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Preparation of Pt/K_2.a_2.i_3._(10) and its photo-catalytic activity for hydrogen evolution from methanol water solution

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Science China Chemistry 2006年第2期49卷 162-168页

作者： CUI Wenquan1,3. LIU Li2. FENG Liangrong1, XU Chenghua1, LI Zijian1, Lü Shaojie1 & QIU Fali1 1. Chengdu Institute of Organic Chemistry, Chinese academy of {2., Chengdu 610041, China 2. Chemistry Department, Sichuan University of Science & Engineering, Zigong 643.3., China 3. graduate {3. of the Chinese academy of {2., beijing 10003., China Correspondence should be addressed to Qiu Fali 1. Chengdu Institute of Organic Chemistry Chinese Academy of Sciences Chengdu 610041 China 3. graduate {2. of the Chinese academy of {3. Beijing 100039 China 2. Chemistry Department Sichuan University of Science & Engineering Zigong 643033 China

A layered perovskite-type oxide K2.a2.i3.10 was prepared with high-temperature solid-state reaction, and characterized with X-ray diffraction (XRD) and ultraviolet-visible diffuse re-flectance spectroscopy (UV-Vis DRS). Platinum was loaded onto K2.a2.i3.10 as a co-catalyst with different methods. The dispersion of platinum on K2.a2.i3.10 was determined with HOT method. The photocatalytic activity of Pt/K2.a2.i3.10 was studied. This catalyst showed much higher activity in hydrogen evolution reaction than Ni/K2.a2.i3.10. The effects of different amounts of loaded platinum and several preparation methods were evaluated. The best achieved hydrogen evolution rate was 2.0}.88 μmol·h?1 by Pt(2.)/K2.a2.i3.10. A possible band structure and mechanism were discussed based on the results.

关键词： photocatalysis hydrogen platinum K_2.a_2.i_3._(10) support

Effective solutions to a global 3. visual system in networking environments

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Science China Earth sciences 2005年第11期48卷 2032-2039页

作者： ZHANG Liqiang1,2. ZHANG Yan3. YANG Chongjun2. LIU Suhong1, REN Yingchao2. RUI Xiaoping2.& LIU Donglin2.1. State Key Laboratory of Remote Sensing sciences, {2. of Geography and Remote Sensing, beijing Normal University, beijing 100875, China 2. State Key Laboratory of Remote Sensing sciences, Institute of Remote Sensing Applications, Chinese academy of sciences, beijing 101001, China 3. Institute of Geographical sciences and Natural Resources Research, Chinese academy of sciences, beijing 101001, China 1. State Key Laboratory of Remote Sensing sciences School of Geography and Remote Sensing Beijing Normal University 100875 Beijing China 2. Chinese academy of sciences State Key Laboratory of Remote Sensing SciencesInstitute of Remote Sensing Applications 101001 Beijing China 3. Institute of Geographical sciences and Natural Resources Research Chinese Academy of Sciences 101001 Beijing China

The development of Web-based global 3. visual system has made progresses. However, there exist few mature and effective ways for managing, transmitting and visualizing massive spatial data. Based on the related work, the paper illustrates the ellipsoidal quadtree technique for rapid access multi-scale and multiple level geographical data, integrates the streaming with level-of-detail rendering method for transmitting the data on the network, and im-plements large-scale terrain surface simplification using M-band wavelet transforms and mul-tiresolution triangulations. We fulfil a web-based global terrain visual system using COM com-ponents on the basis of the above techniques. The system has a good prospect in the military simulation and city plans.

关键词： massive spatial data, streaming transmission, system architecture, M-band wavelet

The regular representation and regular covariant representation of crossed products of Woronowicz C^(*)-algebras

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Science China Mathematics 2005年第9期48卷 1245-1259页

作者： ZHANG Xiaoxia~(1,2. & GUO Maozheng~(1,3. 1. school of Mathematical {2.,Peking University,beijing 100871,China 2. Department of Mathematics,Yantai University,Yantai 2.4005,China 3. LMAM,Peking University,beijing 100871,China 1. school of Mathematical sciences Peking University 100871 Beijing China 2. Department of Mathematics Yantai University 264005 Yantai China 3. LMAM Peking University 100871 Beijing China

In this paper,it is shown that the regular representation and regular covariant representation of the crossed products A×α G correspond to the twisted multiplicative unitary operators,where A is a Woronowicz C~*-algebra acted upon by a discrete group ***,it is also shown that the regular covariant C~*-algebra is the Woronowicz C~*-algebra which corresponds to a multiplicative ***,an explicit description of the multiplicative unitary operator for C(SU_q(2. )×α (?) is given in terms of those of the Woronowicz C~*-algebra C(SU_q(2. ) and the discrete group G.

