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Geochemical characteristics and origin of gases from the Upper,Lower Paleozoic and the Mesozoic reservoirs in the Ordos Basin,china

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Science china Earth Sciences 2008年第S1期51卷 183-194页

作者： HU AnPing 1 ,Li Jian 2.,ZHANG WenZheng 3 ,LI ZhiSheng 2.,HOU Lu 4 &LIU QuanYou 5 1 Department of Earth Sciences,Zhejiang University,Hangzhou 31002.,china 2.Langfang Branch,Reasearch institute of {2. exploration and development,Petrochina,Langfang 065007,china 3 institute of exploration and development,Petrochina changqing Oilfield Company,{12.,china 4 University of {2.,Beijing102.49,china 5 Petrochina Research institute of {2. exploration and development,Beijing 100083,china 1. Department of Earth Sciences Zhejiang University Hangzhou 310027 China2. Langfang Branch Reasearch Institute of Petroleum Exploration and Development PetroChina Langfang 065007 China3. Institute of Exploration and Development PetroChina Changqing Oilfield Company Xi’an 710021 China4. University of Petroleum Beijing 102249 China5. PetroChina Research Institute of Petroleum Exploration and Development Beijing 100083 China

The Ordos Basin,the second largest sedimentary basin in china,contains the broad distribution of natural gas *** far,several giant gas fields have been discovered in the Upper and Lower Paleozoic in this basin,each having over 1000×10 8 m 3 of proven gas reserves,and several gas pools have also been discovered in the *** paper collected the data of natural gases and elucidated the geochemical characteristics of gases from different reservoirs,and then discussed their *** hydrocarbons preserved in the Upper Paleozoic,the elevatedδ13C values of methane,ethane and propane indicate that the gases would be mainly coal-formed gases;the singular reversal in the stable carbon isotopes of gaseous alkanes suggests the mixed gases from humic sources with different *** the Lower Paleozoic,theδ13C 1 values are mostly similar with those in the Upper Paleozoic,but theδ13C 2.andδ13C 3 values are slightly lighter,suggesting that the gases would be mixing of coal-type gases as a main member and oil-type *** are multiple reversals in carbon isotopes for gaseous alkanes,especially abnormal reversal for methane and ethane(i.e.δ13C 1 >δ13C 2.),inferring that gases would be mixed between high-mature coal-formed gases and oil-type *** the Mesozoic,the δ13Cvalues for gaseous alkanes are enriched in 12.,indicating that the gases are mainly derived from sapropelic sources;the carbon isotopic reversal for propane and butane in the Mesozoic is caused by microbial oxidation and mixing of gases from sapropelic sources with different *** contrast to the Upper Paleozoic gases,the Mesozoic gases are characterized by heavier carbon isotopes of iso-butane than normal butane,which may be caused by gases generated from different kerogen types. Finally,according toδ13C 1 -Ro relationship and extremely low total organic carbon contents,the Low Paleozoic gases would not be generated from the Ordovician source as a main gas source,bycontrast, the Upper Pale

关键词： Ordos Basin natural gas chemical composition carbon isotope genesis

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Timing and history of marine hydrocarbon accumulation in Tarim craton

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Chinese Science Bulletin 2002年第S1期47卷 120-127页

作者： ZHAO Jingzhou~(1,2. & LI Qiming~3 1. Department of petroleum Geology, xi’an petroleum {2., xi’an 710065, china 2. Research {2. of petroleum exploration and development, Petrochina, Beijing 100083, china 3. Tarim Oilfield Company, Kuerle, xinjiang 841000, china xian Petr Inst Dept Petr Geol Xian 710065 Peoples R China Petrochina Res Inst Petr Explorat & Dev Beijing 100083 Peoples R China Tarim Oilfield Co Xinjiang 841000 Peoples R China

Based on the analyses of hydrocarbon inclu-sions, K-Ar dating of authigenic illites and oil/gas-watercontact retrospection as well as other methods, the marineprimary reservoirs in the cratonic region of the Tarim Basinare found to have been formed in the late Caledonian toearly Hercynian, late Hercynian, and Himalayan, and oil andgas adjusted and redistributed in the Yanshanian (Jurassic toCretaceous) and Himalayan (Tertiary). The analyses alsoshow that the remaining primary oil accumulations aremostly formed in the late Hercynian, and the secondary oilreservoirs resulted from the adjustment and redistribution ofthe earlier accumulations during the Yanshanian and Hima-layan (especially late Himalayan), of which the Himalayan isalso the major stage of gas accumulation. The primary oilreservoirs formed in the late Hercynian mostly occur withinthe Paleozoic formation, whereas the secondary reservoirsformed in the Himalayan in the Mesozoic. The late adjust-ment and redistribution of reservoirs in the craton region ofthe Tarim Basin is ubiquitous because of the intensified tec-tonic movements since the Mesozoic, especially Cenozoic andintrusion of the high- to over-mature gas. Furthermore, thelower amplitude of reservoirs in the craton region also makesthem easier to be adjusted and redistributed. Therefore, theremaining paleo-uplift and palaeo-slope developed in rela-tively stable tectonic regions are the main potential areas forthe middle-large marine reservoirs in the Tarim Basin.

