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Adsorption of surfactants onto acrylic ester resins with different pore size distribution

Science china Chemistry 2006年第5期49卷 445-453页

作者： YANG Weiben1,2,3.LI Aimin1,3.CAI Jianguo1,3.MENG Guanhua1,3.& ZHANG Quanxing1,3.1. State Key Laboratory of Pollution Control and Resource Reuse,School of the Environment,Nanjing University,Nanjing 210093.china 2. Nanjing College of Chemical Technology,Nanjing 210048,china 3. Jiangsu Engineering & Technology Research Center for Organic Toxicant Control and Resource Reuse,Nanjing 21003.,china State Key Laboratory of Pollution Control and Resource Reuse School of the Environment Nanjing University Nanjing China Nanjing College of Chemical Technology Nanjing China Jiangsu Engineering & Technology Research Center for Organic Toxicant Control and Resource Reuse Nanjing China

In this study, a series of acrylic ester resins with different pore size distribution were prepared successfully by varying the type and the amount of pore-forming agents. In order to inves-tigate the adsorption behavior and mechanism of surfactants on acrylic ester resins, three kinds of surfactants were utilized as adsorbates that were sodium 6-dodecyl benzenesulfonate (6-NaDBS), sodium 1-dodecyl benzene sulfonate (1-NaDBS) and sodium 1-dodecyl sulfonate, respectively. It was observed that the surface area was available in a particular pore size and an appropriate pore size of resins appeared to be more important for the adsorption of surfactants. As compared to commercial acrylic ester resins XAD-7 and HP2MG, 50# and 3.# resins exhibited more excellent adsorption properties toward 1-NaDBS and 6-NaDBS. The experimental equilibrium data were fitted to the Langmuir, and double-Langmuir models. Two models provided very good fittings for all resins over the temperature range studied. The investigation indicated that electrostatic attraction and hydrogen bond between resins and surfactants were the main forces and had an obvious effect on adsorption proc-ess.

关键词： acrylic ester resin, surfactant, adsorption, pore size distribution, isotherm.

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无轨胶轮车防爆柴油机尾气净化装置研制及试验

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矿业安全与环保 2024年

作者：张小荣胡志伟鲍久圣杨文政王飞唐彬展张磊 1.西山煤电(集团)有限责任公司 2.山西西山晋兴能源有限责任公司斜沟煤矿 3.中国矿业大学机电工程学院西山煤电(集团)有限责任公司山西西山晋兴能源有限责任公司斜沟煤矿中国矿业大学机电工程学院

针对煤矿井下无轨胶轮车尾气污染严重，无法满足非道路国Ⅳ排放标准的问题，为其设计了一种新型复合式尾气净化装置并进行了试验验证。首先，设计了由“废气再循环（Exhaust Gas Recirculation,EGR）+氧化催化器（Diesel Oxidation Cata... 详细信息

针对煤矿井下无轨胶轮车尾气污染严重，无法满足非道路国Ⅳ排放标准的问题，为其设计了一种新型复合式尾气净化装置并进行了试验验证。首先，设计了由“废气再循环（Exhaust Gas Recirculation,EGR）+氧化催化器（Diesel Oxidation Catalyst,DOC）+催化型颗粒捕集器（Catalyst Diesel Particulate Filter,CDPF）+防爆水冷结构”组成的尾气净化系统；接着，利用GT-Power仿真软件建立了催化器模型，得到了排气参数对DOC催化反应的影响规律；在此基础上，针对TDE6105DZLQFB02非道路国Ⅲ防爆柴油机研制了尾气净化装置并进行了柴油机性能及排放试验。试验结果表明：加装尾气净化装置后，试验车辆在不同工况下，尾气中CO、HC、NOx和PM的净化效率分别达到了96.8%、50.95%、25.5%和95.2%，可满足非道路国Ⅳ排放法规限值。

关键词：无轨胶轮车防爆柴油机尾气后处理煤矿井下非道路国IV

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Fractal Analysis of Gas Diffusion Layer in PEM Fuel Cells

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Journal of wuhan University of Technology(Materials Science) 2006年第1期21卷 22-25页

作者：石英肖金生 State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070ChinaSchool of Automation Wuhan University of Technology Wuhan 430070 China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070ChinaSchool of Automotive EngineeringWuhan University of Technology Wuhan 430070China

The aim of this study is to show how fractal analysis can be effectively used to characterize the texture of porous solids. The materials under study were carbon papers, the backing material of the gas diffusion layer （GDL） in Proton Exchange Membrane Fuel Cell （PEMFC）. The fractal dimensions were calculated by analyzing data from mercury porosimetry. The polytotrafluoroethylene （PTFE） treated carbon paper shows a significantly high fractal dimension value than pare sample, and the high fractal dimension signifies that the physical complexity of the pore surface is enhanced. The fractal dimension can be used as a valid parameter to monitor the textural evolution of the samples as the treatment progresses, as this behaves in a similar way to other textural parameters. The use of fractal analysis in conjunction with the results of classical characterization methods leads to a better understanding of textural modificatious in the processing of materials.