关键词： multiplicative unitary operator, Woronowicz C*-algebra, crossed product.

Prediction method for October 2.03.solar storm

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Science China(Technological sciences) 2006年第5期49卷 629-640页

作者： XIE Yanqiong1, 2. 3. WEI Fengsi1, FENG Xueshang1 & ZHONG Dingkun1, 2.1. State Key Laboratory of Space Weather, Center for Space Science and Applied Research, Chinese academy of {2., beijing 100080, China 2. {3. school, Chinese academy of {2., beijing 10003., China 3. Institute of Meteorology, PLA University of Science and Technology, Nanjing 2.1101, China State Key Laboratory of Space Weather Center for Space Science Applied Research Chinese Academy of Sciences Beijing 100080 China graduate school Chinese Academy of Sciences Beijing 100039 China Institute of Meteorology PLA University of Science Technology Nanjing 211101 China

Aiming at two intense shock events on October 2. and 2., 2.03. this paper presents a two-step method, which combines synoptic analysis of space weather ——“observing” and quantitative prediction ——“palpating”, and then uses it to test predictions. In the first step of “observing”, on the basis of observations of the solar source surface magnetic field, interplanetary scintillation (IPS) and ACE spacecraft, we find that the propagation of the shocks is asymmetric relative to the normal direction of their solar sources, and the Earth is located near the direction of the fastest speed and the greatest energy of the shocks. As the two fast ejection shock events, the fast explosion of coronal mass of the extremely high temperature, the strong magnetic field, and the high speed background solar wind are also helpful to their rapid propagation. In the second step of “palpating”, we adopt a new membership function of the fast shock events for the ISF method. The predicted results show that for the onset time of the geomagnetic disturbance, the relative errors between the observational and the predicted results are 1.8% and 6.7%; and for the magnetic disturbance magnitude, the relative errors are 4.1% and 3.1%, re- spectively. Furthermore, the comparison among the predicted results of our two-step method with those of five other prevailing methods shows that the two-step method is advantageous. The results tell us that understanding the physical features of shock propagation thoroughly is of great importance in improving the prediction precision.

关键词： solar storm, interplanetary shock, interplanetary scintillation, two-step method, ISF method.

Sporopollen analysis of Core B10 in the southern Yellow Sea and the reflected characteristics of climate changes

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Chinese Science Bulletin 2003年第B06期48卷 42-48页

作者： FU Mingzuo~(1,2.3., LI Zhen~1, XU Xiaowei~1 & SHl Xuefa~1 1. Key Laboratory of Marine Sedimentology and Environmental Geology, First institute of Oceanography. State Oceanic Administration, Qingdao 2.6061. China 2. Institute of Oceanology, Chinese academy of {2., Qingdao 2.6071. China 3. graduate {3., Chinese academy of {2., beijing 10003.. China 1. Key Laboratory of Marine Sedimentology and Environmental Geology First institute of Oceanography State Oceanic Administration 266061 Qingdao China 2. Institute of Oceanology Chinese Academy of Sciences 266071 Qingdao China 3. graduate {2. Chinese Academy of Sciences 100039 Beijing China