关键词： Tarim Basin craton geochronology of hydrocarbon accumulation history of hydrocarbon accumulation marine reservoir primary reservoir secondary reservoir.

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Contributors and potential of hydrocarbon generation of source rocks by solid-state ^(13)C NMR spectroscopy

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Chinese Science Bulletin 1997年第6期42卷 478-481页

作者： WANGZhaoyun, ZHAO Changyi, CHENG Keming and LU Qinghua1. Research institute of petroleum {2. and development, china National petroleum corporation, Beijing 100083, china:2. University of petroleum, Beijing, 100083 china Research institute of petroleum {2. and development China National Petroleum Corporation Beijing China University of petroleum Beijing China

SOLID-STATE 13C nuclear magnetic resonance （NMR） technique is an effective method to study the texture of material. Under the condition of high magnetic field （400 MHz） and by the application of cross polarization, magic angle spinning （CP/MAS）, total sideband suppression （TOSS）, etc., the content of different textural carbons in kerogen has been quantitatively analyzed by the solid-state 13C NMR spectroscopy of a series of kerogen of thermal simulation samples with Ro value ranging from 0.64% to 1.76%. The results show that

关键词： solid 13C NMR analysis aliphatic carbon potential of hydrocarbon generation of source rocks.

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Application of backflush and micro-flow techniques to the analysis of C5—C13 hydrocarbons in crude oils and its geochemical significance

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Progress in Natural Science:Materials International 2007年第11期17卷 1382-1387页

作者： Wang Peirong1,2. Zhao Hong2.3, Xu Guanjun1,4, Zhu Cuishan2.3, xiao Tingrong4, Zhang Min2.3 and Zhang Bin1,4(1. Key Laboratory of petroleum Geochemistry, china National petroleum corporation, Beijing 100083, china 2. Geochemistry Department of Yangtze University, Jingzhou 43402., china 3. Key Laboratory of exploration Technologies for Oil and Gas Resources, Ministry of Education, Yangtze University, Jingzhou 43402., china 4. petroleum Geology Central Laboratory, Research institute of petroleum exploration and {12., Petrochina, Beijing 100083, china) Key Laboratory of petroleum Geochemistry China National Petroleum Corporation Beijing 100083 China Geochemistry Department of Yangtze University Jingzhou 434023 China Key Laboratory of exploration Technologies for Oil and Gas Resources Ministry of Education Yangtze University Jingzhou 434023 China petroleum Geology Central Laboratory Research Institute of Petroleum Exploration and Development PetroChina Beijing 100083 China

An Agilent 6890N GC equipped with both FID and Agilent 5975 MSD analyzer has been employed to analyze C5—C13 hydrocarbon fractions of crude oils. A technical combination of program temperature volatilizer injection, backflush and micro-flow controller afforded a fine separation of C5—C13 compounds on a PONA column with the heavy part of crude oils being cut off before entering the analytical column. Both GC-FID chromatogram and GC-MS mass chromatograms (MID and full scan) could be obtained at the same time. The retension time differences of nC6—nC13 alkanes between GC and TIC were in the range of 0.02.0.58 minutes. Totally 2.6 peaks have been assigned group compositions. Results on 8 typical oil samples from CNPC Key Laboratory Crude Oil Library showed that the characteristics of C6—C13 hydrocarbon group composition could be used in oil-oil correlation studies.

关键词： GC analysis GC/MS analysis backflush micro-flow controller light fraction in crude oil

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Geochemical characteristics and source rock of Ordovician gas reservoir, changqing Gasfield

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Chinese Science Bulletin 1999年第20期44卷 1917-1920页

作者： xiA xinyu, ZHAO Lin, ZHANG Wenzheng and LI JianfengResearch institute of petroleum {2. and development, Beijing 100083, china changqing petroleum {2. Bureau, XL an 71002. , china Research institute of petroleum {2. and development Beijing China changqing petroleum {2. Bureau Xi’an China

Carbon isotopic composition of methane in Ordovician gas reservoir in the changqing Gasfield can reflect the dominance of Upper Paleozoic coal-type gas despite its high mature degree. The 12.-rich ethane in the Ordovician reservoir (δ13C2.2.‰), known as a marker as oil-type gas, does not indicate the Ordovician marine carbonate as main source rock, it is be-

关键词： methane ethane carbon isotope natural gas genesis. changqing Gasfield.

