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Experimental study on interaction between simulated sandstone and acidic fluid

Petroleum Science 2009年第1期6卷 8-16页

作者： Zhang Yongwang Zeng Jianhui Yu Bingsong state key laboratory of Petroleum Resource and Prospecting China University of Petroleum Beijing 102249 China Basin and Reservoir Research Center China University of Petroleum Beijing 102249 China state key laboratory of {3. processes and mineral resources China University of Geosciences Beijing 100083 China

In order to investigate the controlling mechanism of temperature, fluid and other factors on water-rock interaction in the diagenetic process, we performed a series of simulated experiments on the interaction between two kinds of fluids with different salinity and a composite mineral system （simulated sandstone）, which contains albite, K-feldspar and other minerals. The experimental results showed that acidity was the most important factor that affected the dissolution of minerals in the composite mineral system. The lower the pH value, the more easily the minerals dissolved. At the same pH value, the dissolution abilities of different acids for various mineral components were also different. Compared to hydrochloric acid （inorganic acid）, oxalic acid （organic acid） was more able to dissolve aluminosilicate minerals. However, the dissolution ability of oxalic acid for carbonate minerals was lower than that of hydrochloric acid. In the process of fluid-rock interaction, dissolution of feldspar was relatively complicated. Increase of temperature would accelerate the dissolution of feldspar. Under acidic conditions, albite had a higher dissolution rate than K-feldspar. K-feldspar could dissolve and convert into montmorillonite and kaolinite, while albite could dissolve and convert into kaolinite both at 40℃ and 80℃. Presence of organic acid, and decrease of pH value and water salinity were all favorable for the dissolution of feldspar, but weakened the ability to form clay minerals.

关键词： Fluid simulated sandstone dissolution static experiment

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Clay Rocks around Permian-Triassic Boundary at Daxiakou Section in Hubei Province,china

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Journal of Earth Science 2009年第6期20卷 909-920页

作者：张素新袁鹏赵来时童金南杨浩于吉顺史玉芳 state key laboratory of {3. processes and mineral resources China University of Geosciences Faculty of Earth Sciences China University of Geosciences state key laboratory of {3. processes and mineral resources China University of Geosciences

We studied the clay rocks around the Permian-Triassic boundary at the Daxiakou （大峡口） Section in Xingshan （兴山）, Hubei （湖北） Province, china. All clay rocks are predominated by illitemontmorillonite （I/M） mixed-layer minerals, and high-temperature hexagonal bipyramid （HB） quartz and pyrite are contained in different abundances. Clay microspheres are even found in some beds. The results show that volcanic activity was very frequent in this area or in the neighboring areas during the Permian-Triassic transition though the intensity of eruption and the position of the eruption center might have varied during the period. The frequent volcanic activity should be at least one of the leading events to cause the momentous turnover of biota and the ecosystem during the great Permian-Triassic transition.

关键词： volcanic activity Permian-Triassic boundary Daxiakou Section Hubei Province.

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Zircon and apatite fission track analyses on mineralization ages and tectonic activities of Tuwu-Yandong porphyry copper deposit in northern Xinjiang, china

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Science china Earth Sciences 2007年第12期50卷 1787-1795页

作者： YUAN WanMing1,BAO ZengKuan2,DONG JinQuan2,GUO ZhaoJie3.& DENG Jun1 1 state key laboratory of {3. processes and mineral resources,china university of geosciences,Beijing100083.china 2 laboratory of Nuclear Analysis Techniques,Institute of High Energy Physics,Chinese Academy of Sciences,Beijing 10003.,china 3.Department of Geology,Peking university,Beijing 100871,china 1. state key laboratory of {3. processes and mineral resources China University of Geosciences Beijing 100083 China 2. laboratory of Nuclear Analysis Techniques Institute of High Energy Physics Chinese Academy of Sciences Beijing 100039 China 3. Department of Geology Peking University Beijing 100871 China

The mineralization ages reported in the past in the Tuwu-Yandong copper district not only are different,but also fall into the Hercynian *** study has achieved 9 zircon and 7 apatite fission track analysis *** zircon fission track ages range from 158 Ma to 289 Ma and the apatite ages are between 64 Ma and 140 *** mineralization accords with the regional tectonics in the copper *** consider that the zircon fission track age could reveal the mineralization age based on annealing zone temperature of 140―3.0℃ and retention temperature of ～250℃ for zircon fission track,and metallogenetic temperature of 120―3.0℃ in this ore *** three mineralization epochs have been identified,i.e.,289―276 Ma,23.―200 Ma and 165―158 Ma,and indicate occurrence of the min-eralization in the Indosinian and Yanshan *** to apatite fission track ages,the three tectonic-mineralizing epochs are 140―13. Ma,109―97 Ma and 64 Ma,which means age at about 100℃ after the *** three epochs lasted 146 Ma,108 Ma and about 100 Ma from ～250℃ to ～100℃ and trend decrease from early to *** is shown by the fission track modeling that this district underwent three stages of geological thermal histories,stable in Cretaceous and cooling both before Cretaceous and after 20 Ma.

