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Compression behavior of Zr_(41)Ti_(14)Cu_(12.5)Ni_(10)Be_(22.5) bulk metallic glass up to 24 GPa

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science china(physics,Mechanics & Astronomy) 2005年第3期48卷 319-324页

作者： LI Gong 1, 2 , ZHAN Zaiji 2 , LIU Jing 3., YUN Jinku 1 , SUN Liling 2 , LIU Riping 1 , ZHANG Jun 2 & WANG Wenkui 1, 2 1. Key Laboratory of Metastable Materials science and technology, Yanshan University, Qinhuangdao 066004, china 2. {3. for condensed matter physics, Institute of physics, Chinese Academy of sciences, beijing 100080, china 3. BSRF, Institute of High Energy physics, Chinese Academy of sciences, {13. 10003., china Key Laboratory of Metastable Materials science and technology Yanshan University Qinhuangdao China center for condensed matter {3. Institute of Physics Chinese Academy of Sciences Beijing China BSRF Institute of High Energy Physics Chinese Academy of Sciences Beijing China

The compression of a Zr41Ti14Cu12.5Ni10Be22.5 bulk metallic glass (BMG) is investigated at room temperature up to 24 GPa using in-situ high pressure energy dispersive X-ray diffraction with a synchrotron radiation source. The pressure-induced structural relaxation is exhibited. It is found that below about 8 GPa, the existence of excess free volume contributes to the rapid structural relaxation, which gives rise to the rapid volumetric change, and the structural relaxation results in the structural stiffness under higher pressure.

关键词： bulk metallic glass, high pressure, structural relaxation, synchrotron radiation.

An Explicit Function Expression for dc Bias and Temperature Dependence of Magnetoresistances in Magnetic Tunnel Junctions

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Journal of Materials science & technology 2002年第6期18卷 497-501页

作者： Xiufeng HANState Key Laboratory of Magnetism, Institute of physics and center of condensed {3. physics, Chinese Academy of sciences, beijing 100080, china Chinese Acad Sci Inst Phys State Key Lab Magnetism Beijing 100080 Peoples R China Chinese Acad Sci Ctr Condensed Matter Phys Beijing 100080 Peoples R China

An explicit function expression for the bias voltage or/and temperature dependences of tunnel magnetoresistance ratio and resistances were obtained with a unique set of intrinsic parameters. Two of these intrinsic parameters are the Curie temperature TC and the density of state (DOS) for itinerant majority and minority electrons ξ(ρM/ρm), which are the eigen parameters of ferromagnetic electrodes. Others are the spin-dependent matrix-element ratio (i.e., |Td|2/|TJ|2 ) and the anisotropic-wavelength-cutoff energy ECγ of spin-wave spectrum in magnetic tunnel junction (MTJ), which are the structure parameters of an MTJ. These intrinsic parameters can be predetermined using the experimental measurement or, in principle, using the first-principle calculation method for an MTJ with the three key layers of FM/I/FM. Furthermore, a series of experimental data for an MTJ, for example, a spin-valve-type MTJ of Ta (5 nm)/Ni79Fe21(25 nm)/lr22Mn78(12 nm)/Co75Fe25(4 nm)/AI(0.8 nm)-oxide/Co75Fe25(4 nm)/Ni79Fe21(20 nm)/Ta (5 nm) in this work, can be self-consistently evaluated and explained using such concise explicit function formulations.

关键词： Magnetic tunnel junction TMR Spin-electron transport Magnon excitation Spin-polarization Magnetotransport

Fluorescence dynamics of interactions between polyamide PyPyPyβDp and DNA

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science china Chemistry 2006年第1期49卷 75-80页

作者： ZHANG Huijuan1,2, WANG Jin3. WU Yishi1, YUAN Gu3. AI Xicheng1, WANG Li4 & ZHANG Jianping1 1. State Key Laboratory for Structural Chemistry of Unstable and Stable Species, Institute of Chemistry, Chinese Academy of sciences, beijing 100080, china 2. School of Life science and technology, beijing Institute of technology, beijing 100081, china 3. College of Chemistry and Molecular Engineering, Peking University, beijing 100080, china 4. center for condensed {13. physics, Institute of physics, Chinese Academy of sciences, beijing 100080, china Correspondence should be addressed to Ai Xicheng and Zhang Jianping State Key Laboratory for Structural Chemistry of Unstable and Stable Species Institute of Chemistry Chinese Academy of Sciences Beijing China School of Life science and technology Beijing Institute of Technology Beijing China College of Chemistry and Molecular Engineering Peking University Beijing China center for condensed matter {3. Institute of Physics Chinese Academy of Sciences Beijing China

The photophysical properties of the polyamide PyPyPyβDp (PPP) were investigated by means of steady-state absorption and fluorescence spectroscopies, as well as time-resolved fluo-rescence spectroscopy. It was found that the excited-state properties of PPP are very sensitive to solvents. In TKMC buffer PPP exhibited weak fluorescence with a decay time constant of 16 ps, while with the decrease of the solvent polarity PPP showed the blue-shifted peak position, increased inten-sity and lengthened life-time for its fluorescence behavior. In the presence of calf thymus DNA, it was observed that the fluorescence intensity was enhanced and the fluorescence lifetime increased from 16 to 3. ps for PPP, which verified that PPP bound into the minor groove of DNA duplex.

