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Carbon isotope composition of the Lower Triassic marine carbonates, Lower Yangtze Region, South china

Science china Earth sciences 2006年第3期49卷 225-241页

作者： ZUO Jingxun1,2. TONG Jinnan3, QIU Haiou4.& ZHAO Laishi3 1. Nanjing Institute of Geology and Palaeontology, Chinese Academy of sciences, Nanjing 2.0008, {2. 2. Henan Institute of Geological Survey, Zhengzhou 4.0007, {2. 3. State Key Laboratory of Geological Processes and Mineral Resources at {2. University of {4., wuhan 4.0074. china 4. faculty of material sciences and chemical engineering, {2. University of {4., wuhan 4.0074. china 1. Nanjing Institute of Geology and Palaeontology Chinese Academy of Sciences Nanjing 210008 China 2. Henan Institute of Geological Survey Zhengzhou 450007 China 3. State Key Laboratory of Geological Processes and Mineral Resources at china University of geosciences Wuhan 430074 China 4. faculty of material sciences and chemical engineering China University of Geosciences Wuhan 430074 China

Studies on three Lower Triassic sections located on the shallow water platform, the deep water slope and in the deep water basin in the Lower Yangtze Region, South china, show the similar trend of carbon isotope evolution. Biostratigraphic correlations among the Lower Triassic sections on the basis of standard conodont zones indicate that three negative shifts occurred in the Griesbachian, the Smithian and the late Spathian stages respectively, and one distinctly positive shift occurred in the early Spathian stage. Trend of carbon isotope evolution of the Lower Triassic reflects some significant changes in the global carbon cycle. Moreover, δ 13C background values are intensively controlled by palaeogeographic environment. In general, δ 13C values from deep-water slope carbonates are lighter than those from carbonate platform and heavier than those from deep-water basin carbonates. The positive carbon isotope excursion may be induced by a significant amount of organic carbon burial in marine sediments and increase in primary productivity. The large negative carbon isotope excursions during the Early Triassic in Lower Yangtze Region are interpreted to relate to volcano eruptions based on tuffaceous claystone interlayers observed near the Permian-Triassic boundary, the Induan- Olenekian boundary and the Lower Triassic-Middle Triassic boundary.

关键词： Lower Triassic, carbon isotope compositions, palaeogeography, volcanic eruptions, Lower Yangtze Region.

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Synthesis and photochromic properties of WO_3 powder induced by oxalic acid

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Science china Chemistry 2009年第5期52卷 609-614页

作者： SHEN Yi1, ZHU Hua1, HUANG Rong1, ZHAO Li2.& YAN ShaNing1 1 faculty of material Science and {2. engineering, {4. University of geosciences, wuhan 4.0074. china 2.faculty of materials Science and engineering, Hubei University, wuhan 4.0062. {4. 1. faculty of material Science and {2. engineering China University of Geosciences Wuhan 430074 China 2. faculty of materials Science and {2. Hubei University Wuhan 430062 China

Tungsten trioxide powder with the novel morphology was prepared via the hydrothermal method with oxalic acid as the organic inducer, the structure and shape of which were detected by X-ray diffraction (XRD), scanning electron microscopy (SEM) and BET. Furthermore, photochromic properties of the as-prepared powder samples were tested by an ultraviolet-visible spectrophotometer combined with a color difference meter. The corresponding results indicated that the induced product was still hexagonal WO3, made up of regularly spindle particles with 2.0-300 nm in length and 30-50 nm in width. The ratio of the length and width was from 4.to 10. Moreover, the special morphology improved its absorptive capacity to the excitation light source, resulting in its high photochromic properties.

关键词： WO3 powder photochromism oxalic acid organic inducer

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On-line parallel reversed phase two-dimensional liquid chromatography for high-throughput analysis of complex proteomic samples

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Science china Chemistry 2006年第6期49卷 527-533页

作者： WANG Zhicong1,3, ZHANG Qinghe2. LI Tong2. ZHAO Zhongyi3 & ZHANG Weibing1 1. Dalian Institute of chemical Physics, Chinese Academy of sciences, Dalian 116011, {2. 2. Dalian Elite Analytical Instrument Co., Ltd., Dalian 116011, {2. 3. {4. of material Science and chemical engineering, {2. University of geosciences, wuhan 4.0074. china 1. Dalian Institute of chemical Physics Chinese Academy of Sciences Dalian 116011 China 3. faculty of material Science and {2. engineering China University of Geosciences Wuhan 430074 China 2. Dalian Elite Analytical Instrument Co. Ltd. Dalian 116011 China

