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Application of backflush and micro-flow techniques to the analysis of C5—C13 hydrocarbons in crude oils and its geochemical significance

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Progress in Natural Science:Materials International 2007年第11期17卷 1382-1387页

作者： Wang Peirong1,2, Zhao Hong2,3, Xu Guanjun1,4, Zhu Cuishan2,3, Xiao Tingrong4, Zhang Min2,3 and Zhang Bin1,4(1. Key Laboratory of petroleum Geochemistry, china National petroleum Corporation, beijing 100083, china 2. Geochemistry Department of Yangtze University, Jingzhou 434023, china 3. Key Laboratory of exploration Technologies for Oil and Gas Resources, Ministry of Education, Yangtze University, Jingzhou 434023, china 4. petroleum Geology Central Laboratory, Research institute of petroleum exploration and Development, Petrochina, beijing 100083, china) Key Laboratory of petroleum Geochemistry China National Petroleum Corporation Beijing 100083 China Geochemistry Department Yangtze University Jingzhou 434023 China Key Laboratory of exploration Technologies for Oil and Gas Resources Yangtze University Jingzhou 434023 China petroleum Geology Central Laboratory Research Institute of Petroleum Exploration and Development PetroChina Beijing 100083 China

An Agilent 6890N GC equipped with both FID and Agilent 5975 MSD analyzer has been employed to analyze C5—C13 hydrocarbon fractions of crude oils. A technical combination of program temperature volatilizer injection, backflush and micro-flow controller afforded a fine separation of C5—C13 compounds on a PONA column with the heavy part of crude oils being cut off before entering the analytical column. Both GC-FID chromatogram and GC-MS mass chromatograms (MID and full scan) could be obtained at the same time. The retension time differences of nC6—nC13 alkanes between GC and TIC were in the range of 0.02—0.58 minutes. Totally 286 peaks have been assigned group compositions. Results on 8 typical oil samples from CNPC Key Laboratory Crude Oil Library showed that the characteristics of C6—C13 hydrocarbon group composition could be used in oil-oil correlation studies.

关键词： GC analysis GC/MS analysis backflush micro-flow controller light fraction in crude oil

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Biogas charging and dissipating process and its accumulation in the Sebei gasfield,Qaidam Basin,china

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Science china Earth Sciences 2008年第S1期51卷 36-44页

作者： JIN Qiang 1,CHENG FuQi 1,2 ,SU AiGuo 3 ,ZHU GuangYou 3 ,WANG Li 1 &CAO Qian 1 1 china University of petroleum,Dongying,Shandong 257061,china 2 Geological institute of Shengli Oilfield,sinopec,Dongying,Shandong 257015,china 3 petroleum exploration and Development institute,Petrochina,beijing 100083,china china University of petroleum Dongying China Geological institute of Shengli Oilfield SINOPEC Dongying China petroleum exploration and Development institute PetroChina Beijing China

The Sebei gasfield is the largest biogas accumulation found in china and many reservoirs and seal rocks superposed on a syndepositional anticline in *** biogas charging and dissipating process and its distribution have been a research focus for many *** authors suggest a diffusing and accumulating model for the biogas,as they find that the shallower the gas producer,the more methane in the biogas,and the lighter stable carbon isotope composition of *** on the diffusing model,diffused biogas is quantitatively estimated for each potential sandy reservoir in the gasfield,and the gas charging quantity for the sandy reservoir is also calculated by the diffused gas quantity plus gas reserve in-place.A ratio of diffusing quantity to charging quantity is postulated to describe biogas accumulating state in a sandy reservoir,if the ratio is less than 0.6,the reservoir forms a good gas-pool and high-production layer in the gasfield,which often occurs in the reservoirs deeper than 900 m;if the ratio is greater than 0.6,a few gas accumulated in the reservoir,which frequently exists in the reservoirs shallower than 900 ***,a biogas accumulation model is built up as lateral direct charging from gas source for the sands deeper than 900 m and indirect charging from lower gas-bearing sands by diffusion at depth shallower than 900 *** this charging and diffusion quantitative model,the authors conducted re-evaluation on each wildcat in the central area of the Qaidam Basin,and found many commercial biogas layers.

关键词： biogas charging and diffusing model relative dissipated quantity Qaidam Basin

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TTHE METHODOLOGY OF petroleum DEVELOPMENT GEOLOGY(Ⅲ)

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石油勘探与开发 1996年第4期 78-82页

作者： Qiu Yinan (Research institute of petroleum exploration and Development, CNPC, beijing, 100083, P.R.china)

ＴＨＥ　ＭＥＴＨＯＤＯＬＯＧＹ　ＯＦ　ＰＥＴＲＯＬＥＵＭ　ＤＥＶＥＬＯＰＭＥＮＴ　ＧＥＯＬＯＧＹ（Ⅲ）ＴＨＥＭＥＴＨＯＤＯＬＯＧＹＯＦＰＥＴＲＯＬＥＵＭＤＥＶＥＬＯＰＭＥＮＴＧＥＯＬＯＧＹ（Ⅲ）￥ＱｉｕＹｉｎａｎ（Ｒ...

