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Carbon isotope composition of the Lower Triassic marine carbonates, Lower Yangtze Region, South china

science china Earth sciences 2006年第3期49卷 225-241页

作者： ZUO Jingxun1,2, TONG Jinnan3. QIU Haiou4.& ZHAO Laishi3.1. Nanjing Institute of Geology and Palaeontology, Chinese Academy of sciences, Nanjing 210008, china 2. Henan Institute of Geological Survey, Zhengzhou 4.0007, china 3. State Key Laboratory of Geological Processes and Mineral Resources at{3., wuhan 4.0074. china 4. faculty of Material sciences and chemical engineering,{3., wuhan 4.0074. china 1. Nanjing Institute of Geology and Palaeontology Chinese Academy of Sciences Nanjing 210008 China 2. Henan Institute of Geological Survey Zhengzhou 450007 China 3. State Key Laboratory of Geological Processes and Mineral Resources at china university of geosciences Wuhan 430074 China 4. faculty of Material sciences and chemical {3. China University of Geosciences Wuhan 430074 China

Studies on three Lower Triassic sections located on the shallow water platform, the deep water slope and in the deep water basin in the Lower Yangtze Region, South china, show the similar trend of carbon isotope evolution. Biostratigraphic correlations among the Lower Triassic sections on the basis of standard conodont zones indicate that three negative shifts occurred in the Griesbachian, the Smithian and the late Spathian stages respectively, and one distinctly positive shift occurred in the early Spathian stage. Trend of carbon isotope evolution of the Lower Triassic reflects some significant changes in the global carbon cycle. Moreover, δ 13. background values are intensively controlled by palaeogeographic environment. In general, δ 13. values from deep-water slope carbonates are lighter than those from carbonate platform and heavier than those from deep-water basin carbonates. The positive carbon isotope excursion may be induced by a significant amount of organic carbon burial in marine sediments and increase in primary productivity. The large negative carbon isotope excursions during the Early Triassic in Lower Yangtze Region are interpreted to relate to volcano eruptions based on tuffaceous claystone interlayers observed near the Permian-Triassic boundary, the Induan- Olenekian boundary and the Lower Triassic-Middle Triassic boundary.

关键词： Lower Triassic, carbon isotope compositions, palaeogeography, volcanic eruptions, Lower Yangtze Region.

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Experimental study of ore gabbro liquid immiscibility

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science china Earth sciences 2005年第4期48卷 496-505页

作者： SANG Zunan1,2, XIA Bin1, ZHOU Yongsheng3.& JIN Zhenmin4.1. Guangzhou Institute of Geochemistry, Chinese Academy of sciences, Guangzhou 51064., china 2. wuhan {3., wuhan 4.0}072, china 3. Institute of Geology, china Seismological Bureau, Beijing 100029, china 4. faculty of Earth sciences, china university of geosciences,{14. 1. Guangzhou Institute of Geochemistry Chinese Academy of Sciences 510640 Guangzhou China 2. wuhan university 430072 Wuhan China 3. Institute of Geology China Seismological Bureau 100029 Beijing China 4. faculty of Earth sciences China University of Geosciences 430074 Wuhan China

In this paper, the authors present the results of a preliminary experimental study on partial melting of fine-grained gabbro, Panzhihua, Sichuan Province, china. Experiments were conducted under (confining) pressure ranging from 4.0 to 500 MPa and temperature of 900— 1200℃. The results show that the initial melt is distributed along grain boundaries and triple junctions. Liquid immiscibility phenomena are noted in the melt with two compositional different melt phases, i.e. matrix and sphere phases. The matrix phase is relatively rich in Si, Al and K, and is depleted in Mg, Fe, Ca, Na and Ti, whereas the sphere phase shows opposite trends. The calculation of the melt free energy indicates that the liquid immiscibility is governed by the rule of thermodynamics, as the liquid immiscibility would result in the decrease in free energy of the melt system. The field relationships suggest that the liquid immiscibility may have played an important role in the generation of ore magma of Panzhihua V-Ti magnetite ore deposit. This study thus provides experimental constraints on the mechanism of the formation of V-Ti magnetite deposite.