关键词： PEMFC gas diffusion layer fractal dimension mewury porosimetry

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Sm-Nd and zircon SHRIMP U-Pb dating of Huilanshan mafic granulite in the Dabie Mountains and its zircon trace element geochemistry

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Science china Earth Sciences 2005年第12期48卷 2081-2091页

作者： HOU Zhenhui1, LI Shuguang1, CHEN Nengsong2, LI Qiuli1 & LIU Xiaoming3.1. School of Earth and Space Sciences, University of Science and Technology of china, Hefei 23.026, china 2. The Key Laboratory of Continental Dynamics of the Ministry of Education, Northwest University, Xi’an 710069, china 3. Faculty of Earth Sciences, china University of Geosciences, wuhan 43.074, china School of Earth and Space Sciences University of Science and Technology of China Hefei China The Key Laboratory of Continental Dynamics of the Ministry of Education Northwest University Xi’an China Faculty of Earth Sciences China University of Geosciences Wuhan China

The mafic granulites from Huilanshan are outcropped on the center of the Luotian dome in the northern Dabie Mountains. The Sm-Nd isochron defined by granulite-facies meta-morphic minerals (garnet + clinopyroxene + hypersthene) yields an age of 13. ± 18 Ma indicating the early Cretaceous granulite-facies metamorphism. The cathodoluminescence (CL) images of zircons from the granulite show clearly core-mantle-rim structures. The zircon cores are charac-terized by typical oscillatory zoning and highly HREE enriched patterns, which suggests their magma origin. Some zircon cores among them with little Pb loss give SHRIMP U-Pb ages rang-ing from 753.to 780 Ma, which suggests that the protolith of Huilanshan granulite is Neopro-terozoic mafic rocks. The zircon mantles usually cut across the oscillatory zone of the zircon cores have 3.10 times lower REE, Th, U, Y, Nb and Ta contents than the igneous zircon cores but have high common Pb contents. These characteristics suggest that they were formed by hydrothermal alteration of the igneous zircons. The part of zircon mantles with little Pb loss give a similar SHRIMP U-Pb age (716―780 Ma) to the igneous zircon cores, which implies that the hydrothermal events occurred closely to the magmatic emplacement. In view of the strong early Cretaceous magmatism in the Luotian dome, consequently, the Huilanshan mafic granulite was formed by heating of the Neoproterozoic mafic rocks in mid-low crust, which caused the granu-lite-facies metamorphism underneath the Dabie Mountains. The similarity between the granulite metamorphic age (13. ± 18 Ma) defined by Sm-Nd isochron and K-Ar age of 123.127 Ma given by amphible from the gneiss in Luotian dome suggests a rapid uplifting of the Luotian dome, which may result in further exhumation of the ultrahigh pressure metamorphic rocks in the Dabie Mountains.

关键词： Dabie orogen, granulite, zircon U-Pb ages, Sm-Nd age.

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Congruences on ideal nil-extension of completely regular semigroups

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Chinese Science Bulletin 1998年第5期43卷 379-381页

作者： REN Xueming 1, 2 GUO Yuqi 2 and CEN Jiaping (Shum Kar-ping) 3.. Department of Mathematics, Xi’an University of Architecture & Technology, Xi’an 710055, china 2. Department of Mathematics, Yunnan University, Kunming 650091, china 3. Department of Department of Mathematics Xi’an University of Architecture & Technology Xi’an China Department of Mathematics Yunnan University Kunming China Department of Mathematics Chinese University of Hong Kong Hong Kong

Let S be an ideal nil-extension of a completely regular semigroup K by a nil semigroup Q with zero. A concept of admissible congruence pairs (δ,ω) of S is introduced, where δ and ω are a congruence on Q and a congruence on K respectively. It is proved that every congruence on S can be uniquely respresented by an admissible congruence pair (δ,ω) of S. Suppose that ρ K denotes the Rees congruence induced by the ideal K of S. Then it is shown that for any congruence σ on S,a mapping Γ:σ|→(σ Q,σ K) is an order-preserving bijection from the set of all congruences on S onto the set of all admissible congruence pairs of S,where σ K is the restriction of σ to K and σ Q=(σ∨ρ K)/ρ K. Moreover,the lattice of congruences of S is also discussed. As a special case,every congruence on completely Archimedean semigroups S is described by an admissible quarterple of S. The following question is asked: Is the lattice of congruences of the completely Archimedean semigroup a semimodular lattice?

关键词： completely regular semigroups ideal nil-extension congruences.