ＴＨＥ　ＭＥＴＨＯＤＯＬＯＧＹ　ＯＦ　ＰＥＴＲＯＬＥＵＭ　ＤＥＶＥＬＯＰＭＥＮＴ　ＧＥＯＬＯＧＹ（Ⅲ）ＴＨＥＭＥＴＨＯＤＯＬＯＧＹＯＦＰＥＴＲＯＬＥＵＭＤＥＶＥＬＯＰＭＥＮＴＧＥＯＬＯＧＹ（Ⅲ）￥ＱｉｕＹｉｎａｎ（ＲｅｓｅａｒｃｈＩｎｓｔｉｔｕｔｅｏ...

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Seismic multi-arch structures in East china

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Science china Earth Sciences 2006年第2期49卷 133-146页

作者： YANG Wencai1 & CHEN Zhide2 1.institute of Geology, Chinese Academy of Geological Sciences, beijing 100037, china 2.Daqing institute of petroleum exploration and production, Daqing 163712, china institute of Geology Chinese Academy of Geological Sciences Beijing China Daqing institute of petroleum exploration and production Daqing China

In previous papers (Wencai, 2002, 2003), the author has analyzed the deep seismic reflection profiles along some of the Mesozoic plutons in East china, and has pointed out that the crustal structures around these intrusions usually correlate with a special seismic fabric called the seismic multi-arch structure. This paper will continue to show main characteristics of the seismic multi-arch structures and discuss their relationship with mantle-origin magmatism and the lithospheric thinning process. Calibration of seismic reflectors in Chinese continental drilling sites shows that small-scale arch-like reflectors can be generated by fractured eclogites or other plutons, they do not belong to the multi-arch structure specially discussed in the paper. The multi-arch structure is char-acterized by several arch-like reflectors distributed in both the upper and lower crust with granitoid plutons or stocks exposed on the surface, which do not have obvious negative Europium anomalies. Based on the distribution pattern of arch reflectors, the multi-arch magmatic structures can be divided into three main types, namely the simple vertical combination type, the spread arch magmatic struc-ture and the arch-bouquet structure. All of them correlate to mantle-origin magmatism, but occur in different places. The spread arch magmatic structures occur within a Mesozoic/Cenozoic rift zone with very thin and hot lithosphere. The vertical combination type of the multi-arch structures occurred near the rift zones where lithosphere was thin and hot. The arch-bouquet magmatic structures occur far from the rift zones where the lithosphere is not hot. The continental rifting acted as the late episode of the lithospheric thinning process seeing that the rift zones usually coincide with the thinnest parts of the lithosphere in East china. In different locations within the lithospheric thinning areas, mantle-origin magmatic activities have different characteristics, which might generate different

关键词： deep seismic reflection, multi-arch structure, eclogite bodies, mantle-origin magmatism, East china.

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An analysis of seismic attenuation in random porous media

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Science china(Physics,Mechanics & Astronomy) 2010年第4期53卷 628-637页

作者： LIU Jiong1, BA Jing2, MA JianWei1 & YANG HuiZhu1 1 institute of Seismic exploration, School of Aerospace, Tsinghua University, beijing 100084, china 2 Research institute of petroleum exploration & Development, Petrochina, beijing 100083, china institute of Seismic exploration School of Aerospace Tsinghua University Beijing China Research institute of petroleum exploration & Development PetroChina Beijing China

The attenuation of seismic wave in rocks has been one of the interesting research topics, but till now no poroelasticity models can thoroughly explain the strong attenuation of wave in rocks. In this paper, a random porous medium model is designed to study the law of wave propagation in complex rocks based on the theory of Biot poroelasticity and the general theory of stochastic process. This model sets the density of grain, porosity, permeability and modulus of frame as random parameters in space, and only one fluid infiltrates in rocks for the sake of better simulation effect in line with real rocks in earth strata. Numerical simulations are implemented. Two different inverse quality factors of fast P-wave are obtained by different methods to assess attenuation through records of virtual detectors in wave field (One is amplitude decay method in time domain and the other is spectral ratio method in frequency domain). Comparing the attenuation results of random porous medium with those of homogeneous porous medium, we conclude that the attenuation of seismic wave of homogeneous porous medium is far weaker than that of random porous medium. In random porous media, the higher heterogeneous level is, the stronger the attenuation becomes, and when heterogeneity σ = 0.15 in simulation, the attenuation result is consistent with that by actual observation. Since the central frequency (50 Hz) of source in numerical simulation is in earthquake band, the numerical results prove that heterogeneous porous structure is one of the important factors causing strong attenuation in real stratum at intermediate and low frequency.