关键词： mineralization age, tectonic epoch, fission track, zircon, apatite, Tuwu-Yandong, Xinjiang

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Phylogeography of regional fauna on the Tibetan Plateau: A review

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Progress in Natural Science:Materials International 2009年第7期19卷 789-799页

作者： Shujuan Yanga, Hailiang Dongb,c, Fumin Lei d a state key laboratory of {3. processes and mineral resources, china university of geosciences, Beijing 100083. china b Geomicrobiology laboratory, china university of geosciences, Beijing 100083. china c Department of Geology, Miami university, Oxford, OH 45056, USA d Institute of Zoology, Chinese Academy of Sciences, Beijing 100101, china [a]state key laboratory of {3. processes and mineral resources China University of Geosciences Beijing 100083 China [b]Geomicrobiology Laboratory China University of Geosciences Beijing 100083 China [c]Department of Geology Miami University Oxford OH 45056 USA [d]Institute of Zoology Chinese Academy of Sciences Beijing 100101 China

The studies of uplift and glaciations of the Tibetan Plateau are summarized, and a series of recent case studies of the endemic species based on DNA sequences are detailed. In general, these molecular data show that all the organisms originated from Early Pliocene to Late Miocene, and then multi-stages of divergence/speciation occurred within each taxa following their original occupation on the plateau, mainly as a result of periodic glacial cycles and geographic isolation. The regional fauna may have undergone several range contractions and expansions during the Pleistocene glaciations. However, the population expansion and refugia may vary in space, time, and extent. The regional fauna of the Tibetan Plateau may be combinations of ancient movement from adjacent zoogeographical regions, speciation in situ, and postglacial colonization from adjacent areas. Geomorphic and climatic changes on the plateau definitely have a remarkable influence on the regional and adjacent biogeographic patterns, and the mechanism is very complex.

关键词： Divergence Refugia Postglacial colonization Phylogeography Regional fauna Tibetan Plateau

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Criteria for defining and recognizing the various orders of sequences in outcrop sequence stratigraphy

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Science china Earth Sciences 2004年第7期47卷 618-629页

作者： WANG Xunlian Faculty of Earth Sciences and mineral resources, china {3. of geosciences, Beijing 100083. china state key laboratory of Palaeobiology and Stratigraphy, Nanjing Institute of Geology and Palaeontology, Chinese Academy of Sciences, Nanjing 210008, china 1. Faculty of Earth Sciences and mineral resources China University of Geosciences 100083 Beijing China 2. state key laboratory of Palaeobiology and Stratigraphy Nanjing Institute of Geology and Palaeontology Chinese Academy of Sciences 210008 Nanjing China

The regional distribution in different depositional facies belts is here regarded as an important criterion for defining and recognizing the various orders of sequences. The third-order sequence is possibly global in nature, which may be discerned in different depositional facies belts in one continental margin and can be correlated over long distances, sometimes even worldwide. Commonly, correlation of subsequence (fourth-order sequence with time interval of 0.51.5 Ma) is difficult in different facies belts, although some of them may also be worldwide in distribution. A subsequence should be able to discern and correlate within at least one facies belt. The higher-order sequences, including microsequence (fifth-order sequence) and minisequence (sixth-order sequence), are regional or local in distribution. They may reflect the longer and shorter Milankovitch cycles respectively. Sequence and subsequence are usually recognizable in different facies belts, while microsequence and minisequence may be distinguished only in shallow marine deposits, but not in slope and basin facies deposits. A brief discussion is made on the essential conditions for correct identification of sequences, useful methods of study, and problems meriting special attention in outcrop sequence stratigraphy.

关键词： outcrop sequence stratigraphy, facies belt, sequence, subsequence, microsequence, minisequence, meter-scale cyclothem, Milankovitch cycle.