关键词： partial melting, experimental study, gabbro, liquid immiscibility, ore formation mechanism.

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Transport network and flow mechanism of shallow ore-bearing magma in Tongling ore cluster area

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science china Earth sciences 2006年第4期49卷 397-407页

作者： DENG Jun1,2, WANG Qingfei1,2 , HUANG Dinghua3., WAN Li4. YANG Liqiang1,2 & GAO Bangfei1,2 1. State Key Laboratory of Geological Processes and Mineral Resources, china university of geosciences, Beijing 100083. china 2. Key Laboratory of Lithosphere Tectonics and Lithoprobing Technology of Ministry of Education, china {3. of Geo- sciences, Beijing 100083. china 3. faculty of Earth sciences, china university of geosciences, wuhan 4.0074. china 4. School of Mathematics and Information science, Guangzhou {3., Guangzhou 5104.5, china 1. State Key Laboratory of Geological Processes and Mineral Resources China University of Geosciences Beijing 100083 China 2. Key Laboratory of Lithosphere Tectonics and Lithoprobing Technology of Ministry of Education China University of Geosciences Beijing 100083 China 3. faculty of Earth sciences China University of Geosciences Wuhan 430074 China 4. School of Mathematics and Information science Guangzhou University Guangzhou 510405 China

Abundant studies revealed that shallow intrusions of the Yanshanian epoch resulted in the mass mineralization of the Tongling region. Various evidences showed there existed a concealed magma chamber at ?10 km depth in the middle part of this region during Yanshanian epoch, from which the ore-forming magma was generated and then transported to the superficial layer. Yet the transport network and flow mechanism of the shallow ore-bearing magma, the key problem associ- ated with ore-forming process, was relatively little focused on. Integrate analysis of structural me- chanics, statistical fractal and geological facts suggested that NE trending high-angle fold-related thrust faults and the tessellated basement ones served as the main pathways for the shallow magma’s transporting, moreover, the saddle void spaces among adjacent strata in the folds upon this fault system provided the place for magma’s emplacement. So the folds in the upper part and faults in the lower part of the upper crust constituted the fluid’s transport and emplacement network. During the deformation of geologic body with multi-layer structure, the layers in the upper part tended to fold when received the jacking stress from the lower part, while the lower one inclined to fault undergoing loads of the upper part. And the producing probability of this structure assemblage was highly in- creased in the condition, such as in the Tongling area, that the mechanic rigidity of the lower layers was stronger than that of the upper ones. For the pre-existence of fluid-conducting network, the top magma with high volatile in the magma chamber transported rapidly to the superficial layer in dyking pattern, located in the void spaces of folds, filled and reconstructed them. The sudden drop of pres- sure caused the fluid unmixing from the magma and mass ore-forming elements concentration. Pulse activity of the dyking may be the principal reason why magmatic bodies in the Tongling area were spatially-temporally con

关键词： Tongling, structural network, magma intrusion, fractal, dyke.

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Synthesis and photochromic properties of WO_3.powder induced by oxalic acid

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science china Chemistry 2009年第5期52卷 609-614页

作者： SHEN Yi1, ZHU Hua1, HUANG Rong1, ZHAO Li2 & YAN ShaNing1 1 faculty of Material science and chemical {3.,{4., wuhan 4.0074. china 2 faculty of Materials science and {3., Hubei university, wuhan 4.3}062, china 1. faculty of Material science and chemical {3. China University of Geosciences Wuhan 430074 China 2. faculty of Materials science and engineering Hubei University Wuhan 430062 China

Tungsten trioxide powder with the novel morphology was prepared via the hydrothermal method with oxalic acid as the organic inducer, the structure and shape of which were detected by X-ray diffraction (XRD), scanning electron microscopy (SEM) and BET. Furthermore, photochromic properties of the as-prepared powder samples were tested by an ultraviolet-visible spectrophotometer combined with a color difference meter. The corresponding results indicated that the induced product was still hexagonal WO3. made up of regularly spindle particles with 200-3.0 nm in length and 3.-50 nm in width. The ratio of the length and width was from 4.to 10. Moreover, the special morphology improved its absorptive capacity to the excitation light source, resulting in its high photochromic properties.