Eight sporopollen zones have been divided based on the results of high-resolution sporopollen analysis of Core B10 in the southern Yellow Sea. Based on the results along with ^14C datings and the subbottom profiling data,climatic and environmental changes since the last stage of late Pleistocene are discussed. The main conclusions are drawn as follows: (1) the vegetation evolved in the process of coniferous forest-grassland containing broad-leaved trees→coniferous and broad-leaved mixed forest→coniferons and broad-leaved mixed forest-grassland prevailed by coniferous trees→coniferous and broad-leaved mixed forest-grassland containing evergreen broad-leaved trees→coniferons and broad-leaved mixed forest-grassland prevailed by broadleaved trees→deciduous broad-leaved forest-meadow containing evergreen broad-leaved trees→coniferous and broadleaved mixed forest-grassland prevailed by broad-leaved trees→coniferous and broad-leaved mixed forest containing evergreen broad-leaved trees; (2. eight stages of climate changes are identified as the cold and dry stage, the temperate and wet stage, the cold and dry stage, the warm and dry stage, the temperate and wet stage, the hot and dry stage, the temperate and dry stage, then the warm and dry stage in turn; (3. the sedimentary environment developed from land,to littoral zone, to land again, then to shore-neritic zone; and (4) the Yellow Sea Warm Current formed during early-Holocene rather than Atlantic stage.

关键词：中国黄海气候变化碳14年代测定底基压型数据更新世沉积环境大西洋

Experimental and discrete element numerical analysis of side slope instability induced by fissure water underlying impervious bed

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Science China(Technological sciences) 2005年第z1期48卷 65-80页

作者： LIU Bingshan1, LI Shihai1, ZHANG Lei1,2.& WANG Jianguo3.. Institute of Mechanics, Chinese academy of {2., beijing 100080, China 2. {3. school, Chinese academy of {2., beijing 100060, China 3. Tropical Marine Science Institute, National University of Singapore, 10 Kent Ridge Crescent, Singapore 1192.0 Chinese Acad Sci Inst Mech Beijing 100080 Peoples R China Chinese Acad Sci Grad Sch Beijing 100060 Peoples R China Natl Univ Singapore Trop Marine Sci Inst Singapore 119260 Singapore

When the sliding mass contains impervious bed, rainfall can infiltrate into mountain via crevices and form higher artesian aquifer at impervious bed inferior. This will decrease slip resistance and increase sliding forces of the sliding mass, thus lowering the safety factor, and inducing landslide disasters. In this paper, a landslide experimental apparatus is designed for experimental studies on the mechanism of this type of landslides. Meanwhile, the non-dimensional parameters in the model experiment are taken into account using dimensional analysis. The experimental results show that (1) the ratio of the cleft water pressure to the overlying pressure is a crucial parameter affecting the stability of the slope; (2. when the shut-in pressure reaches 80% of the normal component of the pressure on the slip surface made up of rock and soil, landslide will occur; (3. the whole slope will start to slide when the shut-in pressure is equal to the normal component of the pressure formed by the overlying rock and soil on the upper 3.% area. In this article, a discrete element method simulation is used to investigate the influence of cleft water pressure and shearing strength on the landslide stability. It can be concluded that the critical value of Ccr, ?cr, which determines the slide mass stability, increases with the increase of the water pressure; if the water pressure reaches a high level, the stability of the slide mass depends mainly on C, while the influence of ? becomes smaller than C.

关键词： impervious bed, rainfall infiltration, pore water pressure, landslide experiment, displacement monitor, discrete element method.

Chronology of Holocene lacustrine sediments in Co Ngoin, central Tibetan Plateau

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Science China Earth sciences 2006年第9期49卷 991-1001页

作者： WU Yanhong1, WANG Sumin1& HOU Xinhua1,3.1. Key Laboratory of Lake Sedimentation and Environment, Nanjing Institute of Geography and Limnology, Chinese academy of {2., Nanjing 2.0008, China 2. Institute of Tibetan Plateau Research, Chinese academy of {2., beijing 10085, China 3. graduate University of Chinese academy of {2., beijing 10003., China 1. Key Laboratory of Lake Sedimentation and Environment Nanjing Institute of Geography and Limnology Chinese Academy of Sciences Nanjing 210008 China 2. Institute of Tibetan Plateau Research Chinese Academy of Sciences Beijing 10085 China 3. graduate University of Chinese {2. of sciences Beijing 100039 China