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Primary migration and secondary alteration of the Upper Paleozoic gas reservoir in Ordos Basin,china―Application of fluid inclusion gases

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Science china Earth Sciences 2008年第S1期51卷 165-173页

作者： GONG Se 1,2.,PENG PingAn 1 ,SHUAI YanHua 3 ,DAI Jinxing 3 &ZHANG WenZheng 4 1 Guangzhou institute of Geochemistry,the Chinese Academy of Sciences,Guangzhou 510640,china 2.Common Wealth Scientific and Research Organization,{2. Resources,PO Box 136,North Ryde,New South Wales,1670,Australia 3 Research institute of {2. exploration and development,Petrochina,Beijing 100083,china 4 Research institute of exploration and development,{12.,xi’an 71002.,china Guangzhou institute of Geochemistry the Chinese Academy of Sciences Guangzhou 510640 China Common Wealth Scientific and Research Organization Petroleum Resources PO Box 136 North Ryde New South Wales 1670 Australia Research institute

The composition of fluid inclusions(FI)often represents the initial geochemical characteristics of palaeo-fluid in reservoir *** on composition and carbon isotopic composition of gas during primary migration,reservoir-forming and subsequent secondary alterations are discussed through comparing fluid inclusion gas with coal-formed gas and natural gas in present gas reservoirs in the Ordos *** results show that primary migration of gas has significant effect on the molecular but not on the carbon isotopic composition of *** and diffusion fractionation took place during the secondary migration of gas in Upper Paleozoic gas reservoir according to carbon isotopic composition of methane in *** and carbon isotopic composition of natural gas were nearly unchanged after the gas reservoir forming through comparing the FI gases with the natural gas in present gas reservoir.

关键词： secondary alteration fluid inclusion carbon isotope Ordos Basin

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Wave tectono-sedimentary processes in Tarim basin

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Science china Earth Sciences 2005年第11期48卷 1949-1959页

作者： JIN Zhijun1,2. ZHANG Yiwei1 & CHEN Shuping1 1. Key Laboratory for Hydrocarbon Accumulation, Ministry of Education, china University of petroleum, Beijing 102.49, china 2. exploration and Production Research institute, china petroleum & Chemical corporation, Beijing 100083, china 1. Key Laboratory for Hydrocarbon Accumulation Ministry of Education China University of Petroleum 102249 Beijing China 2. exploration and Production Research institute China Petroleum & Chemical Corporation 100083 Beijing China

Based on the unconformities, the formation times of structures, and geological wave filtering applied to basin fills of typical wells around the Manjiaer area in the Tarim basin, the wave tectono-sedimentary processes in the Tarim Basin are discussed. The results of geological wave filtering of basin fills of typical wells show that, in time domain, the evolution of the Tarim basin was controlled by various wave processes with the periods of 740±Ma, 2.0±Ma, 100±Ma and 30±Ma. The analyses of basin fills, basin subsidence and unconformities show that the trends of the sedimentary facies belts, depocenters, and centers of subsidence migrated and interchanged periodically with periods of 2.0±Ma. These show the propagation of wave movements in space domain. The wave evolution of the Tarim basin is of significance to understanding the formation of the oil and gas reservoirs in the basin.

关键词： Tarim basin, tectonics, sedimentation, crustal undation, wave evolution

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Carbon isotope composition and its implications of Lower Cretaceous Aptian-Albian shallow water carbonates in the Cuoqin Basin, North Tibet

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Science china Earth Sciences 2004年第3期47卷 247-254页

作者： ZHU Jingquan1, LI Yongtie2. JIANG Maosheng1 & CHEN Daizhao1 1. institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing 10002., china 2. Research institute of petroleum exploration and development, CNPC, Beijing 100083, china Chinese Acad Sci Inst Geol & Geophys Beijing 100029 Peoples R China CNPC Res Inst Petr Explorat & Dev Beijing 100083 Peoples R China

The d 13C values of Lower Cretaceous Aptian-Albian platform-type carbonates in the Cuoqin Basin, North Tibet vary between 2.48 and 5.46. The mean value is 3.93. The values are not only provided with positive excursion, but also 1.17 higher than those of con-temporaneous pelagic carbonates which possess pretty high d 13C values. The origin is ap-proached. During the oceanic anoxic events, a great number of organisms were rapidly buried, causing the increase of the d 13C value of oceanic total dissolved carbon (TDC) and generally promoting the values of marine carbonates. After that, owing to the organisms undergoing dif-ferent isotopic fractionation in the paleo-ocean with stratified structure, d 13C values of shallow sea carbonate were obviously higher than those of pelagic carbonates.

