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Interfacial Microstructure and Properties of Ti(C, N)/Ni Bonded by Transient Liquid-phase Diffusion

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Journal of wuhan university of technology(Materials {3.) 2009年第3期24卷 432-439页

作者：周世权熊惟皓 School of Mechanical science and Engineering Huazhong University of Science and Technology Department of Mechanical Engineering University of Waterloo School of Materials science and Engineering Huazhong University of Science and Technology

Effects of the main process parameters（temperature and time） on microstructure and properties of Ti（C, N）/Ni interface bonded by （Cu＋Nb） interlayer in a vacuum diffusion bonding device were investigated. The interfacial microstructures consisted initially of Ni3.b metallic compound and eutectic of Ni3.b ＋ CuNiss, and finally transformed to （Ti, Nb）（C, N）＋Ni3.b near Ti （C, N） and NiCuss ＋ Ni3.b near Ni when diffusion bonding temperature was 1 523.1 573.K. It was clear that Cu was a constituent in the transient liquid phase （TLP） into which Ni was dissolved by forming Cu-Ni transition liquid. Nb was dissolved in Cu-Ni transition liquid rapidly. Ti （C, N） conld be wetted by resultant Ni-Nb-Cu transient liquid phase which was followed by a little （Ti, Nb）（C, N） solid solution formed at interface. This increased the interface combining capability. Ultimately the interface shear strength was able to reach 140 MPa. The theoretle analysis and experimental results show that the growth of interfacial reaction layer Ni3.b accords with parabola law, and the activation energy of diffusion reaction is 115.0±0.5 kJ/mol, while the diffusion reaction speed constant is 12.53.mm/s^1/2.

关键词： vacuum diffusion bonding transient liquid phase (TLP) diffusion bonding interlayer activation energy

Nitrogen isotopic geochemical characteristics of crude oils in several basins of china

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science china Earth sciences 2005年第8期48卷 1211-1219页

作者： CHEN Chuanping1,2, MEI Bowen1 & CAO Yacheng3.1. Jianghan Petroleum university, Jingzhou 43.100, china 2. huazhong university of science and technology, {3. 43.047, china 3. Nanjing Institute of Soil science, Chinese Academy of sciences, Nanjing 210008, china Jianghan Petroleum university Jingzhou China huazhong university of science and technology Wuhan China Nanjing Institute of Soil science Chinese Academy of Sciences Nanjing China

Nitrogen isotopic ratios of crude oils with different physical and chemical properties in several basins of china have been measured and their geochemistry has been studied ele-mentally combined with molecular organic geochemistry methods. The data indicate that δ 15N is in the range of ?6‰-20‰. They vary with the oils in different sedimentary types of basins. The oils forming in the limnic environment have lower δ 15N with the value of about 1‰-5‰ whereas the oils in saline or semi-saline environment have higher δ 15N, with most samples being above 10‰ and some exceeding 17‰. The average nitrogen isotopic ratio of oils from the Ordovician formation in the Tarim Basin is the lowest, with most samples having δ 15N below zero, which reflects possibly the characteristic of the oils originating mainly from the organic matter formed in marine carbonate sedimentary environment. The δ 15N distribution can be altered by fractionation. It increases obviously because of biodegradation and decreases during hydrocarbon migration. However, the effect of nitrogen isotopic fractionation in the short distance migration is uncon-spicuous.

关键词： nitrogen isotope, crude oil, sedimentary environment, isotopic fractionation, china.

Flame-retardant Mechanism of Magnesium Oxychloride in Epoxy Resin

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Journal of wuhan university of technology(Materials {3.) 2009年第1期24卷 127-131页

作者：秦麟卿 State Key Laboratory of Advanced technology for Materials Synthesis and Processing Wuhan University of Technology Center for Material Research and Analysis Wuhan University of Technology

Flame-retardant mechanism of magnesium oxychloride （M OC） in EP was in-vestigated by limiting oxygen index （LOI）, XRD, SEM, TG-DTG and DSC. The results show that MOC performed well as an inorganic flame-retardant in EP. When the content of MOC is 50%, the LOI of EP reaches 29.6% and mass of residual char reaches 9.6%. The flame retarde mechanism of MOC is due to the synergies of diluting, cooling, catalyzing char forming and obstructing effects.