Chronology is the basis for using lacustrine sediments to reconstruct the history of en-vironmental change. Radioactive-nuclides such as 14C, 2.0Pb and 13.Cs dating are mainly used to establish the chronology for recent several ten thousand years. Because of being mixed with “dead carbon”, the measured 14C age is always older than the actual age which is recognized as “reservoir effect”. Cs is a kind of active metal element, and easy to migrate vertically in the sediment that leads to the error of the time marker. 2.0Pb dating should make sure to select CIC model or CRS model. On the Tibetan Plateau, most of the lakes are alkaline closed lake where Cs is more moveable in the sediment and the reservoir effect caused by “dead carbon” on 14C dating is stronger. Based on the analysis on results of 14C, 2.0Pb and 13.Cs of the lacustrine sediments from Co Ngoin, central Tibetan Plateau, we use the simple regression method to re-calculate the 14C calendar ages, and establish the time sequence for cores CE-1 and CE-2.with result of 2.0Pb CRS model for the upper 3. cm and re-calculated 14C calendar age for sediments bellow 3. cm. Since 1400 cal. a BP, sedimentation inter-rupted for more than 1000 years. According to this time sequence, variations of environmental proxies confidently reflect the major climatic events in Holocene.

关键词： 14C, 2.0Pb and 13.Cs, chronology, lacustrine sediments, climatic event, Co Ngoin, central Tibetan Plateau.

Study on growth and properties of novel γ-LiAlO_2.substrate

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Science China(Technological sciences) 2006年第2期49卷 188-193页

作者： ZOU Jun1,2. ZHOU Shengming1, XU Jun1 & ZHANG Rong3.1. Shanghai Institute of Optics and Fine Mechanics, Chinese academy of {2., Shanghai 2.1800, China 2. graduate {3. of Chinese academy of {2., beijing 10003., China 3. Laboratory of Solid State Microstructures and Department of Physics, Nanjing University, Nanjing 2.0093. China 1. Shanghai Institute of Optics and Fine Mechanics Chinese Academy of Sciences Shanghai 201800 China 2. graduate school of Chinese {2. of {3. Beijing 100039 China 3. Laboratory of Solid State Microstructures and Department of Physics Nanjing University Nanjing 210093 China

Transparent γ-LiAlO2.single crystal has been grown by Temperature Gradient technique. The surface of the wafer annealed in O2.atmosphere at 1100°C for 70 h became opaque and Li-poor phase (LiAl5O8); while, that annealed in Li-rich atmosphere kept transparent and smooth. The full-width at half maximum value dropped to 3. arcsecs when the wafer was annealed in Li-rich atmosphere. That annealed in O2.atmosphere increased to 78 arcsec. Compared with absorption spectra, we can conclude that the 196 nm absorption peak was caused by Li vacancies and the 73. nm peak was caused by O vacancies.

关键词： γ-LiAlO2 crystal, scanning electron micrograph (SEM), absorption spectra.

Strong decays of N~*(153.) in an extended chiral quark model

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Science China(Physics,Mechanics & Astronomy) 2009年第10期52卷 1452-1457页

作者： AN ChunSheng1,2.3.& ZOU BingSong1,2.3.1 Institute of High Energy Physics,Chinese {2. of sciences,beijing 100049,China 2.Theoretical Physics Center for Science Facilities,Chinese {2. of sciences,beijing 100049,China 3.graduate University of Chinese {2. of sciences,beijing 100049,China Institute of High Energy Physics Chinese Academy of Sciences Beijing 100049 China Theoretical Physics Center for Science Facilities Chinese Academy of Sciences Beijing 100049 China graduate University of Chinese academy of {2. Beijing 100049 China

The strong decays of the N*(153.) resonance are investigated in an extended chiral quark model by including the low-lying $ qqqq\bar q $ components in addition to the qqq component. The results show that these five-quark components in N*(153.) contribute significantly to the N*(153.) → Nπ and N*(153.) → Nη decays. The contributions to the Nη decay come from both the lowest energy and the next-tolowest energy five-quarks components, while the contributions to the Nπ decay come from only the latter one. Taking these contributions into account, the description for the strong decays of N*(153.) is improved, especially for the puzzling large ratio of the decays to Nη and Nπ.

关键词： N*(153.) strong decays five-quark components