关键词： shallow water carbonate, stable carbon isotope, paleooceanography, Aptian-Albian stage, Cuoqin Basin.

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Study on forward modeling of through-casing resistivity logging

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Science china Earth Sciences 2008年第S2期51卷 207-211页

作者： GAO Jie1,LIU FuPing2.BAO DeZhou3,CHENG xi3 & ZHANG YuLing4 1 china University of petroleum,Beijing 102.49,china 2.Beijing institute of Graphic Communication,Beijing 102.00,china 3 china petroleum Logging CO. LTD.,xi’an 71002.,china 4 china National Logging corporation,Beijing 100101,china china Univ Petr Beijing 102249 Peoples R China Beijing Inst Graph Commun Beijing 102600 Peoples R China china Petr Logging CO LTD Xian 710021 Peoples R China china Natl Logging Corp Beijing 100101 Peoples R China

Through-casing resistivity logging (TCRL) is a new kind of logging method for formation evaluation,reservoir monitoring and saturation changes tracking. In this paper,the basic principle of TCRL is de-tailed,and the modified transmission line equation method (MTLEM) is first proposed in china. The MTLEM has been employed to simulate the responses of TCRL,on the basis of which,the effects of formation resistivity,cement and casing on the responses of TCRL are analyzed,and the signals in-duced in different formations are also calculated,which can help the design of TCRL tool and data processing and interpretation in china.

关键词： through-casing resistivity logging (TCRL) modified transmission line equation method (MTLEM) casing cement sheath

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Effects of abnormally high heat stress on petroleum in reservoir——An example from the Tazhong 18 Well in the Tarim Basin

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Science china Earth Sciences 2008年第4期51卷 515-527页

作者： ZHU DongYa1, JIN ZhiJun1, HU WenXuan2.& ZHANG XueFeng3 1 petroleum exploration and Production {2., china petroleum & Chemical corporation, Beijing 100083, china 2.Department of Earth Sciences, Nanjing University, Nanjing 2.0093, china 3 School of Resource and Information, china University of petroleum, Beijing 102.49, china petroleum exploration and Production {2. China Petroleum & Chemical Corporation Beijing China Department of Earth Sciences Nanjing University Nanjing China School of Resource and Information China University of Petroleum Beijing China

An igneous intrusion of 94m thick was discovered intruding into the Silurian sandstone from Tazhong 18 Well. The petroleum previously preserved in the Silurian sandstone reservoir was altered into black carbonaceous bitumen by abnormally high heat stress induced by the igneous intrusion. The reflec-tance of the carbonaceous bitumen reaches as high as 3.54%, indicating that the bitumen had evolved into a high thermal evolution level. Similar to the Silurian samples from the neighboring Tazhong 11, Tazhong 12. Tazhong 45 and Tazhong 47 wells, the distribution of C2., C2. and C2. steranes of the car-bonaceous bitumen is still "V" -shaped and can still be employed as an efficient parameter in oil source correlation. The "V" -shaped distribution indicates that the hydrocarbons from the Tazhong 18 and the neighboring wells were all generated from the Middle-Upper Ordovician hydrocarbon source rocks. However, the oil source correlation parameters associated with and terpanes had been changed greatly by the high heat stress and can no longer be used in oil source correlation. The δ 13C values of the pe-troleum from the neighboring wells are between -32.53‰ and -33.37‰, coincident with those of the Paleozoic marine petroleum in the Tarim Basin. However, the δ 13C values of the carbonaceous bitumen from the Tazhong 18 Well are between -2..18‰ and -2..2.‰, isotopically much heavier than the pe-troleum from the neighboring wells. The content of light hydrocarbons (nC14-nC2.) of the saturated hydrocarbon fraction in the carbonaceous bitumen is extremely higher than the content of heavy hy-drocarbons. The light/heavy hydrocarbon ratios (ΣnC2.-/ΣnC2.+) are between 4.56 and 39.17. In the saturated fraction, the even numbered hydrocarbons are predominant to the odd numbered, and the OEP (Odd to Even Predominance) values are between 0.2. and 0.49. However, the content of light hy-drocarbons in the petroleum from the neighboring wells is relatively low and the content of the even numb

关键词： Tarim Basin igneous intrusive abnormally high heat stress bitumen carbon isotope PAH

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