A comprehensive two-dimensional liquid chromatographic system (2. SCX/RP) is con- structed with a 10-port-2.way valve using strong cation exchange chromatography (Hypersil SCX, 100 mm×4.6 mm I.D.) followed by reversed phase chromatography (Hypersil BDS C18, 15 mm×4.6 mm I.D.) to separate the complex peptides from globin peptic hydrolysate. After the sample was loaded on the SCX column, the phosphate buffer (pH 4.0) was used to elute the peptides. Then, elutes flowed through the interface and the peptides focused on the head of the trapping columns (Hypersil BDS C18, 15 mm×4.6 mm I.D.) but salt passed into the waste. After the valve was switched, the samples were flushed with a backward flow into the RP analytical column. The peptides on the SCX were eluted with 12.discontinuous steps linearly increasing salt concentrations. The peptides enriched on the trapping column were desalted and separated by the RP columns. The resolution and the resolved peaks of the 2. SCX/RP system were greatly increased and the total peak capacity reached as high as 2.80.

关键词： two-dimensional liquid chromatography, interface, trapping column, proteomics, globin.

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Synthesis and photoluminescence property of red phosphors LiEu_(1-x)Y_x(WO_4._(0.5)(MoO_4._(1.5) for white LED

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Science china(Technological sciences) 2009年第7期52卷 1913-1918页

作者： XIE An, YUAN XiMing, WANG JuanJuan & WANG Feng engineering Research Center of Nano-Mineral materials and Application, Ministry of Education, {2. of materials Science and {4. engineering, china University of geosciences, wuhan 4.0074. china 1. engineering Research Center of Nano-Mineral materials and Application Ministry of Education Faculty of Materials Science and Chemical Engineering China University of Geosciences Wuhan 430074 China

A series of novel red phosphors LiEu1-xYx(WO4.0.5(MoO4.1.5 (x=0, 0.1, 0.2. 0.3, 0.4. 0.5, 0.6, 0.8) were synthesized by conventional solid state reaction method with the starting materials: WO3, MoO3, Eu2.3, Li2.O3 and Y2.3. The spectrum and the crystal structure of the phosphors were characterized by F-4.00 and XRD respectively. Meanwhile the effects of flux and Y3+ concentration on the crystal structure and luminescent properties of the phosphors were investigated. The results showed that the optimal content of flux (WAlF3/WH3BO3=1/1) was 1 wt% and the optimal doping concentration of Y3+ was 0.5 mol. The emission spectrum showed the most intense peak was located at 615 nm, which corresponds to the 5D0→7F2.transition of Eu3+ and that Eu3+ occupied the lattice site of noncentrosymmetric environment in the scheelite phases. The excitation spectrum displayed that these phosphors could be effectively excited by ultraviolet (UV) (396 nm) and blue (4.6 nm) light, nicely in correspondence with the widely ap- plied output wavelengths of ultraviolet or blue LED chips. The influence of flux on the luminescent properties of LiEu0.5Y0.5(WO4.0.5(MoO4.1.5 phosphor was analyzed. The XRD spectra indicated that the flux could help to crystallize the phosphor, and no other phases were formed except the tetragonal. When adding flux, the relative intensity of LiEu0.5Y0.5(WO4.0.5(MoO4.1.5 became much stronger and the average particle size of the phosphor decreased.

关键词： red emitting phosphor LiEu1-xYx(WO4.0.5(MoO4.1.5 flux white LED

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Proton induced X-ray emission (PIXE) analysis of sources of porcelain body of Ru Guan and Jun Guan porcelains

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Science china(Physics,Mechanics & Astronomy) 2006年第4期49卷 411-420页

