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Study on the two and three-parameter working stability regions of 3.-TZP suspension

Science China(Technological Sciences) 2006年第5期49卷 547-568页

作者： CHEN Youqiang1, 2, ZHANG Xinni3. CHEN Sha’ou3.& QI Ping3.1. department of Chemistry, Qingdao University, Qingdao 266071, China 2. department of Chemistry, Tsinghua University, Beijing 100084, China 3. department of Physics, Qingdao University, Qingdao 266071, China department of Physics Qingdao University

We determined the variation tendency of viscosity (η) at various solids load- ing (α) for 3.-TZP suspension as a function of dispersant concentration (Cw) using vis- cosity measurement, measured the diameter of particles as a function of Cw in very dilute suspension using light scattering method, and obtained the surface features of the sedi- ment of suspension with different Cw using SEM. We also discussed the influence of the microstructure of adsorbed polymer layers on particles and their interactions in the dis- persing medium on the stability of suspension. Then two different stable states and two different unstable states for 3.-TZP suspension were given. Accordingly, the (Cw, η), (Cw, α), and (α, η) two-parameter, and (Cw, α, η) three-parameter stability maps were con- structed. Based on the DLVO theory calculations, the dispersant concentration, particle distance (r), and interparticle potential energy (VT) maps with various solids loading for 3.-TZP aqueous suspension were also constructed. In (Cw, r) two-parameter coordinate system, the stable motion region map for particles was established. The Cw, α, and VT,max (the highest potential energy) surface of the potential barrier map was obtained through calculation and simulation on the basis of the surfaces of Cw, r, VT maps introduced above. The (Cw, α) two-parameter stability map was then obtained from the Cw, α, VT,max map. The results showed that this theoretical map can qualitatively prove the experimentally obtained results—the existence of different dispersed states of particles in suspension system and the variation tendency of suspension stability with changing each parame- ter—were reasonable.

关键词： 3.-TZP, suspension, stability, DLVO theory, interparticle potential energy.

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Congruences on ideal nil-extension of completely regular semigroups

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Chinese Science Bulletin 1998年第5期43卷 379-381页

作者： REN Xueming 1, 2 GUO Yuqi 2 and CEN Jiaping (Shum Kar-ping) 3.. department of Mathematics, Xi’an University of Architecture & Technology, Xi’an 710055, China 2. department of Mathematics, Yunnan University, Kunming 650091, China 3. department of department of Mathematics Xi’an University of Architecture & Technology Xi’an China department of Mathematics Yunnan University Kunming China department of Mathematics Chinese University of Hong Kong Hong Kong

Let S be an ideal nil-extension of a completely regular semigroup K by a nil semigroup Q with zero. A concept of admissible congruence pairs (δ,ω) of S is introduced, where δ and ω are a congruence on Q and a congruence on K respectively. It is proved that every congruence on S can be uniquely respresented by an admissible congruence pair (δ,ω) of S. Suppose that ρ K denotes the Rees congruence induced by the ideal K of S. Then it is shown that for any congruence σ on S,a mapping Γ:σ|→(σ Q,σ K) is an order-preserving bijection from the set of all congruences on S onto the set of all admissible congruence pairs of S,where σ K is the restriction of σ to K and σ Q=(σ∨ρ K)/ρ K. Moreover,the lattice of congruences of S is also discussed. As a special case,every congruence on completely Archimedean semigroups S is described by an admissible quarterple of S. The following question is asked: Is the lattice of congruences of the completely Archimedean semigroup a semimodular lattice?

关键词： completely regular semigroups ideal nil-extension congruences.

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Mathematic Expression of Kinetic Compensation Effect and Relationship between the Exothermic Decomposition Temperature and Critical Temperature of Thermal Explosion of Eighty-six Energetic Materials

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含能材料 2001年第1期9卷 8-9页

作者： HU Rong zu 1, YANG De suo 2, ZHANG Jiao qiang 3. (1. department of Chemistry,Northwest University, Xi′an 710065, China 2. department of Chemistry and Chemical Engineering, Baoji College of Arts and Science, Baoji 721007, China 3. department of 西北大学陕西西安 710065 宝鸡文理学院陕西 721007 西北工业大学陕西西安 710072

Two relationships are established using the least squares method,between the kinetic parameters (the apparent activation energy and pre exponential constant),and the exothermic decomposition temperature and ther... 详细信息

关键词： critical temperature of thermal explosion decomposition temperature DSC energetic materials.