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SHRIMP Zircon U-Pb Ages and Geochemical Characteristics of the Neoproterozoic Granitoids in the Huangling Anticline and Its Tectonic Setting

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Journal of Earth Science 2012年第5期23卷 659-675页

作者：魏运许彭松柏蒋幸福彭中勤彭练红李志宏周鹏曾雄伟 wuhan Institute of Geology and minerals resources Wuhan Center of Geological Survey Faculty of Earth Sciences China University of Geosciences Three Gorges Research Center for Geo-hazard Ministry of EducationChina University of Geosciences state key laboratory of {3. processes and mineral resources China University of Geosciences

SHRIMP zircon U-Pb dating of the Neoproterozoic Maoping （茅坪） series （Sandouping （三斗坪） rock suite） granites exposed in the southern part of the Huangling （黄陵） anticline shows that the formation time of Sandouping biotite-hornblende tonalite intrusion, Jinpansi （金盘寺） hornblende-biotite tonalite intrusion, and Longtanping （龙潭坪） monzogranite are 863.9, 842±10, and 844±10 Ma, respectively. Their geochemical features include A/CNK=0.98-1.06, from metaluminous to weakly peraluminous, δ=1.3.-1.53. Sm/Nd=0.17-0.24, and RbN/YbN=1.1-3.62. These indicate that the granite rocks are supersaturated SiO2 calc-alkaline granitoids. The characteristic of Sr-Nd isotopic composition is that the values of εNd（t） and εsr（t） are -12.4 to -11.0 and 20.2-3..2, respectively. It also suggests that the material source of the granite rocks mainly originated from the crust, and they formed in a volcanic arc tectonic environment. These facts suggest that the occurrence of Neoproterozoic granitoids in the southern part of the Huangling anticline should be related to an arc environment along an active continental margin caused by southward subduction of oceanic crust beneath the northern Yangtze craton, and the formation age is not later than 863.Ma.

关键词： Huangling anticline Yangtze plate Neoproterozoic granitoid SHRIMP zircon U-Pbdating geochemistry tectonic setting.

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Hydrocarbon Reservoir Model of Glutenite in the Fourth Member of Shahejie Formation in Northern Dongying Depression

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地学前缘 2009年第S1期16卷 136-137页

作者： Hui Liu~(1,2),Yingchang Cao~3.Yanzhong Wang~3.1.state key laboratory of {3. processes and mineral resources,china university of geosciences,Beijing 100083. china. 2.School of Energy resources,china university of geosciences(Beijing),Beijing 100083.china 3.Faculty of Geo-resources and Information,china university of Petroleum,Dongying 257061,china

The glutenite in the fourth member of Shahejie Formation(Es^4) in northern Dongying depression straightforwardly penetrated into the muddy bathyal -abyss *** conditions of reservoir is very superior:(1) the high quality thick bedded oil source rock is developed very well in the Lijin sag and Minfeng sag of the study area,and it has the higher capability of generating hydrocarbon;(2) the

关键词： glutenite hydrocarbon reservoir formation northern Dongying depression fourth member of Shahejie Formation

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Ostracod fauna across the Permian-Triassic boundary at Chongyang, Hubei Province, and its implication for the process of the mass extinction

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Science china Earth Sciences 2010年第6期53卷 810-817页

作者： LIU Hao1, WANG YongBiao1, YUAN AiHua2, YANG Hao1, SONG HaiJun1 & ZHANG SuXin21 key laboratory of Biogeology and Environmental Geology of Ministry of Education, wuhan 4.0074. china 2 {3. key laboratory of geological processes and mineral resources, wuhan 4.0074. china 1. key laboratory of Biogeology and Environmental Geology of Ministry of Education Wuhan 430074 China2. State Key Laboratory of Geological Processes and Mineral Resources Wuhan 430074 China

Thirty species of 10 ostracod genera were identified from 440 fossil specimens isolated through the hot acetolysis of the rock samples collected across the Permian-Triassic boundary at Chongyang section. Twenty species of 6 genera are found to occur in the limestone of Changxing Formation, and 11 species of 7 genera above the main faunal mass extinction horizon. The os-tracod assemblages identified at the Chongyang section are obviously different from those previously reported in the contem-poraneous microbialites in Guangxi and Chongqing regions, not only in the ostracod components but also in the abundance of filter-feeding ostracods relative to the deposit-feeding ostracods, an indicator of the oxygen level of the seawater. This spatial difference in ostracod assemblages might reflect the diversity of oceanic environmental conditions after the end-Permian mass extinction. Ostracods disappear at 200 cm below and near the main mass extinction horizon, and on the top of the microbialites, respectively, showing an episodic and gradual collapse process at the Chongyang section. The carbon isotope composition is found to appear at 200 cm below the main mass extinction horizon, indicating the initial deterioration of oceanic environment. Fluctuation of the carbon isotope composition is obviously related with the episodic evolution of ostracod species, but not with the abundance of ostracods.