作者： LI Guoxia1, ZHAO Weijuan1, LI Rongwu2. SUN Hongwei1, GUO Min1, WANG Yanfang1, LIU Hui1, ZHAO Qingyun3, SUN Xinmin3, ZHAO Wenjun3 & CHENG Huansheng4.1. faculty of Physical {2., Zhengzhou University, Zhengzhou 4.0052. china 2. Department of Physics, Beijing Normal University, Beijing 100875, china 3. Institute of Cultural Relic and Archaeology of Henan Province, Zhengzhou 4.0000, china 4. Institute of Modern Physics, Fudan University, Shanghai 2.04.3, china faculty of Physical engineering Zhengzhou University Zhengzhou 450052 China Department of Physics Beijing Normal University Beijing 100875 China Institute of Cultural Relic Archaeology of Henan Province Zhengzhou 450000 China Institute of Modern Physics Fudan University Shanghai 200433 China

34.samples of Ru Guan porcelain body and 50 samples of Jun Guan porcelain body (both kinds being in different body colors) were selected with the purpose of finding out the source of raw materials and their classification relationship so as to search for ways of non-destructive discrimination. Proton induced X-ray emission (PIXE) has been applied to these samples to determine their {2. elements. The data of seven major {2. elements collected from these samples were further studied through fuzzy cluster analysis. Results indicate that the origin of raw materials of Jun Guan porcelain body samples is comparatively more concentrated in certain places, while that of Ru Guan porcelain body samples is scattered about. The places of origin of raw materials of the majority of Ru Guan and Jun Guan porcelain body samples have something in common, but some differences still exist. It might be an important way for non-destructive discrimination among Ru Guan and Jun Guan porcelains by combining PIXE with fuzzy cluster analysis.

关键词： Ru Guan and Jun Guan porcelain, source of porcelain body, PIXE, fuzzy cluster analysis, non-destructive discrimination.

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Composite Cathode Bi_(1.14.Sr_(0.4.)O_(2.14.-Ag for Intermediate-temperature Solid Oxide Fuel Cells

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Journal of wuhan University of Technology(materials Science) 2008年第3期23卷 350-353页

作者：高展张萍 faculty of material Science and {2. engineering China University of Geosciences

Composites consisting of strontium stabilized bismuth oxide （Bi1.14.r0.4.O2.14. SSB） and silver were investigated as cathodes for intermediate-temperature solid oxide fuel cells with doped ceria electrolyte. There were no chemical reactions between the two components. The microstructure of the interfaces between composite cathodes and Ce0.8Sm0.2.1.9 （SDC） electrolytes was examined by scanning electron microscopy （SEM）. Impedance spectroscopy measurements show that the performance of cathode fired at 700 ℃ is the best. When the content of Ag2. is 70 wt%, polarization resistance values for the SSB-Ag cathodes are as low as 0.2.Ωcm^2.at 700℃ and 0.2. Ωcm^2.at 650℃. These results are much smaller than some of other reported composite cathodes on doped ceria electrolyte and indicate that SSB-Ag composite is a potential cathode material for intermediate temperature SOFCs.

关键词： solid oxide fuel cells (SOFCs) composite cathode strontium stabilized bismuth oxide (SSB) samaria doped ceria (SDC)

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New stylophorans(Echinodermata) from the Upper Cambrian of Guangxi,South china

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Science china Earth sciences 2008年第2期51卷 181-186页

作者： HAN NaiRen1 & CHEN GuiYing1,2.1 Department of Resources and Environmental engineering, Guilin University of Technology, Gulin 54.004. china 2.faculty of Earth sciences, china University of Geoscience, wuhan 4.0074. china Department of Resources and Environmental engineering Guilin University of Technology Gulin 541004 China faculty of Earth sciences China University of Geoscience Wuhan 430074 China

This paper describes for the first time the cornute stylophorans (Echinodermata) in china. The new material came from the Guole Formation of the Furongian (Late Cambrian) in the Guole area of Jingxi, Guangxi Province, South china. These new cornute specimens are preserved in situ and found along with well-preserved trilobites and brachiopods. One new species, Phyllocystis jingxiensis sp. nov., is proposed to accommodate these unusual materials. The new species is defined by the small, heart-shaped theca with the frame composed of ten narrow, smooth and thick marginal plates, three adoral plates and distinctive zygal and aulacophore. Both supracentrals and infracentrals are polygonal-outlined. The marginal plate M1' on the inferior face extends posteriorly to form zygal that possesses a broadened proximal end and the proximal portion joining with the conjunction between M4.and M5 on the inferior face. Aulacophore comprises ten segments at its proximal part and is conical at the middle part (named stylocone). Its distal portion is rather long and bears conspicuous ambulacrum grooves. Tectals are horizontally arranged on superior face and obliquely arranged on inferior face. Both cothurnopore and anal pyramid are vaguely seen on the right anterior corner and the extremity of theca's superior face.