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On-line parallel reversed phase two-dimensional liquid chromatography for high-throughput analysis of complex proteomic samples

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Science china Chemistry 2006年第6期49卷 527-533页

作者： WANG Zhicong1,3. ZHANG Qinghe2, LI Tong2, ZHAO Zhongyi3.& ZHANG Weibing1 1. Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116011, china 2. Dalian Elite Analytical Instrument Co., Ltd., Dalian 116011, china 3. Faculty of Material Science and Chemical Engineering, china University of Geosciences, {3., china Dalian Institute of Chemical Physics Chinese Academy of Sciences Dalian China Faculty of Material Science and Chemical Engineering China University of Geosciences Wuhan China Dalian Elite Analytical Instrument Co. Ltd. Dalian China

A comprehensive two-dimensional liquid chromatographic system (2D SCX/RP) is con- structed with a 10-port-2-way valve using strong cation exchange chromatography (Hypersil SCX, 100 mm×4.6 mm I.D.) followed by reversed phase chromatography (Hypersil BDS C18, 15 mm×4.6 mm I.D.) to separate the complex peptides from globin peptic hydrolysate. After the sample was loaded on the SCX column, the phosphate buffer (pH 4.0) was used to elute the peptides. Then, elutes flowed through the interface and the peptides focused on the head of the trapping columns (Hypersil BDS C18, 15 mm×4.6 mm I.D.) but salt passed into the waste. After the valve was switched, the samples were flushed with a backward flow into the RP analytical column. The peptides on the SCX were eluted with 12 discontinuous steps linearly increasing salt concentrations. The peptides enriched on the trapping column were desalted and separated by the RP columns. The resolution and the resolved peaks of the 2D SCX/RP system were greatly increased and the total peak capacity reached as high as 2280.

关键词： two-dimensional liquid chromatography, interface, trapping column, proteomics, globin.

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Indian Ocean-MORB-type isotopic signature of Yushigou ophiolite in North Qilian Mountains and its implications

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Science china Earth Sciences 2006年第6期49卷 561-572页

作者： HOU Qingye1,2, ZHAO Zhidan1,2, ZHANG Hongfei3. ZHANG Benren3.& CHEN Yuelong2 1. State Key Laboratory of Geological Processes and Mineral Resources, china University of Geosciences, Beijing 100083. china 2. School of Earth Science and Mineral Resources, china University of Geosciences, Beijing 100083. china 3. Faculty of Earth Sciences, china University of Geosciences, wuhan 43.074, china State Key Laboratory of Geological Processes and Mineral Resources China University of Geosciences Beijing China School of Earth Science and Mineral Resources China University of Geosciences Beijing China Faculty of Earth Sciences China University of Geosciences Wuhan China

In order to explore the disputed issue concerning the tectonic affinity ofthe ancient ocean mantle of North Qilian Mountains (NQM), geochemical and Sr, Nd, Pb isotopiccompositions of pillow basalts of the Yushigou Ophiolite (YSGO) suite from NQM have been analyzedsystematically. The pillow basalts exhibit tholeiitic characteristics, with flatchondrite-normalized REE patterns ((La/Yb)_N = 0.98—1.27). They display no Nb, Ta, Zr, Hf negativeanomalies, and show MORB features in 2Nb-Zr/4-Y and Ti/100-Zr-YX3.tectonic discrimination *** results indicate that the Yushigou ophiolite is most likely to be formed in a mid-ocean ridgeor mature back-arc basin. Their isotopic data show a relatively broad and enriched ^(87)Sr/^(86)Sr(0.70509 — 0.70700), restricted ^(143.Nd/^(144)Nd (0.512955-0.512978). Pb isotopes are in the rangeof ^(206)Pb/^(204)Pb (18.054-20.562), ^(207)Pb/^(204)Pb (15.53.-15.743. and ^(208)Pb/^(204)Pb(3..068-3..53.). These isotopic data imply that the basalts originated from the depleted mantle(DMM), with the involvement of enriched mantle components (mainly EMII). Geochemical comparisonsbetween the basalts in YSGO and the MORB-type basalts of ophiolite suites occurring in the knownancient Tethyan tectonic domain indicate that the ancient oceanic mantle represented by YSGO suiteforming in early Paleozoic in the North Qilian Moutains is very similar to the Tethyan mantle inboth trace elements and isotopic compositions. The North Qilian Mountains should be a part of theTethyan tectonic domain in early Paleozoic. This further implies that the Tethyan tectonic domaincan be deduced to early Paleozoic in the study area, which will be helpful to discussing thetectonic affinity and evolution of the North Qilian Mountains.

关键词： geochemistry, Indian Ocean-MORB-type isotopic signatures, Tethyan tectonic domain, Yushigou ophiolite, North Qilian Mountains.