关键词： magnesium oxychloride epoxy resin flame-retardant properties flame retardedmechanism

Algorithm of graph isomorphism with threedimensional DNA graph structures

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Progress in Natural science:Materials International 2005年第2期15卷 86-89页

作者： LIU Guangwu 1,2*, YIN Zhixiang 1,3. XU Jin1 and DONG Yafei1(1. Department of Control science and Engineering, Hua Zhong university of science and {3., wuhan 43.074, china 2. College of Transportation, wuhan university of {3., wuhan 43.063. china 3. Department of Mathematics and Physics, Anhui university of science and {3., Huainan 23.001, china) Dept. of Control science and Eng. Huazhong Univ. of Sci. and Technol. Wuhan 430074 China Coll. of Transportation Wuhan Univ. of Technology Wuhan 430063 China Dept. of Mathematics and Physics Anhui Univ. of Sci. and Technol. Huainan 232001 China

An algorithm for solving the graph isomorphism problem with 3.D DNA structures is proposed in this paper. The k-armed branched junction molecules are used to code k-degree vertices. Double stranded molecules are used to code edges. Then the molecules are mixed in a tube to be ligated. The result can be detected by gel electrophoresis. The time complexity of the algorithm is O(n2), where n is the number of vertices of the graph.

关键词： DNA computing DNA graph structure graph isomorphism

A study of two-dimensional magnetic polaron

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science china(Physics,Mechanics & Astronomy) 2006年第4期49卷 421-429页

作者： LIU Tao1, ZHANG Huaihong1, FENG Mang1,2 & WANG Kelin1,3.1. School of science, Southwest university of science and {3., Mianyang 621010, china 2. wuhan Institute of Physics and Mathematics, Chinese Academy of sciences, wuhan 43.070, china 3. Department of Modern Physics, university of science and {3. of china, Hefei 23.026, china School of science Southwest University of Science and Technology Mianyang China wuhan Institute of Physics and Mathematics Chinese Academy of Sciences Wuhan China Department of Modern Physics University of Science and Technology of China Hefei China

By using the variational method and anneal simulation, we study in this paper the self-trapped magnetic polaron (STMP) in two-dimensional anti-ferromagnetic material and the bound magnetic polaron (BMP) in ferromagnetic material. Schwinger angular momentum theory is applied to changing the problem into a coupling problem of carriers and two types of Bosons. Our calculation shows that there are single-peak and multi-peak structures in the two-dimensional STMP. For the ferromagnetic material, the properties of the two-dimensional BMP are almost the same as that in one-dimensional case; but for the anti-ferromagnetic material, the two-dimensional STMP structure is much richer than the one-dimensional case.

关键词： self-trapped magnetic polaron, bound magnetic polaron, impurity potential, anti-ferromagnet.

On the Symmetry Classes of Functions

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wuhan university Journal of Natural sciences 2005年第5期10卷 813-816页

作者： ZHU Ping~1,2, FAN Yun~3.1. School of Mathematics and Statistics, wuhan university, wuhan 43.072, Hubei, {3. 2. School of science, Beijing university of Posts and Telecommunications, Beijing 100876, {3. 3. School of Mathematics and Statistics, huazhong Normal university, wuhan 43.079, Hubei, {3. School of Mathematics and Statistics Wuhan University Wuhan Hubei China School of science Beijing University of Posts and Telecommunications Beijing China School of Mathematics and Statistics Huazhong Normal University Wuhan Hubei China

Let R be an integral domain of characteristic zero such that the corresponding group rings have block decompositions. We first prove that the submodule consisting of all the R-valued ξi-symmetric functions of several variables is a symmetry class, where ξi is any block character. Then we present a relationship among certain operators introduced for block character. Then we present a relationship among certain operators introduced for block characters. As a consequence, we obtain a decomposition of an arbitrary R-valued function of several variables. Finally, we describe the symmetry property of such summands and determine all the symmetry classes.

关键词： symmetry class strict symmetry class blockcharacter ξi-symmetric function block idempotent

A low frequency piezoelectric power harvester using a spiral-shaped bimorph

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science china(Physics,Mechanics & Astronomy) 2006年第6期49卷 649-659页

作者： HU Yuantai1,2,HU Hongping2 & YANG Jiashi3.1. Institute of Mechanics and Sensing technology,Central South university,Changsha 410083.china 2. Department of Mechanics,{3.,wuhan 43.074,china 3. Department of Engineering Mechanics,university of Nebraska,Lincoln,NE 68588-0526,USA Institute of Mechanics and Sensing technology Central South University Changsha China Department of Mechanics Huazhong University of Science and Technology Wuhan China Department of Engineering Mechanics University of Nebraska Lincoln USA

We propose a spiral-shaped piezoelectric bimorph power harvester operating with coupled flexural and extensional vibration modes for applications to low frequency energy sources. A theoretical analysis is performed and the computational results show that the spiral structure has relatively low operating frequency compared to beam power harvesters of the same size. It is found that to optimize the performance of a piezoelectric spiral-shaped harvester careful design is needed.