关键词： ostracod microbialite Permian-Triassic mass extinction Chongyang

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Laser Ablation ICP-MS Titanite U-Th-Pb Dating of the Tonglushan Cu-Fe-Au Skarn Deposit,Southeastern Hubei Province

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矿物学报 2009年第S1期29卷 314-316页

作者： LI Jian-wei 1,2,DENG Xiao-dong1,2,ZHOU Mei-fu3.LIU Yong-sheng1(1. state key laboratory of {3. processes and mineral resources,china university of geosciences,wuhan 4.0074.china 2. Faculty of Earth resources,china university of geosciences,wuhan 4.0074.china 3. Department of Earth Sciences,the university of Hong Kong,Hong Kong)

Titanite(CaTi2SiO5) is an important accessory mineral not only in magmatic and metamorphic rocks,but also commonly in hydrothermal mineral deposits. It incorporates appreciable amounts(usually 10×10-6 s to 100×10-6 s) of U and Th into its structure and has a closure temperature of Pb diffusion higher than 660～700 ℃(Scott and St-Onge,1995) ,making it an ideal U-Th-Pb geochronometer. The Daye metallogenic district is located in the west of the giant Middle-Lower Yangtze River(MLYR) Cu-Fe-Au province,eastern china and is well endowed with Fe,Cu,and polymetallic skarn deposits.

关键词： Pb Laser Ablation ICP-MS Titanite U-Th-Pb Dating of the Tonglushan Cu-Fe-Au Skarn Deposit,Southeastern Hubei Province Th Fe ICP Cu MS

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An experimental study of dehydration melting of phengite-bearing eclogite at 1.5―3.0 GPa

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Chinese Science Bulletin 2009年第10期54卷 2090-2100页

作者： LIU Qiang1,2, JIN ZhenMin1,2 & ZHANG JunFeng1,2 1 state key laboratory of {3. processes and mineral resources, china university of geosciences, wuhan 4.0074. china 2 Faculty of Earth Sciences, china university of geosciences, wuhan 4.0074. china state key laboratory of {3. processes and mineral resources China University of Geosciences Wuhan 430074 China Faculty of Earth Sciences China University of Geosciences Wuhan 430074 China

Dehydration melting experiments were performed on ultrahigh-pressure eclogite from Bixiling in the Dabie orogen at 1.5―3.0 GPa and 800―950℃ using piston cylinder apparatus. The results show that (1) eclogite with ~5% phengite started to melt at T≤800―850℃ and P = 1.5―2.0 GPa and produced about 3. granitic melt; (2) the products of dehydration melting of phengite-bearing eclogite vary with temperature and pressure. Fluid released from dehydration of phengite and zoisite leads to partial melting of eclogite and formation of plagioclase reaction rim around kyanite at pressures of 1.5―2.0 GPa and temperatures of 800―850℃; (3. phengite reacted with omphacite and quartz and produced oligoclase, kyanite and melt at elevated temperatures. Oligoclase is the primary reaction product produced by partial melting of phengite in the eclogite; and (4) the dehydration melting of phengite-bearing eclogite at pressures of 1.5―3.0 GPa and temperatures ≥900 ℃ results in formation of garnets with higher molar fraction of pyrope (3..67 wt.%―45.94 wt.%). Potassium feldspar and jadeite occur at P = 2.4―3.0 GPa and T≥900 ℃ , indicating higher pressure and fluid-absent conditions. Our results constrain the solidus for dehydration melting of phengite-bearing eclogite at pressures of 1.5―3.0 GPa. Combining experi- mental results with field observations of partial melting in natural eclogites, we concluded that phengite-bearing eclogites from the Dabie-Sulu orogen were able to partially molten at P = 1.5―2.0 GPa and T = 800―850℃ during exhumation. The ultrahigh-high pressure eclogites would have experienced partial melting in association with metamorphic phase transformation under different fluid conditions.

关键词：超高压榴辉岩脱水熔融实验水白云母反应压力部分熔融大别造山带苏鲁造山带反应产物

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