关键词： polyamide (PPP), calf thymus DNA (ctDNA), time-resolved fluorescence spectroscopy, recognition dynamics.

Approaches to improving critical current density of YBCO superconducting thick films deposited by electrophoresis

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science china(physics,Mechanics & Astronomy) 2004年第2期47卷 165-172页

作者： ZHU Yabin1,2, ZHOU Yueliang2, LIU Zhen2, WANG Shufang2, CHEN Zhenghao2, L?Huibin2, YANG Guozhen2, XIAO Ling3. REN Hongtao3. JIAO Yulei3.& ZHENG Minghui3.1. Department of physics, College of science, beijing Jiaotong University, beijing 100044, china 2. Laboratory of Optical physics, Institute of physics and center for condensed matter physics, Chinese Academy of sciences, beijing 100080, china 3. General Research Institute for Nonferrous Metals, beijing 100088, china Correspondence should be addressed to Zhu Yabin (email: ybzhu@***) Department of physics College of Science Beijing Jiaotong University Beijing 100044 China

Fabrication of YBCO superconducting thick films by electrophoresis has been widely reported. However, the value of critical current density (J c) is far from what the practical application requires. The superconducting thick films are obtained using top-seeded melt growth method with different proportional Y2BaCuO5 (Y211) addition. High-pressure oxygen has been used in the annealing process to improve the uniformity of the oxygen content in the superconducting thick films. When 40mol% Y211 powder is added to the YBa2Cu3.7–5 (Y123. powder,J c for the superconducting thick film by approaches described above reaches 7.008×103.A/cm2 (77 K, 0 T), which is greater than the value ever reported.

关键词： YBCO thick films, electrophoretic deposition, melt-textured.

The size effect on transport properties of colossal magnetoresistance materials La_(0.67)Ca_(0.3.)MnO_3

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science china(physics,Mechanics & Astronomy) 2008年第3期51卷 251-257页

作者： LI PeiGang1,2,LEI Ming1,2,GUO YanFeng2,GUO Xi2,CHEN LeiMing2, TANG WeiHua1,2,SONG PengYun3.& CHEN JinPing3.1 Department of physics,center for Optoelectronics Materials and Devices,Zhejiang Sci-Tech University,Hangzhou 3.0018,china 2 National Laboratory for {3. matter physics,Institute of physics,Chinese Academy of sciences,beijing 100080,china 3.Department of physics,Peking University,beijing 100875,china Department of physics Center for Optoelectronics Materials and Devices Zhejiang Sci-Tech University Hangzhou China National Laboratory for condensed matter physics Institute of Physics Chinese Academy of Sciences Beijing China Department of physics Peking University Beijing China

High quality La0.67Ca0.3.MnO3.(LCMO) film was deposited via a novel pulsed electron deposition technique on SrTiO3.100) single crystal substrate. The micro-bridge with different widths was fabricated by using electron beam lithography (EBL) technique and their transport properties were studied. For the micro-bridges with width of 2 and 1.5 μm,the insulator-to-metal transition temperature (TP) keeps un-changed compared with the film. For the micro-bridges with width of 1 μm,the TP shifts towards the lower temperature by 50 K. When the width decreases down to 500 nm,the insulator-to-metal transition disappears. The magnetoresistance be-havior of these micro-bridges was studied,and the results show that the low field magnetoresistance (LFMR) decreases and the high field magnetoresistances (HFMR) keep almost unchanged as the width of micro-bridge is reduced.

关键词： colossal magnetoresistance pulsed electron deposition electron beam lithography electrical transport properties

Containerless solidification of Zr_(41)Ti_(14)Cu_(12.5)Ni_(10)Be_(22.5) glass-forming alloy in drop tube

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Chinese science Bulletin 2002年第20期47卷 1700-1703页

作者： LI Gong, SUN Liling & WANG WenkuiCollege of Material sciences and Engineering, Yanshan University, Qinhuangdao 066004, china center for {3. matter physics, Institute of physics, Chinese Academy of sciences, beijing 100080, china National Microgravit Coll. of Mat. Sci. and Engineering Yanshan University Qinhuangdao 066004 China center for condensed matter {3. Institute of Physics Chinese Academy of Sciences Beijing 100080 China National Microgravity Laboratory Chinese Academy of Sciences Beijing 100080 China

