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The Process of TiB_2-Cu Composite Phase and Structure Formation during Combustion Synthesis

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Journal of Wuhan university of Technology(materials science) 2006年第4期21卷 113-116页

作者：徐强 School of materials science and engineering Beijing Insitute of TechnologyBeijing 100081China

The reaction process of combustion synthesis for TiB2 -Cu was investigated in detail using combustion-wave arresting experiment, X-ray diffraction （ XRD ） analysis, SEM analysis and differential thermal analysis （ DTA ）. The XRD analysis results for the different parts of the quenched specimen show that TiCux intermetallic phase firstly forms with the propagation of combustion wave, and then Ti1.87 B50 and Ti3B4 metastable phases come forth due to the diffusion of B atoms and finally the stable TiB2 phase forms because of the continuous diffusion of B atoms. The formation of TiB2 phase is uot completed by one step, but undergoes several transient processes. The process of reaction synthesis for Ti-B-Cu ternary system can be divided into three main stages： melting of Cu and Ti , and the formation of Cu- Ti melt and few TiCux , TiBx intermetallic phases ; large numbers of TiCux intermetallic phases formation and some fine TiB2 particles precipitation ; and the TiB2 particles coarsening and the stable TiB2 and Cu two phases formation in the final product.

关键词： combustion synthesis reaction process TiB2 phase combustion-wave arresting experiment

Preparation of nanocrystalline BaTiO_3 ceramics

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science china(Technological sciences) 2009年第6期52卷 1730-1734页

作者： DENG XiangYun1,2,LI DeJun1,LI JianBao2,WANG XiaoHui3 & LI LongTu3 1 College of Physics and Electronic Information,Tianjin Normal university,Tianjin 300387,china 2 materials and Chemical engineering Institute,Key Laboratory for Hainan Advantage Resources and Applied Technology in Chemical engineering Material of Ministry of Education,Hainan Provincial Key Laboratory of Research on Utilization of Si-Zr-Ti,Hainan university,Haikou 570228,china 3 department of materials science and engineering,tsinghua university,beijing 100084,china College of Physics and Electronic Information Tianjin Normal University Tianjin 300387 China materials and Chemical engineering Institute Key Laboratory for Hainan Advantage Resources and Applied Technology in Chemical Engineering Material of Ministry of Education Hainan Provincial Key Laboratory of Research on Utilization of Si-Zr-Ti Hainan University Haikou 570228 China department of materials science and engineering Tsinghua University Beijing 100084 China

The high-dense nanocrystalline BaTiO3(BT)ceramics with grain size smaller than 100nm have been successfully prepared by the two step sintering and the spark plasma sintering(SPS)*** successive transitions in nanograin BT ceramics from rhombohedral to orthorhombic,tetragonal and cubic transitions,similar to those in coarse BT ceramics,were revealed by in-situ temperature dependent Raman *** multiphase coexistence and the diffused phase transition character were demonstrated in the 8nm nanocrystalline BT ceramics.

关键词： nanocrystalline BaTiO3 ceramics preparation microstructure size effect

CORRELATION BETWEEN STRESS COMPONENTS AND STRESS CORROSION CRACKS IN BRASS Lecturer,department of materials Physics,university of science and Technology beijing,beijing 100083,china

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Acta Metallurgica Sinica(English Letters) 1992年第9期5卷 178-182页

作者： QIAO Lijie LIU Rui XIAO Jimei university of science and Technology beijing,beijing,china

The effects of stress components on nucleation sites and propagation directions of stress cor- rosion cracks in brass were investigated with specimens under mode Ⅱ and mode Ⅲ loadings. The results indicated that under mode Ⅱ loading,stress corrosion cracks nucleated on the site with maximum normal stress component and propagated along the plane perpendieular to the maximum normal stress,under mode Ⅲ loading,the stress corrosion crack was not evident on the 45°plane due to the general corrosion in aqueous solution with high NH_4OH concentra- tion,while stress corroded in aqueous solution with low NH_4OH concentration, numerous cracks with spacings of 10—150μm were found on the 45°plane with maximum normal stress and no stress corrosion cracks was observed on the plane with maximum shear stress.

关键词： stress corrosion cracking stress compoonent brass ammonia solution

TEXTURE DETERMINATION OF THIN FILM ZrO_2 BY ELECTRON DIFFRACTION

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Acta Metallurgica Sinica(English Letters) 1993年第12期6卷 472-473页

作者： WANG Yinghua tsinghua university,beijing,china department of materials science and engineering,tsinghua university,beijing 100084,china tsinghua Univ Beijing China

A method for semi-quantitative determination of thin film texture using electron diffrac- tion is *** texture state of a zirconia thin film with a cubic structure has been determined in this way and is presented as an... 详细信息

关键词： texture thin film electron diffraction ZrO_2

Effects of Si Content and the Addition Amount of Al-3B Master Alloy on the Solidification Structures of Hypoeutectic Al-Si Alloys

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Rare Metals 2001年第3期20卷 168-173页

作者： Donghui Wang,Jianguo Li, Yankang Zheng, Bingzhe Bai department of materials science and engineering, tsinghua university, beijing 100084, china Tsing Hua Univ Dept Mat Sci & Engn Beijing 100084 Peoples R China

Effects of Si content and the addition amount of Al-3B master alloy on the solidification structures of hypoeutectic Al-Si alloys were studied. The addition amounts of the master alloy were 0.2%, 0.4%, 0.7% and 1% (mass fraction, so as the follows), respectively. The Si content of Al-Si binary alloys investigated varied from 1% to 11%. The observation of macrostructures of non-refined samples showed that 3% Si constitutes a transition point at which the minimum grain size can be obtained. It was also found that Al-3B master alloy can shift the transition point towards a higher Si value when its addition amount increases, making this point appear at 4%, 5% and 6% Si as its addition amount increases up to 0.4%, 0.7% and 1%, respectively.

