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Synthesis and magnetic properties of CdS/α-Fe_2O_3 hierarchical nanostructures

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Science china(Physics,Mechanics & Astronomy) 2009年第7期52卷 997-1002页

作者： CHEN YuJin1,2,3, SHI XiaoLing1, CAO MaoSheng1 & ZHU ChunLing4 1 School of Materials Science and engineering, Beijing institute of technology, Beijing 100081, china 2 Micro-Nano Technologies Research Center, Hunan University, Changsha 410082, china 3 college of Science, Harbin engineering University, Harbin 150001, china 4 college of Material Science and Chemical engineering, Harbin engineering University, Harbin 150001, china 1. School of Materials Science and engineering Beijing Institute of Technology Beijing 100081 China 2. Micro-Nano Technologies Research Center Hunan University Changsha 410082 China 3. college of Science Harbin Engineering University Harbin 150001 China 4. college of Material Science and Chemical engineering Harbin Engineering University Harbin 150001 China

CdS/α-Fe2O3 hierarchical nanostructures, where the CdS nanorods grow irregularly on the side surface of α-Fe2O3 nanorods, were synthesized via a three-step process. The diameters and lengths of CdS nanorods can be tuned by changing the ethylenediamine (EDA) and Cd ion concentrations. The magnetic investigations by superconducting quantum interference device indicate that the hierarchical nanostructures have an Morin transition at lower temperature (230 K) than that of the single bulk α-Fe2O3 materials (263 K). Importantly, the hierarchical nanostructures exhibit weakly ferromagnetic characteristics at 300 K. A sharp peak assigned to the surface trap induced emission are observed in room temperature PL spectra. Combining with the optoelectronic properties of CdS, the CdS/ α-Fe2O3 hierarchical nanostructures may be used as multi-functional materials for optoelectronic and magnetic devices.

关键词： α-Fe2O3 CdS hierarchical nanostructures magnetic properties

The characteristics of arc beam shaping in hybrid plasma and laser deposition manufacturing

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Science china(Technological Sciences) 2006年第2期49卷 238-247页

作者： ZHANG Hai’ou1, QIAN Yingping1,3, WANG Guilan1 & ZHENG Qiguang2 1. School of Material Science and technology, Huazhong University of Science and technology, Wuhan 430074, china 2. institute of Laser technology and engineering, Huazhong University of Science and technology, Wuhan 430074, china 3. Mechanical engineering college, Hubei University of technology, Wuhan 430068, china 1. School of Material Science and technology Huazhong University of Science and Technology Wuhan 430074 China 3. Mechanical engineering college Hubei University of Technology Wuhan 430068 China 2. institute of Laser technology and engineering Huazhong University of Science and Technology Wuhan 430074 China

As a new direct metal prototyping technology,the hybrid plasma and laser deposition manufacturing (PLDM) is proposed in this paper. In order to figure out the characteristics of plasma arc beam and mould in the PLDM process of high temperature alloy, the high speed CCD camera is used to obtain the picture around the plasma arc. Afterwards the sketch of picture is clearly obtained. And the effect of laser parameter, such as average power, pulse width, pulse repetition frequency and the angle between laser beam and plasma arc beam on the plasma arc appearance, is studied experimentally. The results show that the modality of plasma arc beam is markedly influenced by laser beam. And the improvements of shape precision and surface state of the layer deposited by PLDM are confirmed.

关键词： plasma hybrid laser, direct deposition, plasma arc beam, molding character, high-temperature alloy.

Preparation and microstructure of CuO-CoO-MnO/SiO2 nanocomposite aerogels and xerogels as catalyst carriers

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Progress in Natural Science:Materials International 2011年第4期21卷 330-335页

作者： Yue-qing ZHAO~1,Ying-hua LIANG~2,Xi-zhe ZHAO~3,Qian-yi JIA~4,Hong-sheng LI~4 1.college of Light Industry,Hebei United University,Tangshan 063000,china 2.college of Chemical engineering,Hebei United University,Tangshan 063009,china 3.college of Printing and Packaging engineering,Beijing institute of Graphic Communication,Beijing 102600,china 4.college of Materials Science and engineering,Hebei United University,Tangshan 063009,china [a] college of Light Industry Hebei United University Tangshan 063000 China [b] college of Chemical engineering Hebei United University Tangshan 063009 China [c] college of Printing and Packaging engineering Beijing Institute of Graphic Communication Beijing 102600 China [d] college of Materials Science and engineering Hebei United University Tangshan 063009 China

