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Analytical method of Cr stable isotope and its application to water pollution survey

Chinese Science Bulletin 2010年第7期55卷 664-669页

作者： GAO YongJuan 1,2,3.MA Teng 4,5,LING WenLi 1,2,LIU CunFu 4,5 & LI Li 4,5 1Faculty of Earth Science,china university of geosciences,{3. 43.074,china 2State Key Laboratory of Geological Processes and Mineral Resources,china university of geosciences,{3. 43.074,china 3.Graduate School,china university of geosciences,{3. 43.074,china 4 Biogeological and Environmental Geology Laboratory of Ministry of Education(china university of geosciences) ,{3. 43.074,china 5 Sino-Hungary Joint Laboratory of Environmental Sciences and Health,china university of geosciences,{3. 43.074,china Faculty of Earth Science China University of Geosciences Wuhan 430074 China State Key Laboratory of Geological Processes and Mineral Resources China University of Geosciences Wuhan 430074 China Graduate School China University of Geosciences Wuhan 430074 China Biogeological and Environmental Geology Laboratory of Ministry of Education (china university of geosciences) Wuhan 430074 China Sino-Hungary Joint Laboratory of Environmental Sciences and Health China University of Geosciences Wuhan 430074 China

High Cr(VI) concentration is a potential serious risk to environment and ecologic ***,it is essential to effectively monitor Cr contamination in water systems and scientifically evaluate its evolution trend.A new method of in-situ tracer technique by Cr isotopic analysis for quantitatively estimating Cr-contamination and its regional evolution in natural waters as well as a case application are reported in this *** on documented literatures,an experimental procedure for chemical separation and purification of Cr in water samples and its analytical method for Cr isotopic measurement by thermal ionization mass spectrometry(TIMS) are *** samples collected around a chemical factory in Hubei Province were analyzed by this *** samples showδ53.r values ranging from-1.7‰to 7.3.and an elevating trend with an increasing in distance from the sampling site to pollution source.A functional correlation following Rayleigh fractionation law was established between sample'sδ53.r value and its extent of Cr *** study suggests that Cr isotopic analysis is an effective method to reveal the spatial distribution and its evolution trend of Cr contamination in the regional water *** is thus helpful to assessing the self-purifying ability of local water system according to Cr isotopic fractionation.

关键词：铬(VI) 水污染调查稳定同位素应用同位素分析供水系统演变趋势示踪技术

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Mechanical Research on Biucleus-Type Vortex Structures

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Acta Geologica Sinica(English Edition) 1990年第4期64卷 345-362,462页

作者： Zeng Zuoxun Section of Geomechanics, china university of geosciences, {3., Hubei Fei Zhenbi Section of Geomechanics China University of Geosciences Wuhan Hubei

A new type of vortex structure-binucleus-type vortex structure-is presented in this paper. It is charac-terized by two nuclear columns which distinguish it from uninuclcus-type vorlex structure. The vortical sur-faces of the structure are commonly s-shaped and reversed s-shaped and subordinately of clliptic andhyperbolic shape. and sometimes turbine-like surfaces are observed. On the basis of field structural studies. a mechanical model of rotation around a binuclear column ofcrustal materials is presented in the paper. Burgers viscoelastic solutions of the stress field and deformationfield of this structural type have been obtained using the principle and method of rheology. and simulation ex-periments have been performed. The results of the theoretical calculation and experiments indicate that theproposed mechanical model is applicable.

关键词： Mechanical Research on Biucleus-Type Vortex Structures

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Carbon isotope composition of the Lower Triassic marine carbonates, Lower Yangtze Region, South china

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Science china Earth Sciences 2006年第3期49卷 225-241页