Droplets of Zr41Ti14Cu12.5Ni10Be22.5 glass forming alloys with different sizes are solidified in a drop tube containerless processing. Glass transition behavior, crystallization kinetics, and the phase evolution during annealing of the Zr41Ti14Cu12.5Ni10Be22.5 glassy spheres are investigated. The experimental results indicate that the apparent activation energy of the glass transition (Eg=43..5 kJ/mol), and the activation energy of the main crystallization reaction (Ep1 = 249.6 kJ/mol) are obviously different from those of bulk glass samples prepared by water quenched (Eg=559.1 kJ/mol and Ep1=192.5 kJ/mol). The difference is discussed in the view point of the atomic configuration of the liquid state of the metallic glass and nucleation mechanism.

关键词： ZrTiCuNiBe alloy containerless processing activation energy drop tube.

Mechanisms of the pancake vortex and vortex line movement in the high T_c superconductors Bi_2Sr_2CaCu_2O_8+δ and La_(1.93.Sr0.0_7CuO_4+δ

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science china(physics,Mechanics & Astronomy) 2007年第2期50卷 240-248页

作者： WANG WeiXian1,ZHOU Fang2,TAN Shun1,WU Huan1 & ZHANG YuHeng1 1 National High Magnetic Field Laboratory,University of science and technology of china,Hefei 23.026,{3. 2 National Laboratory for Superconductivity,lnstitute of physics and the center for condensed matter physics,Chinese Academy of sciences,beijing 100080,{3. National High Magnetic Field Laboratory University of Science and Technology of China Hefei China National Laboratory for Superconductivity Institute of Physics and the Center for Condensed Matter Physics Chinese Academy of Sciences Beijing China

In the strict sense, it is not very clear why with magnetic field increasing, the normal-superconductive (NS) transition becomes broad for Bi2Sr2CaCu208+δ(Bi2212) while the NS transitions are almost parallel for La193.roo7Cu04+δ(La214). In this paper, R-T relations are measured by the six-probe method. We propose a moving mechanism of the pancake vortex and vortex line for Bi2212. The theoretical curves fit the experiment data well.

关键词： superconductivity superconductive pancake vortex dynamics

Studies of Structure Evolution of Nanostructured Hf_(11)Ni_(89) Alloy

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Journal of Materials science & technology 1998年第3期14卷 205-210页

作者： Zhenfu DONG and Lianmao PENG(beijing Lab. of Electron Microscopy, Institute of physics and center for {3. matter physics,Chinese Academy of sciences, P.O.Box 2724, beijing 100080, china)Ke LU and Zhuangqi HU(State Key Lab. for RSA, Institute of Meta beijing Lab. of Electron Microscopy Institute of Physics and Center for Condensed Matter Physics Chinese Academy of Sciences P.O.Box 2724 Beijing 100080 China State Key Lab. for RSA Institute of Metal Research Chinese Academy of Sciences Shenyang 110015 China

A nanostructured Hf11Ni89 ribbon sample was prepared by melt-spinning. It was found that the as-quenched sample is composed of a major HfNi5 compound nanophase and an interfacial magnetic Ni(Hf) solid solution phase. The structure evolution of the sample was studied by using X-ray difFraction (XRD), transmission electron microscopy (TEM), difFerential scanning calorimetry (DSC), resistivity and magnetothermal analysis. Upon heating, a second precipitation process of the Ni(Hf) phase prior to grain growth wa5 detected by means of both structural analysis and physical property measurements. The measurement results are discussed based on the relationship between microstructure and physical properties.

关键词： Studies of Structure Evolution of Nanostructured Hf Alloy Ni

High-pressure and high-tem-perature synthesis of MgB_2 and its superconductivity

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Chinese science Bulletin 2001年第22期46卷 1932-1934页

作者： ZHU Jialin, LI Shaochun, YU Richeng, LI Fengying LIU Zhengxing & JIN ChangqingLaboratory for Extreme Condition physics, Institute of physics, center for {3. matter Physcis and beijing High Pressure Research center, Chinese Academy of sciences, beijing 100080, china Laboratory for Extreme Condition physics Institute of Physics Center for Condensed Matter Physcis and Beijing High Pressure Research Center Chinese Academy of Sciences Beijing China

The single-phase sample of MgB2 was prepared successfully at the temperature of 900℃ and under the pressure of 3.GPa. The structure of the sample was investigated using powder X-ray diffraction and Rietveld analysis. The results show that the structure of the sample belongs to the hexagonal structure with space group of P6/mmm, a=3.0861(5) A, c=3.5222(8) A. The magnetic and resistance measurements indicate that the superconducting transition temperature Tc is 3. K.

关键词： superconductivity magnetization resistance.