关键词： WO3 powder photochromism oxalic acid organic inducer

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Relationships between bacterial-algal proliferating and mass extinction in the Late Devonian Frasnian-Famennian transition:Enlightening from carbon isotopes and molecular fossils

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science china Earth sciences 2005年第10期48卷 1656-1665页

作者： GONG Yiming1,2, XU Ran1, TANG Zhongdao1, SI Yuanlan3.& LI Baohua4.1. faculty of Earth science and State Key Laboratory of Geological Processes and Mineral Resources, china university of geosciences,{3. 2. Institute of Resources & Environments, Henan Polytechnic university, Jiaozuo 4.4.03. china 3. Department of Computer science, South-Central university for Nationalities,{3. 4. Laboratory of Marine Geology, Tongji university, Shanghai 200092, china faculty of Earth science and State Key Laboratory of Geological Processes and Mineral Resources china university of geosciences {3. {4. Institute of Resources & Environments Henan Polytechnic university Jiaozuo china Department of Computer science South-Central university for Nationalities wuhan {3. Laboratory of Marine Geology Tongji university Shanghai china

Studies show positive shifts of inorganic and organic carbon isotope values (δ 13.carb and δ 13.kerogen) from +0.4.0}(‰ V-PDB) to +3.54.(‰ V-PDB) and from ?29.3. (‰ V-PDB) to ?24.14.(‰ V-PDB), respectively, B* (Ba* = Ba/ (Al2O3.X 15%)) values from 0.015 to 0.14., TOC values from 0.02% to 0.21%, V/Cr values from 0.3.to 2.0, Sr/Ba values from 3.20 to 4..50 in the Late Devonian Frasnian Upper rhenana zone to the top linguiformis zone of the Yangdi sec-tion deposited in carbonate slope facies of Guilin, Guangxi, South china, which indicates that biomass, productivity, organic carbon burial and salinity increase and that oxygenation near the boundary between sediments and waters decreases from the Late Devonian Frasnian Upper rhenana zone to the top linguiformis zone. Abundance of molecular fossils increases and normal alkanes, isoprenoid hydrocarbon, terpanes and steranes are dominated from the Late Devonian Frasnian to the bottom of Famennian, which shows that the predecessors of molecular fossils of the Frasnian-Famennian (F-F) transition are dominated by marine phytoplankton, zooplankton and benthic bacteria with no photosynthesis. Therefore, it is considered that the F-F transitional mass extinction with a multistage, selection and global synchronizing was caused by bacte-rial-algal proliferating, continuing deterioration of the shallow marine ecoenvironment of the mid-dle-lower latitudes. A simple cause and effect chain can be expressed as: appearance of seed plants and multi-storied forests → enhanced chemical and biochemical weathering and pe-dogenesis → wide development of soils → increasing riverine nutrient fluxes in epicontinental sea → from superoligotrophic to eutrophic in epicontinental sea → proliferating of marine phyto-plankton and zooplankton → frequent red tide and anoxia → mass extinction of shallow marine organisms in the middle-lower latitudes. It is worth notice that the factor drawdown of atmos-pheric Pco2, climatic cooling and sea level falling c

关键词： mass extinction, bacteria-algae, carbon isotopes, molecular fossils, biodiversity, Late Devonian, Guangxi, South china.