作者： ZUO Jingxun1,2, TONG Jinnan3. QIU Haiou4 & ZHAO Laishi3.1. Nanjing Institute of Geology and Palaeontology, Chinese Academy of Sciences, Nanjing 210008, china 2. Henan Institute of Geological Survey, Zhengzhou 450007, china 3. State Key Laboratory of Geological Processes and Mineral Resources at china {3. of geosciences, wuhan 43.074, china 4. Faculty of Material Sciences and Chemical Engineering, china {3. of geosciences, wuhan 43.074, china 1. Nanjing Institute of Geology and Palaeontology Chinese Academy of Sciences Nanjing 210008 China 2. Henan Institute of Geological Survey Zhengzhou 450007 China 3. State Key Laboratory of Geological Processes and Mineral Resources at china university of geosciences Wuhan 430074 China 4. Faculty of Material Sciences and Chemical Engineering China University of Geosciences Wuhan 430074 China

Studies on three Lower Triassic sections located on the shallow water platform, the deep water slope and in the deep water basin in the Lower Yangtze Region, South china, show the similar trend of carbon isotope evolution. Biostratigraphic correlations among the Lower Triassic sections on the basis of standard conodont zones indicate that three negative shifts occurred in the Griesbachian, the Smithian and the late Spathian stages respectively, and one distinctly positive shift occurred in the early Spathian stage. Trend of carbon isotope evolution of the Lower Triassic reflects some significant changes in the global carbon cycle. Moreover, δ 13. background values are intensively controlled by palaeogeographic environment. In general, δ 13. values from deep-water slope carbonates are lighter than those from carbonate platform and heavier than those from deep-water basin carbonates. The positive carbon isotope excursion may be induced by a significant amount of organic carbon burial in marine sediments and increase in primary productivity. The large negative carbon isotope excursions during the Early Triassic in Lower Yangtze Region are interpreted to relate to volcano eruptions based on tuffaceous claystone interlayers observed near the Permian-Triassic boundary, the Induan- Olenekian boundary and the Lower Triassic-Middle Triassic boundary.

关键词： Lower Triassic, carbon isotope compositions, palaeogeography, volcanic eruptions, Lower Yangtze Region.

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Petrogenesis and dating of the Kangding complex,Sichuan Province

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Science china Earth Sciences 2005年第5期48卷 622-634页

作者： CHEN Yuelong 1 , LUO Zhaohua 1 , ZHAO Junxiang, LI Zhihong, ZHANG Hongfei & SONG Biao 3.1. Faculty of Earth Sciences and Natural Resources, china university of geosciences, Beijing 100083. china 2. Faculty of Earth Sciences, china university of geosciences, wuhan 43.074, china 3. Beijing SHRIMP Center, Institute of Geology, Chinese Academy of Geological Sciences, Beijing 10003., china 1. Faculty of Earth Sciences and Natural Resources China University of Geosciences 100083 Beijing China 2. Faculty of Earth Sciences China University of Geosciences 430074 Wuhan China 3. Beijing SHRIMP Center Institute of Geology Chinese Academy of Geological Sciences 100037 Beijing China

An analysis of major and trace element geochemistry and SHRIMP U-Pb zircon dating of mafic, intermediate, and felsic rocks from the Mianning metamorphic complex of Si- chuan Province was conducted. One of our conclusions is that a majority of the zircons crystal- lized between 721 and 773.Ma in a magmatic regime. The complexes contain early to late Pa- leo-proterozoic relict zircons from ancient continental crust. The oldest age, 2468 Ma, may rep- resent the basement of the Yangtze block. Overgrowth zircon rims and palingenetic zircons have been observed and dated, and are believed to have formed after crystallization, during Paleozoic and Mesozoic metamorphic-anatexis. We also conclude that depletion of Nb, Ta, HREE, in a spider-diagram normalized to primitive mantle and calc-alkaline association, implies that they formed in island-arc or under-plating settings.

关键词： Kangding complex, zircons, SHRIMP, tectonic setting.