CuO-CoO-MnO/SiO2nanocomposite aerogels and xerogels were prepared using tetraethyl orthosilicate（TEOS） as Si source,and aqueous solution of Cu,Co and Mn acetates as the precursor via sol-gel process,CO2supercritical drying（SCD） technique or ambient pressure drying *** microstructure of the CuO-CoO-MnO/SiO2nanocomposite aerogels and xerogels were characterized by field emission scanning electron microscopy（FE-SEM）,transmission electron microscopy（TEM） and X-ray diffraction（XRD）.The specific surface area,pore size and pore size distribution of the nanocomposite aerogels and xerogels were determined by the Brunauer-Emmett-Teller（BET） *** results showed that CuO-CoO-MnO/SiO2nanocomposite aerogels are porous,with a pore size distribution of 2-50 nm,an average pore size of 19.4 nm,a specific surface area of 384.9 m2/g and a particle size distribution of 10-150 nm,whereas the pore size distribution of CuO-CoO-MnO/SiO2composite xerogels is 1.7-128.6 nm,the average pore size is only 9.9 nm,the specific surface area is only 99.1 m2/g,and the particle size distribution is 100-500 *** structure of CuO-CoO-MnO/SiO2nanocomposite aerogels is favorable to increase the loading of catalysts.

关键词： composite aerogel composite xerogel catalyst carrier preparation microstructure

Description to wear debris boundaries by radar graph fractal method

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Chinese Science Bulletin 2007年第16期52卷 2285-2290页

作者： LIU HongTao1,2 & GE ShiRong1 1 institute of Tribology and Reliability engineering,china University of Mining & technology,Xuzhou 221008,china 2 college of Mechanical and Electrical engineering,china University of Mining & technology,Xuzhou 221116,china institute of Tribology and Reliability engineering China University of Mining and Technology Xuzhou 221008 China

In this paper,radar graph fractal method is introduced to describe wear debris boundaries. Research results show that it is a nice way to describe wear debris boundaries. Since the longest axis is selected as the first coordinate axis,its center point selected as the center point of the radar graph,and the co-ordinate value of wear debris boundary selected as the measure parameter,the limitations existing in Yard fractal measure method can be avoided. For any wear debris,its radar graph fractal dimension value is one and only,and as the wear debris shape changes from round to strip,the radar graph fractal dimension value also changes from low to high,showing strong uniqueness and independence. Due to the fact that the researched wear debris is gotten in different wear states,the results also prove that radar graph fractal dimension value is correlated with frictional pairs work condition and wear state. Radar graph fractal method is compared with Yard fractal measure methods,and results show that ra-dar graph fractal dimension values gotten from different wear debris have enough value grads to avoid effect of errors,and provide higher sensitivity for wear debris shape. This paper also discusses the influencing factors for radar graph fractal method. With the increase of the decomposing degree value,the radar graph fractal dimension tends to keep stable at one certain value,showing the typical characteristic of the fractal theory. All this proves that radar graph fractal method is an effective description method for wear debris boundaries.

关键词：磨粒边界雷达图表分形法

One-pot synthesis of crystalline SnO_2 nanoparticles and their low-temperature ethanol sensing characteristics

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Science china(Physics,Mechanics & Astronomy) 2009年第10期52卷 1601-1605页

作者： CHEN YuJin1,2,3,ZHU ChunLing4,WANG LiJiao3 & WANG TaiHong2 1 School of Materials Science and engineering,Beijing institute of technology,Beijing 100081,china 2 Micro-Nano Technologies Research Center,Hunan University,Changsha 410082,china 3 college of Science,Harbin engineering University,Harbin 150001,china 4 college of Material Science and Chemical engineering,Harbin engineering University,Harbin 150001,china School of Materials Science and engineering Beijing Institute of Technology Beijing 100081 China Micro-Nano Technologies Research Center Hunan University Changsha 410082 China college of Science Harbin Engineering University Harbin 150001 China college of Material Science and Chemical engineering Harbin Engineering University Harbin 150001 China

Crystalline SnO2 nanoparticles(NPs) with a diameter less than 6 nm are synthesized using potassium stannate trihydrate as the precursor in a basic *** synthesized NPs can detect ethanol at a ppm level even at 100℃.Furthermore,the NPs have good selectivity to *** excellent ethanol sensing performances are attributed to the small size effect according to the space-charge model.

关键词： SnO2 nanoparticles sensing characteristics

Investigation of 'chazi'(damaged-enamels)on Chenghua doucai Porcelains

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Science china(Technological Sciences) 2009年第6期52卷 1722-1729页

作者： DU Feng1 & SU BaoRu2 1 institute of Chemistry & Molecular engineering,Qingdao University of Science & technology,Qingdao,china 2 college of Information Science & technology,Qingdao University of Science & technology,Qingdao,china institute of Chemistry & Molecular engineering Qingdao University of Science & Technology Qingdao China college of Information Science & technology Qingdao University of Science & Technology Qingdao China