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Analytical method of Cr stable isotope and its application to water pollution survey

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Chinese science Bulletin 2010年第7期55卷 664-669页

作者： GAO YongJuan 1,2,3.MA Teng 4.5,LING WenLi 1,2,LIU CunFu 4.5 & LI Li 4.5 1faculty of Earth science,china {3. of geosciences,wuhan 4.0074.china 2State Key Laboratory of Geological Processes and Mineral Resources,china {3. of geosciences,wuhan 4.0074.china 3.Graduate School,china {3. of geosciences,wuhan 4.0074.china 4.Biogeological and Environmental Geology Laboratory of Ministry of Education(china {3. of geosciences) ,wuhan 4.0074.china 5 Sino-Hungary Joint Laboratory of Environmental sciences and Health,china {3. of geosciences,wuhan 4.0074.china faculty of Earth science China University of Geosciences Wuhan 430074 China State Key Laboratory of Geological Processes and Mineral Resources China University of Geosciences Wuhan 430074 China Graduate School China University of Geosciences Wuhan 430074 China Biogeological and Environmental Geology Laboratory of Ministry of Education (china university of geosciences) Wuhan 430074 China Sino-Hungary Joint Laboratory of Environmental sciences and Health China University of Geosciences Wuhan 430074 China

High Cr(VI) concentration is a potential serious risk to environment and ecologic ***,it is essential to effectively monitor Cr contamination in water systems and scientifically evaluate its evolution trend.A new method of in-situ tracer technique by Cr isotopic analysis for quantitatively estimating Cr-contamination and its regional evolution in natural waters as well as a case application are reported in this *** on documented literatures,an experimental procedure for chemical separation and purification of Cr in water samples and its analytical method for Cr isotopic measurement by thermal ionization mass spectrometry(TIMS) are *** samples collected around a chemical factory in Hubei Province were analyzed by this *** samples showδ53.r values ranging from-1.7‰to 7.3.and an elevating trend with an increasing in distance from the sampling site to pollution source.A functional correlation following Rayleigh fractionation law was established between sample'sδ53.r value and its extent of Cr *** study suggests that Cr isotopic analysis is an effective method to reveal the spatial distribution and its evolution trend of Cr contamination in the regional water *** is thus helpful to assessing the self-purifying ability of local water system according to Cr isotopic fractionation.

关键词：铬(VI) 水污染调查稳定同位素应用同位素分析供水系统演变趋势示踪技术

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Synthesis and photoluminescence property of red phosphors LiEu_(1-x)Y_x(WO_4._(0.5)(MoO_4._(1.5) for white LED

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science china(Technological sciences) 2009年第7期52卷 1913-1918页

作者： XIE An, YUAN XiMing, WANG JuanJuan & WANG Feng engineering Research Center of Nano-Mineral Materials and Application, Ministry of Education, faculty of Materials science and {3. engineering, china university of geosciences, wuhan 4.0074. china 1. engineering Research Center of Nano-Mineral Materials and Application Ministry of Education Faculty of Materials Science and Chemical Engineering China University of Geosciences Wuhan 430074 China

A series of novel red phosphors LiEu1-xYx(WO4.0.5(MoO4.1.5 (x=0, 0.1, 0.2, 0.3. 0.4. 0.5, 0.6, 0.8) were synthesized by conventional solid state reaction method with the starting materials: WO3. MoO3. Eu2O3. Li2CO3.and Y2O3. The spectrum and the crystal structure of the phosphors were characterized by F-4.00 and XRD respectively. Meanwhile the effects of flux and Y3. concentration on the crystal structure and luminescent properties of the phosphors were investigated. The results showed that the optimal content of flux (WAlF3.WH3.O3.1/1) was 1 wt% and the optimal doping concentration of Y3. was 0.5 mol. The emission spectrum showed the most intense peak was located at 615 nm, which corresponds to the 5D0→7F2 transition of Eu3. and that Eu3. occupied the lattice site of noncentrosymmetric environment in the scheelite phases. The excitation spectrum displayed that these phosphors could be effectively excited by ultraviolet (UV) (3.6 nm) and blue (4.6 nm) light, nicely in correspondence with the widely ap- plied output wavelengths of ultraviolet or blue LED chips. The influence of flux on the luminescent properties of LiEu0.5Y0.5(WO4.0.5(MoO4.1.5 phosphor was analyzed. The XRD spectra indicated that the flux could help to crystallize the phosphor, and no other phases were formed except the tetragonal. When adding flux, the relative intensity of LiEu0.5Y0.5(WO4.0.5(MoO4.1.5 became much stronger and the average particle size of the phosphor decreased.