关键词： Al-3B master alloy hypoeutectic Al-Si alloy grain refinement

INTERFACIAL REACTIONS OF METAL FILMS WITH AlN SUBSTRATE

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中国有色金属学会会刊：英文版 1996年第2期6卷 81-85页

作者： He Xiangjun Tao Kun Fan Yudian (department of materials science and engineering, tsinghua university, beijing 100084) department of materials science and engineering Tsinghua University Beijing 100084 China

ＩＮＴＥＲＦＡＣＩＡＬＲＥＡＣＴＩＯＮＳＯＦＭＥＴＡＬＦＩＬＭＳＷＩＴＨＡｌＮＳＵＢＳＴＲＡＴＥＨｅＸｉａｎｇｊｕｎ；ＴａｏＫｕｎ；ＦａｎＹｕｄｉａｎ（ＤｅｐａｒｔｍｅｎｔｏｆＭａｔｅｒｉａｌｓＳｃｉｅｎｃｅａｎｄＥ... 详细信息

ＩＮＴＥＲＦＡＣＩＡＬＲＥＡＣＴＩＯＮＳＯＦＭＥＴＡＬＦＩＬＭＳＷＩＴＨＡｌＮＳＵＢＳＴＲＡＴＥＨｅＸｉａｎｇｊｕｎ；ＴａｏＫｕｎ；ＦａｎＹｕｄｉａｎ（ＤｅｐａｒｔｍｅｎｔｏｆＭａｔｅｒｉａｌｓＳｃｉｅｎｃｅａｎｄＥｎｇｉｎｅｅｒｉｎｇ，Ｔｓｉｎｇｈ...

关键词： thin films interfacial reactions AlN substrate

Design of policy mechanism to promote cleaner production in china

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Journal of Environmental sciences 2001年第3期13卷 346-350页

作者： ZHANG Tian zhu(department of Environmental science and engineering, tsinghua university, beijing 100084, china. department of Environmental science and engineering Tsinghua University Beijing 100084 China. zhangtz@***

In order to promote cleaner production in china, a package of policy options was presented based on the identification of the barriers encountered in the CP demonstration project and the effectiveness and feasibility of policy options for the CP implementation were analyzed. Furthermore, the policy mechanism framework was given, which composes of compulsory, economic incentive, social pressure and supportive function. Finally, the implementation strategy of the policy mechanism, in which the emphasis will be changed from compulsory policy options towards economic and social pressure policy options, was proposed.

关键词： cleaner production barrier identification policy mechanism china

A New hcp Phase Formed in the Ni-Nb System during Ion-beam-assisted Deposition

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Journal of materials science & Technology 2004年第5期20卷 577-579页

作者： Bin ZHAO, Kuiwei GENG, Fei ZENG and Feng PANLaboratory of Advanced materials, department of materials science and engineering, tsinghua university, beijing 100084, china Lab. of Adv. Mat. Dept. of Mat. Sci. and Eng. Tsinghua Univ. Beijing 100084 China

The Ni80Nb20 films were prepared by ion beam assisted deposition (IBAD) with various Ar+ ion energies. A phase evolution of fcc→amorphous→Ni+Nb→Ni+hcp was observed with the increasing of ion beam energy from 2 keV to 8 keV. When bombarded by Ar+ ions of 8 keV during deposition, a new crystalline phase with hcp structure was obtained, of which the lattice parameters are a=0.286 nm and c=0.483 nm, different from those of the similar A3B-type hcp phase previously reported. The experimental results were discussed in terms of thermodynamics and restricted kinetic conditions in the far-from-equilibrium process of IBAD. The formation of hep phase may also be related to the valence electron effect.

关键词： Hcp phase Ni-Nb Ion beam assisted deposition Thermodynamics Valence electron effect

HIGH TEMPERATURE OXIDATION AND STRUCTURE OF SCALE AND WHISKERS FOR Fe-Ni-Cr SEALING ALLOYS

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Acta Metallurgica Sinica(English Letters) 1993年第8期6卷 147-150页

作者： DONG Zhili MA Jusheng TANG Xiangyun YOU Liang tsinghua university,beijing,china lecturer department of materials science and engineering,tsinghua university,beijing 100084,china tsinghua Univ Beijing China

The oxidation rate,the growth,morphology and structure of oxide scale and whiskers for Fe-Ni-Cr sealing alloys in H_2-H_2O atmosphere at high temperatures have been studied. The growth rate of scale is controlled by *... 详细信息

关键词： oxidation oxide scale oxide whisker Fe-Ni-Cr sealing alloy