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Morphology and electrical conductivity of PACS

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Journal of Environmental Sciences 2000年第3期12卷 319-324页

作者： GAO Bao\|yu\+1, LIU Zong\|gang\+2, YUE Qin\|yan\+3. ZHAO Hua\|zhang\+3.(1. department of Environmental Engineering, Shandong University, Jinan 250100, China 2. Environmental Monitoring Station of Huaiyin, Jinan 250022, China 3. department of Environ 山东大学山东济南 2 50 1 0 0 山东济南市槐荫区环境监测山东济南 2 50 0 2 2

Polyaluminium chlorides with sulfate ion(PACS) were prepared by using AlCl 3.6H 2O, Al(SO 4) 3.18H 2O and Na 2CO 3.as raw materials. The effects of basicity ( r ), Al 3. /SO 4 2- molar ratio and aging time on the morphology of PACS were observed by transmission electrical microscope. The influence of aging time on charge neutralization and coagulation effect of PACS was studied. The effects of basicity ( r ), Al 3. /SO 4 2- molar ratio and aging time on the electrical conductivity of PACS solution were also investigated. The experimental results show that the degree of polymerization of polyaluminium chloride(PAC) increases when SO 4 2- ion is added. The higher the basicity( r ) and the longer the aging time, the larger the size of polymer PACS. The ability of PACS neutralizing the charge on Kaolinite decreases with the increase of aging time. The electrical conductivity of PACS solution(the concentration of Al 3. ion is 0.18 mol/L) with different aging time is the function of the basicity and Al 3. /SO 4 2- molar ratios and has its maximum at r =0.5 and Al 3. /SO 4 2- =12.

关键词： coagulant PACS morphology transmission electron microscope electrical conductivity coagulation

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Analysis on cohesive crack opening displacement considering the strain softening effect

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Science China(Physics,Mechanics & Astronomy) 2006年第1期49卷 88-101页

作者： WANG Limin1, XU Shilang2 & ZHAO Xiqiang3.1. Mechanics department, Shandong University of Technology, Zibo 255049, China 2. Civil Engineering department, Dalian University of Technology, Dalian 116024, China 3. Mathematics department, Ocean University of China, Qingdao 266071, China Mechanics department Shandong University of Technology Zibo China Civil Engineering department Dalian University of Technology Dalian China Mathematics department Ocean University of China Qingdao China

In order to investigate the crack propagation in quasi-brittle materials like rock, ceramic and concrete, Hillerborg and his co-researchers abstracted the fracture process zone in front of a stress free crack in terms of a “fictitious crack zone”. On the fictitious crack zone, cohesive stresses distribute following a given softening relationship of stress vs. crack opening. Based on the polynomial or power series expression of cohesive crack opening displacement, the relationship of the cohesive stress vs. the crack opening displacement is established using elastic theory and integral equation, and some unknown physics variables are obtained using variation approach. The calculation results gained in this paper are close to the experimentally test ones.

关键词： cohesive crack, softening, dissipation work, variation approach.

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CMC surfaces in the hyperbolic 3.space

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Chinese Science Bulletin 1998年第7期43卷 547-550页

作者： YU Zuhuan 1, 2 and LI Zhenqi 1, 3.1. Institute of Mathematics, Fudan University, Shanghai 20043., China 2. department of Mathematics,Sichuan Union University, Chengdu 610064, China 3. department of Mathematics, Nanchang University, Nanchang 3. nstitute of Mathemalics Fudan University Shanghai China department of Mathematics Sichuan Union University Chengdu China department of Mathematics Nanchang University Nanchang China

CMC-H surfaces satisfying H≥1 are studied. It is proved that these surfaces possess a natural representation which is a generalization of the Bryant’s result.

关键词： hyperbolic space CMC surface Weierstrass representation.

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Parabolic equation of the m-Laplacian with nonlinear boundary condition

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Chinese Science Bulletin 1998年第11期43卷 905-908页

作者： WANG Shu+ 1, 2, WANG Mingxin 3. XIE Chunhong 1 1. department of Mathematics, Nanjing University, Nanjing 210093. China 2. department of Mathematics, Henan University, Kaifeng 475001, China 3. department of Applied Mathematics, Southeast University, department of Mathernntics Nanjing University Nanjing China department of Mathematics Henan University Kaifeng China department of Applied Mathematics Southeast University Nanjing China

The existence and nonexistence of global positive weak solutions of parabolic equation of the m-Laplician with nonlinear boundary condition are dealt with. The necessary and sufficient conditions on the existence of a... 详细信息

关键词： nonlinear boundary condition parabolic equation of m-Laplacian global solution blow-up.