关键词： Phyllocystis Stylophora Echinodermata Cambrian Guangxi South china

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Research into Exploitation and Application of Three Sorts of

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Journal of Earth Science 2000年第2期19卷 96-97页

作者： Li Zhen Shen Shangyue Chi bo Zhang De Yang Mei faculty of material {2. and Chemistry engineering, {4. University of geosciences, wuhan 4.0074

In this paper the authors introduce their past years’study results about the exploitation and application of three sorts of nontraditional nonmetal minerals. In this research, the main aspects and techniques of basic study for the exploitation and application are summarized, and some key science and technological problems are proposed as the objects of their future research.

关键词： nontraditional nonmetal minerals exploitation application medified superfine papermaking plastic rubber.

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Research on semi-solid slurry of a hypoeutectic Al-Si alloy prepared by low superheat pouring and weak electromagnetic stirring

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Rare Metals 2006年第2期25卷 177-183页

作者： LIU Zheng MAO Weiming ZHAO Zhengduo material of Science and engineering School University of Science and Technology Beijing Beijing 100083 China faculty of material and {2. engineering Jiangxi University of Science and Technology Ganzhou 341000 China

The semi-solid slurry of a hypoeutectic Al-Si alloy was manufactured by low superheat pouring and weak electromagnetic stirring. The effects of pouting temperature and stirring power on the semi-solid slurry were investigated. The results indicated that the semi-solid slurry to satisfy rheocasting can be manufactured by low superheat pouring and weak electromagnetic stirring. The pouring temperature （or superheat） and the stirring power remarkably affected the morphology of primary α-Al and the size of primary α-Al, and there is no obvious effect of stirring time on primary α-Al. Compared with the samples made by low superheat pouring with no stirring, the nucleation rate, particle morphology and grain size of primary α-Al in A356 were markedly improved by low superheat pouring and weak electromagnetic stirring. On the condition of weak electromagnetic stirring, the pouring temperature with low superheat can be suitably raised to reach the effectiveness obtained from the lower pouring temperature without stirring.

关键词： semi-solid low superheat pouring weak electromagnetic stirring hypoeutectic Al-Si alloy A356 Al alloy

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Surface roughness and removal rate in magnetorheological finishing of a subsurface damage free surface

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Progress in Natural Science:materials International 2005年第6期15卷 538-544页

作者： CHENG Haobo1*, WANG Yingwei2. FENG Zhijing1 and CHENG Kai3(1. State Key Laboratory of Tribiology, Tsinghua University, Beijing 100084. china 2. Department of {2. sciences, Changchun University of Science and Technology, Changchun 13002., china 3. {4. of Information and engineering Systems, City Campus, Leeds LS1 3HE, UK) State Key Laboratory of Tribiology Tsinghua University Beijing 100084 China Department of material sciences Changchun University of Science and Technology Changchun 130021 China faculty of Information and engineering Systems City Campus Leeds LS1 3HE UK

Based on computer-controlled optical surfacing, a new technique called magnetorheological finishing (MRF), is presented. The new technique combines the features of conventional loose abrasive machining with a wheel shaped polishing tool. The tool incorporates a host of features and has unprecedented fabricating versatility. The pre-polishing and fine polishing processes can be performed only by adjusting different parameters. The material removal function is studied theoretically and the results of simulation present a Gaussian distribution feature. Based on the established theoretical model, material removal rate experiments involving a parabolic mirror are designed and carried out to determine the effect of controllable parameters on size of the gap between the workpiece and the polishing wheel, rotating speed of the polishing wheel, concentration of volume fraction of non-magnetic particles and polishing time. Further experiments are carried out on the surface microstructure of the workpiece, the final surface roughness with an initial value of 10.98 nm reaches 1.2. nm root mean square (RMS) after 2. min of polishing. The subsurface damage experiment and the atomic force microscopy (AFM) measurement on the polished surface can also verify the feasibility of the MRF technique.

关键词： magnetorheological finishing surface roughness computer controlled optical surfacing subsurface damage removal function.

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