and the secondary oilreservoirs resulted from the adjustment and redistribution ofthe earlier accumulations during the Yanshanian and Hima-layan (especially late Himalayan), of which the Himalayan isalso the major stage of gas accumulation. The primary oilreservoirs formed in the late Hercynian mostly occur withinthe Paleozoic formation, whereas the secondary reservoirsformed in the Himalayan in the Mesozoic. The late adjust-ment and redistribution of reservoirs in the craton region ofthe Tarim Basin is ubiquitous because of the intensified tec-tonic movements since the Mesozoic, especially Cenozoic andintrusion of the high- to over-mature gas. Furthermore, thelower amplitude of reservoirs in the craton region also makesthem easier to be adjusted and redistributed. Therefore, theremaining paleo-uplift and palaeo-slope developed in rela-tively stable tectonic regions are the main potential areas forthe middle-large marine reservoirs in the Tarim Basin.

关键词： Tarim Basin craton geochronology of hydrocarbon accumulation history of hydrocarbon accumulation marine reservoir primary reservoir secondary reservoir.

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A New SHRIMP Age of the Xiamaling Formation in the North china Plate and Its geological Significance

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Acta Geologica Sinica(English Edition) 2007年第6期81卷 1103-1109页

作者： GAO Linzhi~(1,*)ZHANG Chuanheng~2.SHI Xiaoying~2.ZHOU Hongrui~2.WANG Ziqiang~2.SONG Biao~(1,3. 1 institute of geology,Chinese Academy of {2. sciences,{4. 10003.,china 2.7} University of Geosciences({4.),{4. 100083.china 3.{4. SHRIMP Central,10003. {4.,china institute of geology Chinese Academy of Geological Sciences Beijing 100037 China

Setting up the hypostratotype of late Precambrian is the main aim of the research on the Meso-and Neoproterozoic in North *** chronostratigraphic position is the key in this study. However,many key horizons have not been calibrated with the high-quality isotopic *** the reported new U-Pb age with the Sensitive High-Resolution Ion Microprobe（SHRIMPⅡ）,a zircon U- Pb age was obtained of the ash bed in the Xiamaling Formation in North china Plate,yielding a weighted mean;Pb/;U age of 13.8±12.*** is the first SHRIMP U-Pb age from the Xiamaling Formation in the North china Plate,and represents the depositing time of the middle part of the Xiamaling *** zircon age plays an important role to understanding {2. evolution of the North china Plate during Meso-and Neoproterozoic.

关键词： SHRIMP U-Pb Dating Mesoproterozoic Xiamaling Formation North china Plate

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