关键词： the theory of stochastic process the theory of Biot poroelasticity the attenuation of seismic wave inverse quality factor

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A kind of coccoid dinoflagel-lates-like fossils gives a new explanation of source of dinosterane in the Early-Middle Cambrian

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Chinese Science Bulletin 2001年第5期46卷 420-423,442页

作者： BIAN Lizeng, ZHANG Shuichang, ZHANG Baomin, MAO Shaozhi & YIN LeimingDepartment of Earth Sciences, Nanjing University, Nanjing 210093,china Key Laboratory of petroleum Geochemistry, china National petroleum Corporation, beijing 100083, china Research institute of petroleum exploration and Development, china National petroleum Corporation, beijing 100083, china china University of Geosciences, beijing 100083, china Nanjing institute of Geology and Palaeontology, Chinese Academy of Sciences, Nanjing 210008, china Department of Earth Sciences Nanjing University Nanjing China Key Laboratory of petroleum Geochemistry China National Petroleum Corporation Beijing China Research institute of petroleum exploration and Development China National Petroleum Corporation Beijing China china University of Geosciences Beijing China Nanjing institute of Geology and Palaeontology Chinese Academy of Sciences Nanjing China

The coccoid fossils covered with thick gelatinous envelop containing several gametes are discovered in gyps and salt deposits of Cambrian, H4 well and chert bed of the base of Yuertus Formation (∈11) of Xiaoerbulake Section. The fossils are described and compared with coccoid dinoflagellates. These fossils may be a coccoid life-cycle stage (vegetative cyst) of coccoid dinoflagellates. If this identification is correct, the coccoid dinoflagellates-like fossils could give a reasonable explanation of the dinoflagellate-specific biomarkers from Cambrian, H4 well, Tarim Basin.

关键词： coccoid dinoflagellates-like fossils dinoflagellate-specific biomarkers Cambrian Tarim Basin.

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Timing and history of marine hydrocarbon accumulation in Tarim craton

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Chinese Science Bulletin 2002年第S1期47卷 120-127页

作者： ZHAO Jingzhou~(1,2) & LI Qiming~3 1. Department of petroleum Geology, Xi’an petroleum institute, Xi’an 710065, china 2. Research institute of petroleum exploration and Development, Petrochina, beijing 100083, china 3. Tarim Oilfield Company, Kuerle, Xinjiang 841000, china Department of petroleum Geology Xi’an Petroleum Institute Xi’an China Research institute of petroleum exploration and Development PetroChina Beijing China Tarim Oilfield Company Kuerle Xinjiang China

Based on the analyses of hydrocarbon inclu-sions, K-Ar dating of authigenic illites and oil/gas-watercontact retrospection as well as other methods, the marineprimary reservoirs in the cratonic region of the Tarim Basinare found to have been formed in the late Caledonian toearly Hercynian, late Hercynian, and Himalayan, and oil andgas adjusted and redistributed in the Yanshanian (Jurassic toCretaceous) and Himalayan (Tertiary). The analyses alsoshow that the remaining primary oil accumulations aremostly formed in the late Hercynian, and the secondary oilreservoirs resulted from the adjustment and redistribution ofthe earlier accumulations during the Yanshanian and Hima-layan (especially late Himalayan), of which the Himalayan isalso the major stage of gas accumulation. The primary oilreservoirs formed in the late Hercynian mostly occur withinthe Paleozoic formation, whereas the secondary reservoirsformed in the Himalayan in the Mesozoic. The late adjust-ment and redistribution of reservoirs in the craton region ofthe Tarim Basin is ubiquitous because of the intensified tec-tonic movements since the Mesozoic, especially Cenozoic andintrusion of the high- to over-mature gas. Furthermore, thelower amplitude of reservoirs in the craton region also makesthem easier to be adjusted and redistributed. Therefore, theremaining paleo-uplift and palaeo-slope developed in rela-tively stable tectonic regions are the main potential areas forthe middle-large marine reservoirs in the Tarim Basin.

关键词： Tarim Basin craton geochronology of hydrocarbon accumulation history of hydrocarbon accumulation marine reservoir primary reservoir secondary reservoir.