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The role of aerial algae in the formation of the landscape of the Yunnan Stone Forest,Yunnan Province, china

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Science china Earth Sciences 2004年第9期47卷 846-864页

作者： TIAN Youping1,3. ZHANG Jie2, SONG Linhua1 & BAO Haosheng2 1. Institute of Geographic Sciences and Natural Resources Research, Chinese Academy of Sciences, Beijing 100101, china 2. Department of Geography, Nanjing University, Nanjing 210093. china 3. School of Earth Sciences and Resources, china University of Geosciences, Beijing 100083. china Institute of Geographic Sciences and Natural Resources Research Chinese Academy of Sciences Beijing China School of Earth Sciences and Resources China University of Geosciences Beijing China Department of Geography Nanjing University Nanjing China

Aerial algae on the surface of carbonate rocks at the Stone Forest, Shilin County, Yunnan Province, china, and their bioerosion were investigated in the field and studied in the laboratory in detail. Through the observation, identification and statistics of more than one hun- dred algal samples and rock samples with the optical microscopes (stereomicroscope, biological microscope) and the scanning electronic microscope (SEM), the relationships between erosional forms on the surface of the Stone Forest and algae and/or algal communities and the genetic mechanism for the formation of erosional forms were analyzed. It is suggested that aerial algae play an active role in bioerosive processes that may affect the formation of karst erosional forms. These effects include both direct and indirect ones. The direct effect is the initiative control (algal shape-controlling role) of algae on the formation of karst forms of various scales, mostly mi- cro-scale (3.) and minor-scale (10-3.10-1m) erosional forms. The algal shape-controlling roles can be divided into the algal individual shape-controlling role and the algal community shape-controlling role. The former mostly controls the formation of micro-scale erosional forms, while the latter mostly controls the formation of micro-scale and smaller minor-scale erosional forms. The indirect effect refers to the promoting role of algae in the formation of karst forms, which may affect the formation of karst forms of all types and scales. The bioerosion of algae accelerates the weathering process of the whole Stone Forest karst landforms.

关键词： aerial algae, bioerosion, the Stone Forest, Yunnan Province, china.

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盾构隧洞斜螺栓接头在不均匀沉降作用下的受力分析

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水利水电技术(中英文) 2024年

作者：刘闯齐慧君杰德尔别克·马迪尼叶提 1.国电南京自动化股份有限公司 2.河海大学水利水电学院 3.新疆农业大学水利与土木工程学院新疆农业大学水利与土木工程学院国电南京自动化股份有限公司河海大学水利水电学院

With the construction of water transfer projects， shield tunnels have been widely used. Long distance water transfer tunnels inevitably traverse sections of poor geology and potential uneven settlement may occur in shield tunnels under non-uniform geology. As the main load-bearing structure， the current assembled outer lining mainly uses diagonal bolted joints. A reasonable modelling of the diagonal bolted joints and an analysis of their mechanical behavior under uneven settlement is of great importance for the analysis of the longitudinal stability of tunnels. In this paper， the mechanical performance of inclined bolted joints under the action of external forces is investigated. The distribution of axial force and bending moment of the inclined bolts under different operating conditions is studied， the bolts are simulated using the generalized displacement method of buried beams， and a numerical simulation method is established considering the interpolation of the corner displacement. By comparing the finite element analysis results with the test results， it is concluded that the interpolation of the corner displacement of the bolt has a significant influence on the numerical simulation， and it will generate a certain bending stress under uneven settlement， which provides a reference for engineering design.

关键词：盾构隧洞不均匀沉降装配式外衬斜螺栓受力分析

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归一化模型在人类认知活动中的应用

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应用心理学 2024年

作者：孙阳阳罗鑫宇周柳芳李海燕孙彦良 1.山东师范大学心理学院 2.上海外国语大学国际工商管理学院 3.山东大学齐鲁医院神经外科山东师范大学心理学院上海外国语大学国际工商管理学院山东大学齐鲁医院神经外科

神经计算模型是深入解析神经元信息编码过程的重要方法。近年来，归一化模型(normalization model)作为一种新兴神经计算方法，在人类认知活动中广泛应用。此模型基于当前反应神经元的活动与神经元池活动总和的比率，来揭示神经元的实... 详细信息

神经计算模型是深入解析神经元信息编码过程的重要方法。近年来，归一化模型(normalization model)作为一种新兴神经计算方法，在人类认知活动中广泛应用。此模型基于当前反应神经元的活动与神经元池活动总和的比率，来揭示神经元的实际响应。最初用于解析初级视觉皮层中的神经元活动，随后在感知觉和注意机制研究中得到了充分的验证和应用，但在高级认知活动研究中的应用仍显不足。展望未来，归一化模型在高级认知活动研究中的应用值得进一步拓展。

关键词：归一化模型感觉注意决策工作记忆

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