At the end of the 1950s,Sun Yingzhou considered that the 'chazi'(damaged colour)on Chenghua doucai imperial porcelain as a defect was originally produced in firing process during Chenghua period(1465―1487).Researchers in china have accepted his *** any fragment with the 'chazi' has never been found in several tons of Chenghua imperial sherds excavated from Ming imperial kiln site in *** china,few scholars have questioned the formation of 'chazi',and further investigated *** researchers at the Research Laboratory in the British Museum,employing unde-structive EDXRF,have analyzed the chemical composition of the 'chazi'(damaged colour)on a Chen-ghua doucai stem cup in the museum,and they have confirmed that the 'chazi'(damaged colour)was caused by the fire of the Jianfu palace in the Forbidden City in *** on their research,the authors studied the colour chemical principle of the 'chazi's' formation *** to the ceramic technology principle,scientific reasoning for the 'chazi' was carried *** the help of the history of Qing court,the brainteaser of the 'chazi' was totally uncovered,the misunderstanding for the 'chazi' has also been *** research also suggests that employing modern science and technology is a direction to study Chinese ancient ceramic further.

关键词： Chenghua doucai porcelains court eunuchs the set on fire at the Jianfu palace ’chazi’(damaged-enamels) the British Museum colour chemical principle archaeology using science and technology

Implementation of the Fredkin gate with a three-qubit mixed-spin Heisenberg model

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Science china(Physics,Mechanics & Astronomy) 2010年第7期53卷 1276-1280页

作者： FAN QiuBo college of Mathematics and Physics,Xuzhou institute of technology,Xuzhou 221008,china 1. college of Mathematics and Physics Xuzhou Institute of Technology Xuzhou 221008 China

We show that a local unitary(LU) equivalent Fredkin gate can be obtained from the free evolution of three mixed-spin qubits by virtue of numerical simulation with only one *** spin-1 qubit acts as the control qubit,and two spin-1/2 qubits,which interact with the spin-1 qubit via the first neighbor spin interaction,respectively,play the role of target *** also examine the imperfect Fredkin gate operation by considering the effects of nonidentical coupling constants,uniform and inhomogeneous magnetic fields.

关键词： Fredkin gate mixed spin quantum computation

Particle swarm optimization with a leader and followers

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Progress in Natural Science:Materials International 2008年第11期18卷 1437-1443页

作者： Junwei Wang Dingwei Wang institute of Systems engineering,college of Information Science and engineering,Northeastern University,Shenyang 110004,china institute of Systems engineering College of Information Science and Engineering Northeastern University Shenyang 110004 China

Referring to the flight mechanism of wild goose flock,we propose a novel version of Particle Swarm Optimization(PSO)with a leader and *** is referred to as Goose Team Optimization(GTO).The basic features of goose team flight such as goose role division, parallel principle,aggregate principle and separate principle are implemented in the recommended *** GTO,a team is formed by the particles with a leader and some *** role of the leader is to determine the search *** followers decide their flying modes according to their distances to the leader ***,a wide area can be explored and the particle collision can be really *** GTO is applied to four benchmark examples of complex nonlinear functions,it has a better computation perfor- mance than the standard PSO.

关键词： Particle swarm optimization Goose team optimization Role division Parallel principle Aggregate principle Separate principle

Further study of sources of the imported cobalt-blue pigment used on Jingdezhen porcelain from late 13 to early 15 centuries

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Science china(Technological Sciences) 2008年第3期51卷 249-259页

作者： DU Feng1 & SU BaoRu2 1 institute of Chemistry & Molecular engineering, Qingdao University of Science & technology, Qingdao 266000, china 2 college of Information Science technology, Qingdao University of Science & technology, Qingdao 266000, china institute of Chemistry & Molecular engineering Qingdao University of Science & Technology Qingdao 266000 China college of Information Science technology Qingdao University of Science & Technology Qingdao 266000 China

Based on the conclusion of modern scientific analysis: the cobalt-blue pigment applied on Jingdezhen official porcelain during Yuan Dynasty and prior to Xuande reign of Ming Dynasty (1271―1425) contains high iron and low manganese con- tents, and the cobalt during Xuande and after Xuande periods (after 1426) of Ming Dynasty contains high manganese and low iron contents, in combination with the traditional archaeological method, the related historical textual records were in- vestigated and analyzed, the imported cobalt employed on Jingdezhen official porcelain was studied comprehensively, systematically and logically. In fact, 'Su Ma Li Qing' (Samarra-blue) and 'Su Bo Ni Qing' (Sumatra-blue) are definitely different cobalt ores originated in different places, because of their very similar translitera- tions in Chinese, the confusion has appeared in ancient books for more than 400 years, which considered 'Su Ma Li Qing' and 'Su Bo Ni Qing' as the same co- balt-blue pigment. In this article the mistake was corrected, the possible producing places and the approximate eras of the two pigments imported to china and used at Jingdezhen were also suggested.

关键词： imported cobalt-blue pigments employed on official blue-and-white porcelain Yuan Dynasty early Ming Dy- nasty Mn/Fe content ratio Su Ma Li Qing (Samarra-blue) Su Bo Ni Qing (Sumatra-blue) scientific archae- ological research transliteration