关键词： spiral-shaped bimorph,piezoelectric harvester,power density.

On the new results of global attractive set and positive invariant set of the Lorenz chaotic system and the applications to chaos control and synchronization

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science in china(Series F) 2005年第3期48卷 304-321页

作者： LIAO Xiaoxin 1, 2, 3., FU Yuli 4 & XIE Shengli 4 1. Department of Control science & Control Engineering, huazhong university of science & technology, wuhan 43.074, china 2. School of Automation, wuhan university of science & technology, wuhan 43.070, china 3. School of Information, Central South university of Economy, Politics and Law, wuhan 43.064, china 4. School of Electronics & Information Engineering, South china university of technology, Guangzhou 510640, china Correspondence should be addressed to Liao Xiaoxin (email: xiaoxin_liao@***) Department of Control science & Control Engineering Huazhong University of Science & Technology Wuhan China School of Automation Wuhan University of Science & Technology Wuhan China School of Information Central South University of Economy Politics and Law Wuhan China School of Electronics & Information Engineering South China University of Technology Guangzhou China

Constructing a family of generalized Lyapunov functions, a new method is proposed to obtain new global attractive set and positive invariant set of the Lorenz chaotic system. The method we proposed greatly simplifies the complex proofs of the two famous estimations presented by the Russian scholar Leonov. Our uniform formula can derive a series of the new estimations. Employing the idea of intersection in set theory, we extract a new Leonov formula-like estimation from the family of the estimations. With our method and the new estimation, one can confirm that there are no equilibrium, periodic solutions, almost periodic motions, wandering motions or other chaotic attractors outside the global attractive set. The Lorenz butterfly-like singular attractors are located in the global attractive set only. This result is applied to the chaos control and chaos synchronization. Some feedback control laws are obtained to guarantee that all the trajectories of the Lorenz systems track a periodic solution, or globally stabilize an unstable (or locally stable but not globally asymptotically stable) equilibrium. Further, some new global exponential chaos synchronization results are presented. Our new method and the new results are expected to be applied in real secure communication systems.

关键词： Lorenz chaotic system global attractive set positive invariant set globally exponential tracking globally exponential synchronization.

Study on the two and three-parameter working stability regions of 3.-TZP suspension

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science china(Technological sciences) 2006年第5期49卷 547-568页

作者： CHEN Youqiang1, 2, ZHANG Xinni3. CHEN Sha’ou3.& QI Ping3.1. Department of Chemistry, Qingdao university, Qingdao 266071, china 2. Department of Chemistry, Tsinghua university, Beijing 100084, china 3. Department of Physics, Qingdao university, Qingdao 266071, china Department of Chemistry Qingdao University Qingdao China Department of Chemistry Tsinghua University Beijing China Department of Physics Qingdao University Qingdao China

We determined the variation tendency of viscosity (η) at various solids load- ing (α) for 3.-TZP suspension as a function of dispersant concentration (Cw) using vis- cosity measurement, measured the diameter of particles as a function of Cw in very dilute suspension using light scattering method, and obtained the surface features of the sedi- ment of suspension with different Cw using SEM. We also discussed the influence of the microstructure of adsorbed polymer layers on particles and their interactions in the dis- persing medium on the stability of suspension. Then two different stable states and two different unstable states for 3.-TZP suspension were given. Accordingly, the (Cw, η), (Cw, α), and (α, η) two-parameter, and (Cw, α, η) three-parameter stability maps were con- structed. Based on the DLVO theory calculations, the dispersant concentration, particle distance (r), and interparticle potential energy (VT) maps with various solids loading for 3.-TZP aqueous suspension were also constructed. In (Cw, r) two-parameter coordinate system, the stable motion region map for particles was established. The Cw, α, and VT,max (the highest potential energy) surface of the potential barrier map was obtained through calculation and simulation on the basis of the surfaces of Cw, r, VT maps introduced above. The (Cw, α) two-parameter stability map was then obtained from the Cw, α, VT,max map. The results showed that this theoretical map can qualitatively prove the experimentally obtained results—the existence of different dispersed states of particles in suspension system and the variation tendency of suspension stability with changing each parame- ter—were reasonable.

关键词： 3.-TZP, suspension, stability, DLVO theory, interparticle potential energy.