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Geothermal and fluid flowing simulation of ore-forming antimony deposits in Xikuangshan

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Science china Earth Sciences 2006年第8期49卷 862-871页

作者： YANG Ruiyan1,2, MA Dongsheng2, BAO Zhengyu3. PAN Jiayong2, CAO Shuanglin2 & XIA Fei2 1. School of Mathematics and Physics, china university of geosciences,{3., china 2. State Key Laboratory for Research of Mineral Deposits, Nanjing university, Nanjing 210093. china 3. Faculty of Earth Sciences, china university of geosciences,{3., china 1. School of Mathematics and Physics China University of Geosciences Wuhan 430074 China 2. State Key Laboratory for Research of Mineral Deposits Nanjing University Nanjing 210093 China 3. Faculty of Earth Sciences China University of Geosciences Wuhan 430074 China

The Xikuangshan Antimony Deposit located in the Mid-Hunan Basin, china, is the larg- est antimony deposit in the world. Based on the hydrogeological and geochemical data collected from four sections, Xikuangshan-Dajienao (AO), Xikuangshan-Dashengshan (BO), Xikuang- shan-Longshan (CO) and Dafengshan (DO) in the Basin, an advanced metallogenic model related to deep-cyclic meteoric water of Xikuangshan Antimony Deposit is put forward in this paper using a model of heat-gravity-driving fluid flow transportation. The simulation results show that the ore-forming fluid of the deposit mainly comes from the Dashengshan and Longshan areas where BO and CO sections are located if the overall basin keeps a constant atmospheric precipitation and infiltration rate during mineralization, and that the average transportation speed of the ore-forming fluids is about 0.2―0.4 m/a.

关键词： ore-forming fluid, numerical simulation, geothermal field, geofluid transport, Xikuangshan, antimony deposits.

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Evolutionary patterns of Productida (Brachiopoda) morphology during the Permian in South china

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Science china Earth Sciences 2008年第11期51卷 1589-1600页

作者： ZHANG Yang1 & HE WeiHong1,2 1 Faculty of Earth Sciences, china university of geosciences,{3., china 2 Key Laboratory of Biogeology and Environmental Geology of Ministry of Education, china university of geosciences,{3., china 1. Faculty of Earth Sciences China University of Geosciences Wuhan 430074 China 2. Key Laboratory of Biogeology and Environmental Geology of Ministry of Education China University of Geosciences Wuhan 430074 China

The evolutionary patterns of Productida (brachiopod) morphology throughout the Permian show that while the percentage proportion of Productida (brachiopod) with strongly concentric and radial ornamentation declined from the Cisuralian to the Guadalupian, and then increased towards the Changhsingian via Wuchiapingian, the percentage proportion of Productida (brachiopod) with fine concentric and radial ornamentation distinctly increased from the Cisuralian to the Guadalupian, slightly declined towards the Wuchiapingian, and then increased towards the Changhsingian. From the Cisuralian to the Changhsingian, the percentage proportion of brachiopods with spinose ornamentation shows a persistent declining trend. The shell size generally indicates a miniaturization trend at species level during the Wuchiapingian to Changhsingian (including the transitional bed). These evolutionary patterns of brachiopod ornamentation and size are possibly related to the anoxia, food shortage, sea-level fluctuation, and change of substrate in the Permian (including the Permian-Triassic transitional interval) in South china.

关键词： brachiopod ornamentation size Permian South china

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Comprehensive evaluation of mechanism of "chimney effect" using principles of magnetism, geochemistry and mineralogy

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Chinese Science Bulletin 1998年第9期43卷 743-748页

作者： LIU Qingsheng 1, CHENG Tongjin 2 and LIU Shugen 3.1. Department of Applied Geophysics, china university of geosciences,{3., china 2. Center of Petroleum Geochemistry, china National Star Petroleum Corporation, Hefei 23.022, china 3. The St Department of Applied Geophysics China University of Geosciences Wuhan China Center of Petroleum Geochemistry China National Star Petroleum Corporation Hefei China The State Key Laboratory of Oil/Gas Reservoir Geology and Exploitation of china Chengdu Institute of Technology Chengdu China

Study of forming mechanism of "chimney-effect" (CE) has important significance for basic theory and applications of non-seismic geophysical and geochemical methods locating oil/gas reservoirs. The theoretical basis of comprehensive evaluation of mechanism of CE using principles of magnetism, geochemistry and mineralogy has been reviewed, with the problems to be solved: (ⅰ) study for the relationship between process of oil/gas migration and geochemical field; (ⅱ) analysis of genesis of magnetic, geochemical and mineralogical anomaly; (ⅲ) interpretation of surface soil magnetism and geochemical anomaly combined with seismic data.