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THE METHODOLOGY OF petroleum DEVELOPMENT GEOLOGY(Ⅱ)

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石油勘探与开发 1996年第3期 93-96页

作者： Qiu Yinan (Research institute of petroleum exploration and Development, CNPC, beijing, 100083, P. R. china)

ＴＨＥＭＥＴＨＯＤＯＬＯＧＹＯＦＰＥＴＲＯＬＥＵＭＤＥＶＥＬＯＰＭＥＮＴＧＥＯＬＯＧＹ（Ⅱ）￥ＱｉｕＹｉｎａｎ（ＲｅｓｅａｒｃｈＩｎｓｔｉｔｕｔｅｏｆＰｅｔｒｏｌｅｕｍＥｘｐｌｏｒａｔｉｏｎａｎｄＤｅｖｅｌｏｐｍｅｎ...

ＴＨＥＭＥＴＨＯＤＯＬＯＧＹＯＦＰＥＴＲＯＬＥＵＭＤＥＶＥＬＯＰＭＥＮＴＧＥＯＬＯＧＹ（Ⅱ）￥ＱｉｕＹｉｎａｎ（ＲｅｓｅａｒｃｈＩｎｓｔｉｔｕｔｅｏｆＰｅｔｒｏｌｅｕｍＥｘｐｌｏｒａｔｉｏｎａｎｄＤｅｖｅｌｏｐｍｅｎｔ，ＣＮＰＣ，Ｂｅｉｊｉｎｇ，１０...

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Geochemical characteristics of abiogenic alkane gases

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petroleum Science 2009年第4期6卷 327-338页

作者： Yunyan Ni Jinxing Dai Petrochina Res Inst Petr Explorat & Dev Beijing 100083 Peoples R China

Recently abiogenic alkanes have been found in various locations in the world and other celestial bodies. The chemical composition of abiogenic alkane gases varies widely. The content of methane is low and nearly no C2+ is found in the abiogenic alkane gases from fluid inclusions in volcanic rocks or hot springs in china. In the unsedimented submarine hydrothermal vent system C1/C2+ ratios are much greater than those for the thermogenic gases, mostly >800 and in some cases up to 8,000. In the Songliao Basin, china, C1/C2+ of some abiogenic gases are often less than 150. Abiogenic alkane gases which have been found in nature often have carbon isotopic reversal among C1–C4 alkanes (δ13C1>δ13C2>δ13C3>δ13C4), whereas both regular and reversed hydrogen isotope distribution pattern among C1–C4 alkanes have been reported. The δ13C of abiogenic methane is mainly greater than ?30‰ though laboratory synthesized methane can have δ13C as low as ?57‰, and its δD1 values vary widely and overlap with biogenic gases. High 3He/4He ratios often indicate the addition of mantle-derived helium and are related to abiogenic gases. However, some biogenic gases can also have high 3He/4He ratios up to 8. The CH4/3He end-member is often lower than 106 for abiogenic alkane gases while greater than 1013 for biogenic gases, and the values between these two end-members often reflect the mixing of biogenic and abiogenic gases.

关键词： Abiogenic origin alkane gas carbon isotopic reversal trend geochemical characteristics

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Application of C5-C13 light hydrocarbons in depositional environment diagnosis

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Progress in Natural Science:Materials International 2008年第9期18卷 1129-1137页

作者： Peirong Wanga,b,, Guanjun Xu a,c, Tingrong Xiaoc, Dajiang Zhanga,c, Bin Zhanga,c a Key Laboratory of petroleum Geochemistry, china National petroleum Corporation, beijing 100083, china b Department of Organic Geochemistry, Yangtze University, Jingzhou 434023, china c Central Laboratory of petroleum Geology, Research institute of petroleum exploration and Development, Petrochina, beijing 100083, china Key Laboratory of petroleum Geochemistry China National Petroleum Corporation Beijing 100083 China Department of Organic Geochemistry Yangtze University Jingzhou 434023 China Central Laboratory of petroleum Geology Research Institute of Petroleum Exploration and Development PetroChina Beijing 100083 China

Based on the geological background and Gammacerane/C31H(S + R) ratios, source rock depositional environments of the studied oil samples (194) from 13 oilfields were classified into three groups according to salinity:saline-lacustrine facies, fresh to brackish lacustrine facies (including limnetic facies), and semi-saline to saline facies (including marine facies of the Tarim Basin).C5-C13 compound groups in the crude oils were separated by GC, and about 286 compounds were qualitatively *** geochemical application of the C6-C13 compound groups and their ratios between each group with individual carbon number was *** studies show that (1) C6-C13 compound groups and their ratios in the crude oils could serve as new reliable parameters for oil-oil correlation because the C6-C13 light fractions are the major oil component, especially in light oil or condensate, in which they account for almost 90% of the whole oil;(2) the compound groups of C7 light hydrocarbons in oils derived from difierent depositional environments with difierent salinity have difierent characteristics;(3) C6-C13 compound groups and ratios may be afiected by other factors such as maturity, but they are mainly controlled by salinity of depositional waters.

关键词： Light hydrocarbons Crude oil Depositional environment Salinity

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