关键词： red emitting phosphor LiEu1-xYx(WO4.0.5(MoO4.1.5 flux white LED

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Distributions of fatty acids in a stalagmite related to paleoclimate change at Qingjiang in Hubei,southern china

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science china Earth sciences 2005年第9期48卷 1463-1469页

作者： XIE Shucheng1,HUANG Junhua1,WANG Hongmei2,YI Yi1,HU Chaoyong1, CAI Yanjun3.& CHENG Hai4.1. faculty of Earth science,china {3. of geosciences,wuhan 4.0074.china 2. School of Environmental Studies,china {3. of geosciences,wuhan 4.0074.china 3. SKLLQG,Institute of Earth Environment,Chinese Academy of sciences,Xi’an 710075,china 4. Department of Geology and Geophysics,{3. of Minnesota,MN554.5,USA 1. faculty of Earth science China University of Geosciences 430074 Wuhan China 2. School of Environmental Studies China University of Geosciences 430074 Wuhan China 3. SKLLQG Institute of Earth Environment Chinese Academy of Sciences 710075 Xi’an China 4. Department of Geology and Geophysics University of Minnesota 55455 MN USA

Fatty acids extracted from a subtropical stalagmite at Qingjiang in Southern china’s Hubei Province were analysed using gas chromatography-mass spectrometry. These n-alkanoic acids range from C14.to C26 in carbon number, maximizing at C16, with a second dominance at C22. In contrast to the stalagmite analysed, the overlying soils are characterized by the dominance of heavy-molecular-weight homologues (>C20). The n-fatty acids in the stalagmite were proposed to be contributed by both the soil ecosystems and the microbes harboring in the percolating water and the cave. The ratios of unsaturated to saturated n-fatty acids (C16:1i/C16:0, C18:1/C18:0) appear to show trends comparable with the oxygen isotope records of the stalagmite carbonate, with enhanced values associated with the cold episode such as Heinrich event 1. This paleoclimate-dependent record of the n-fatty acids might reflect microbial changes in physiology and activity in response to the temperature. This record shows somewhat difference from the previous paleoclimate signal extracted from n-alkanols and n-alkan-2-ones of the same stalagmite. The acid record fails to document the well-known Younger Dryas event which was effectively shown by the latter two biomarkers derived from soil ecosystems. This discrepancy might result from the changing biogeochemical impact on different lipid fractions as well as the varied organism populations in different ecosystems.

关键词： biomarker, ecosystem, microbe, speleothem, paleoclimate, Quaternary.

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Indian Ocean-MORB-type isotopic signature of Yushigou ophiolite in North Qilian Mountains and its implications

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science china Earth sciences 2006年第6期49卷 561-572页

作者： HOU Qingye1,2, ZHAO Zhidan1,2, ZHANG Hongfei3. ZHANG Benren3.& CHEN Yuelong2 1. State Key Laboratory of Geological Processes and Mineral Resources, china university of geosciences, Beijing 100083. {4. 2. School of Earth science and Mineral Resources, china university of geosciences, Beijing 100083. {4. 3. faculty of Earth sciences, china university of geosciences, wuhan 4.0074. china 1. State Key Laboratory of Geological Processes and Mineral Resources China University of Geosciences Beijing 100083 China 2. School of Earth science and Mineral Resources China University of Geosciences Beijing 100083 China 3. faculty of Earth sciences China University of Geosciences Wuhan 430074 China