关键词： chimney effect (CE) hydrocarbon microseepage oil/gas accumulation.

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Sm-Nd and zircon SHRIMP U-Pb dating of Huilanshan mafic granulite in the Dabie Mountains and its zircon trace element geochemistry

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Science china Earth Sciences 2005年第12期48卷 2081-2091页

作者： HOU Zhenhui1, LI Shuguang1, CHEN Nengsong2, LI Qiuli1 & LIU Xiaoming3.1. School of Earth and Space Sciences, university of Science and Technology of china, Hefei 23.026, china 2. The Key Laboratory of Continental Dynamics of the Ministry of Education, Northwest university, Xi’an 710069, china 3. Faculty of Earth Sciences, china university of geosciences, wuhan 43.074, china 1. School of Earth and Space Sciences University of Science and Technology of China 230026 Hefei China 2. The Key Laboratory of Continental Dynamics of the Ministry of Education Northwest University 710069 Xi’an China 3. Faculty of Earth Sciences China University of Geosciences 430074 Wuhan China

The mafic granulites from Huilanshan are outcropped on the center of the Luotian dome in the northern Dabie Mountains. The Sm-Nd isochron defined by granulite-facies meta-morphic minerals (garnet + clinopyroxene + hypersthene) yields an age of 13. ± 18 Ma indicating the early Cretaceous granulite-facies metamorphism. The cathodoluminescence (CL) images of zircons from the granulite show clearly core-mantle-rim structures. The zircon cores are charac-terized by typical oscillatory zoning and highly HREE enriched patterns, which suggests their magma origin. Some zircon cores among them with little Pb loss give SHRIMP U-Pb ages rang-ing from 753.to 780 Ma, which suggests that the protolith of Huilanshan granulite is Neopro-terozoic mafic rocks. The zircon mantles usually cut across the oscillatory zone of the zircon cores have 3.10 times lower REE, Th, U, Y, Nb and Ta contents than the igneous zircon cores but have high common Pb contents. These characteristics suggest that they were formed by hydrothermal alteration of the igneous zircons. The part of zircon mantles with little Pb loss give a similar SHRIMP U-Pb age (716―780 Ma) to the igneous zircon cores, which implies that the hydrothermal events occurred closely to the magmatic emplacement. In view of the strong early Cretaceous magmatism in the Luotian dome, consequently, the Huilanshan mafic granulite was formed by heating of the Neoproterozoic mafic rocks in mid-low crust, which caused the granu-lite-facies metamorphism underneath the Dabie Mountains. The similarity between the granulite metamorphic age (13. ± 18 Ma) defined by Sm-Nd isochron and K-Ar age of 123.127 Ma given by amphible from the gneiss in Luotian dome suggests a rapid uplifting of the Luotian dome, which may result in further exhumation of the ultrahigh pressure metamorphic rocks in the Dabie Mountains.

关键词： Dabie orogen, granulite, zircon U-Pb ages, Sm-Nd age.

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The role of aerial algae in the formation of the landscape of the Yunnan Stone Forest,Yunnan Province, china

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Science china Earth Sciences 2004年第9期47卷 846-864页

作者： TIAN Youping1,3. ZHANG Jie2, SONG Linhua1 & BAO Haosheng2 1. Institute of Geographic Sciences and Natural Resources Research, Chinese Academy of Sciences, Beijing 100101, china 2. Department of Geography, Nanjing university, Nanjing 210093. china 3. School of Earth Sciences and Resources, china university of geosciences, Beijing 100083. china Institute of Geographic Sciences and Natural Resources Research Chinese Academy of Sciences Beijing 100101 China Department of Geography Nanjing University Nanjing 210093 China School of Earth Sciences and Resources China University of Geosciences Beijing 100083 China