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Syntheses,characterization,crystal structure and magnetic properties of copper(Ⅱ) α,β-unsaturated carboxylate complexes with trimethyl phosphate

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Chinese Science Bulletin 2001年第12期46卷 987-991页

作者： WANG Yaoyu, LIU Ping, SHI Qian, GAO Yici & SHI Qizhen1. department of Chemistry, Northwest University, Xi’an 710069, China 2. department of Chemistry, Wenzhou Teachers College, Wenzhou 3.5003. China 3. department of Chemistry, Lanzhou University, Lanzhou 73.000, China department of Chemistry Northwest University Xi’an China department of Chemistry Wenzhou Teachers College Wenzhou China department of Chemistry Lanzhou University Lanzhou China

Two ternary complexes Cu2A4[OP(OCH3.3.2 (A represents CH2=CH-COO- and CH2=C(CH3.-COO-) have been synthesized, and elemental analyses, IR, ESR, electronic reflectance spectra and magnetic studies were carried out. The single crystal X-ray diffraction shows that Cu2[CH2=C(CH3.-COO]4[OP(OCH3.3.2 is triclinic, with space group P1, a = 1.05128(13., b = 1.7559(5), c = 1.94479(3. nm, α =91.263.14)°,(β = 102.559(6)°,γ= 106.3.9(13.°, Z = 4 and R = 0.0668. Two copper(Ⅱ) atoms are bridged by four (a-methacrylate groups, and each copper(Ⅱ) atom is coordinated with a trimethyl phosphate molecule in the axial position, forming a distorted square pyramidal configuration. The symmetric center is between the two copper(Ⅱ) atoms, and the Cu-Cu bond distance is 0.26098(6) nm. The Cu-Cu distance and magnetic studies suggest that there exist anti-ferromagnetic interactions between the two copper(Ⅱ) atoms.

关键词： copper(Ⅱ ) complex α β-unsaturated carboxylate trimethyl phosphate magnetic property crystal structure.

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Superconductivity of small metal grains

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Science China(Physics,Mechanics & Astronomy) 2005年第4期48卷 431-441页

作者： ZHENG Renrong1 CHEN Zhiqian2 & ZHU Shunquan1,3.1. department of Physics, Shanghai Normal University, Shanghai 20023., China 2. department of Physics, Southwest Normal University, Chongqing 400715, China 3. department of Computer and Electric Technology, Shanghai Business School, Shanghai 201400, China department of Physics Shanghai Normal University Shanghai China department of Physics Southwest Normal University Chongqing China department of Computer and Electric Technology Shanghai Business School Shanghai China

The formulas of the energy gap and superconducting critical temperature appropriate for systems with both odd and even number of electrons are derived; the bases of the derivations are BCS theory and energy level statistics. Numerical results qualitatively agree with the experimental phenomena. i.e., the superconductivity of small metallic grains will first enhance then decrease to zero when the grain are getting smaller and smaller. The calculations indicate that the above phenomena happen in the metallic grains belonging to Gaussian Orthogonal Ensemble (GOE) and Gaussian Unitary ensemble (GUE) with zero spin; The superconductivity of small metallic grains in Gaussian Symplectic Ensemble (GSE) will monotonically decrease to zero with the decreasing of the grain size. The analyses suggest that the superconductivity enhancements come from pairing and the balance of the strengths between spin-orbital coupling and external magnetic field. In order to take the latter into account, it is necessary to include the level statistics given by Random Matrix Theory (RMT) in describing small metallic grains.

关键词： size effect, superconductivity enhancements, small metallic grains.

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Simultaneously inducing synthesis of semiconductor selenium multi-armed nanorods and nanobars through bio-membrane bi-templates

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Science China Chemistry 2004年第6期47卷 507-511页

作者： LI Li1, WU Qingsheng1 DING Yaping2 & LI Ping3.1. department of Chemistry, Tongji University, Shanghai 200092, China 2. department of Chemistry, Shanghai University, Shanghai 20043., China 3. department of Food, Anhui Agricultural University, Hefei 23.03., China department of Chemistry Tongji University Shanghai 200092 China

Multi-armed nanorods and nanobars of semiconductor selenium were simultane- ously synthesized in the light of biomineralization process through bio-membrane bi-templates of rush at room temperature. The multi-armed nanorods are 60 nm in diameter and 1.5 μm in length; the nanobars are 150 nm in diameter and 1000—1100 nm in length. The XRD pattern indicates that these nanocrystals were crystallized in the hexagonal structure with lattice constants a = 0.43. nm, c = 0.495 nm. The possible formation mechanism was investigated.

关键词： selenium, multi-armed nanorods, nanobars, bio-membrane, bi-templates.

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