In order to explore the disputed issue concerning the tectonic affinity ofthe ancient ocean mantle of North Qilian Mountains (NQM), geochemical and Sr, Nd, Pb isotopiccompositions of pillow basalts of the Yushigou Ophiolite (YSGO) suite from NQM have been analyzedsystematically. The pillow basalts exhibit tholeiitic characteristics, with flatchondrite-normalized REE patterns ((La/Yb)_N = 0.98—1.27). They display no Nb, Ta, Zr, Hf negativeanomalies, and show MORB features in 2Nb-Zr/4.Y and Ti/100-Zr-YX3.tectonic discrimination *** results indicate that the Yushigou ophiolite is most likely to be formed in a mid-ocean ridgeor mature back-arc basin. Their isotopic data show a relatively broad and enriched ^(87)Sr/^(86)Sr(0.70509 — 0.70700), restricted ^(14.1}Nd/^(14.)Nd (0.512955-0.512978). Pb isotopes are in the rangeof ^(206)Pb/^(204.Pb (18.054.20.562), ^(207)Pb/^(204.Pb (15.53.-15.74.1} and ^(208)Pb/^(204.Pb(3..068-3..53.). These isotopic data imply that the basalts originated from the depleted mantle(DMM), with the involvement of enriched mantle components (mainly EMII). Geochemical comparisonsbetween the basalts in YSGO and the MORB-type basalts of ophiolite suites occurring in the knownancient Tethyan tectonic domain indicate that the ancient oceanic mantle represented by YSGO suiteforming in early Paleozoic in the North Qilian Moutains is very similar to the Tethyan mantle inboth trace elements and isotopic compositions. The North Qilian Mountains should be a part of theTethyan tectonic domain in early Paleozoic. This further implies that the Tethyan tectonic domaincan be deduced to early Paleozoic in the study area, which will be helpful to discussing thetectonic affinity and evolution of the North Qilian Mountains.

关键词： geochemistry, Indian Ocean-MORB-type isotopic signatures, Tethyan tectonic domain, Yushigou ophiolite, North Qilian Mountains.

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On-line parallel reversed phase two-dimensional liquid chromatography for high-throughput analysis of complex proteomic samples

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science china Chemistry 2006年第6期49卷 527-533页

作者： WANG Zhicong1,3. ZHANG Qinghe2, LI Tong2, ZHAO Zhongyi3.& ZHANG Weibing1 1. Dalian Institute of chemical Physics, Chinese Academy of sciences, Dalian 116011, {4. 2. Dalian Elite Analytical Instrument Co., Ltd., Dalian 116011, {4. 3. faculty of Material science and chemical engineering, china university of geosciences, wuhan 4.0074. china 1. Dalian Institute of chemical Physics Chinese Academy of Sciences Dalian 116011 China 3. faculty of Material science and chemical {3. China University of Geosciences Wuhan 430074 China 2. Dalian Elite Analytical Instrument Co. Ltd. Dalian 116011 China

A comprehensive two-dimensional liquid chromatographic system (2D SCX/RP) is con- structed with a 10-port-2-way valve using strong cation exchange chromatography (Hypersil SCX, 100 mm×4.6 mm I.D.) followed by reversed phase chromatography (Hypersil BDS C18, 15 mm×4.6 mm I.D.) to separate the complex peptides from globin peptic hydrolysate. After the sample was loaded on the SCX column, the phosphate buffer (pH 4.0) was used to elute the peptides. Then, elutes flowed through the interface and the peptides focused on the head of the trapping columns (Hypersil BDS C18, 15 mm×4.6 mm I.D.) but salt passed into the waste. After the valve was switched, the samples were flushed with a backward flow into the RP analytical column. The peptides on the SCX were eluted with 12 discontinuous steps linearly increasing salt concentrations. The peptides enriched on the trapping column were desalted and separated by the RP columns. The resolution and the resolved peaks of the 2D SCX/RP system were greatly increased and the total peak capacity reached as high as 2280.

关键词： two-dimensional liquid chromatography, interface, trapping column, proteomics, globin.

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