Aerial algae on the surface of carbonate rocks at the Stone Forest, Shilin County, Yunnan Province, china, and their bioerosion were investigated in the field and studied in the laboratory in detail. Through the observation, identification and statistics of more than one hun- dred algal samples and rock samples with the optical microscopes (stereomicroscope, biological microscope) and the scanning electronic microscope (SEM), the relationships between erosional forms on the surface of the Stone Forest and algae and/or algal communities and the genetic mechanism for the formation of erosional forms were analyzed. It is suggested that aerial algae play an active role in bioerosive processes that may affect the formation of karst erosional forms. These effects include both direct and indirect ones. The direct effect is the initiative control (algal shape-controlling role) of algae on the formation of karst forms of various scales, mostly mi- cro-scale (3.) and minor-scale (10-3.10-1m) erosional forms. The algal shape-controlling roles can be divided into the algal individual shape-controlling role and the algal community shape-controlling role. The former mostly controls the formation of micro-scale erosional forms, while the latter mostly controls the formation of micro-scale and smaller minor-scale erosional forms. The indirect effect refers to the promoting role of algae in the formation of karst forms, which may affect the formation of karst forms of all types and scales. The bioerosion of algae accelerates the weathering process of the whole Stone Forest karst landforms.

关键词： aerial algae, bioerosion, the Stone Forest, Yunnan Province, china.

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Transport network and flow mechanism of shallow ore-bearing magma in Tongling ore cluster area

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Science china Earth Sciences 2006年第4期49卷 397-407页

作者： DENG Jun1,2, WANG Qingfei1,2 , HUANG Dinghua3., WAN Li4, YANG Liqiang1,2 & GAO Bangfei1,2 1. State Key Laboratory of Geological Processes and Mineral Resources, china university of geosciences, Beijing 100083. china 2. Key Laboratory of Lithosphere Tectonics and Lithoprobing Technology of Ministry of Education, china university of Geo- sciences, Beijing 100083. china 3. Faculty of Earth Sciences, china university of geosciences, wuhan 43.074, china 4. School of Mathematics and Information Science, Guangzhou university, Guangzhou 510405, china 1. State Key Laboratory of Geological Processes and Mineral Resources China University of Geosciences Beijing 100083 China 2. Key Laboratory of Lithosphere Tectonics and Lithoprobing Technology of Ministry of Education China University of Geosciences Beijing 100083 China 3. Faculty of Earth Sciences China University of Geosciences Wuhan 430074 China 4. School of Mathematics and Information Science Guangzhou University Guangzhou 510405 China

Abundant studies revealed that shallow intrusions of the Yanshanian epoch resulted in the mass mineralization of the Tongling region. Various evidences showed there existed a concealed magma chamber at ?10 km depth in the middle part of this region during Yanshanian epoch, from which the ore-forming magma was generated and then transported to the superficial layer. Yet the transport network and flow mechanism of the shallow ore-bearing magma, the key problem associ- ated with ore-forming process, was relatively little focused on. Integrate analysis of structural me- chanics, statistical fractal and geological facts suggested that NE trending high-angle fold-related thrust faults and the tessellated basement ones served as the main pathways for the shallow magma’s transporting, moreover, the saddle void spaces among adjacent strata in the folds upon this fault system provided the place for magma’s emplacement. So the folds in the upper part and faults in the lower part of the upper crust constituted the fluid’s transport and emplacement network. During the deformation of geologic body with multi-layer structure, the layers in the upper part tended to fold when received the jacking stress from the lower part, while the lower one inclined to fault undergoing loads of the upper part. And the producing probability of this structure assemblage was highly in- creased in the condition, such as in the Tongling area, that the mechanic rigidity of the lower layers was stronger than that of the upper ones. For the pre-existence of fluid-conducting network, the top magma with high volatile in the magma chamber transported rapidly to the superficial layer in dyking pattern, located in the void spaces of folds, filled and reconstructed them. The sudden drop of pres- sure caused the fluid unmixing from the magma and mass ore-forming elements concentration. Pulse activity of the dyking may be the principal reason why magmatic bodies in the Tongling area were spatially-temporally con

关键词： Tongling, structural network, magma intrusion, fractal, dyke.

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