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Effect of As Interstitial Diffusionon on the Properties of Undoped Semi-insulating LECGaAs

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Rare Metals 2001年第3期20卷 187-191页

作者： Ruixia Yang, Fuqiang Zhang, Nuofu Chen 1) Hebei University of technology, Tianjin 300130, china 2. {2. of Semiconductors, chinese academy of sciences, Beijing 100083, china Hebei Univ Technol Tianjin 300130 Peoples R China chinese Acad Sci Inst Semicond Beijing 100083 Peoples R China

Annealing was carried out at 950 and 112. degreesC under various As pressure for undoped (ND) semi-insulating (SI) LECGaAs. The effects of annealing on native defects and electrical properties were investigated. Experimental results indicate that, after an annealing at 950 degreesC for 14 h under low As pressure, the Hall mobility decreases and the resistivity increases dramatically for the samples. These changes in electrical properties are due to the generation of intrinsic acceptor defects, and the generation of the intrinsic acceptor defects originates from the outdiffusion of As interstitial at high temperature. The generation of the intrinsic defects and these changes in electrical properties can be suppressed by increasing the applied As pressure during annealing. The concentration of the main donor defect E12.(AsGaVGa) can be decreased by about one order of magnitude by an evacuated annealing at 112. degreesC for 2.8 h followed by a fast cooling. The decrease in E12.concentration can also be suppressed by increasing the As pressure during annealing.

关键词： semi-insulating GaAs intrinsic acceptor defects As interstitial indiffusion As pressure annealing

Monte Carlo calculation method on low energy electronscattering in polybasic medium

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chinese Science Bulletin 1998年第2期43卷 171-174页

作者： TAN Zhenyu 1 and HE Yancai 2.1. College of Electric Power, Shandong University of technology, Jinan 2.0061, china 2. Shanghai {2. of Ceramics, chinese academy of sciences, Shanghai 2.0050, china College of Electric Power Shandong University of Technology Jinan China Shanghai institute of Ceramics Chinese Academy of Sciences Shanghai China

A novel Monte Carlo method of simulating low energy electron (LEE) scattering in polybasic medium is presented. The Mott cross section is adopted to describe the elastic scattering of LEE, and a mean cross section idea is proposed instead of usual determination of the scattering center. The Joy’’s modified Bethe equation is used to calculate energy loss of LEE. The scattering processes of LEE in bulk PMMA have been simulated. And the electron backscattering coefficients, the electron interaction range and energy dissipation distribution of LEE in bulk PMMA have been calculated and compared with those calculated by the method of determining scattering center.

关键词： low_energy electron scattering Monte Carlo method cross_section.

Friction-reducing and antiwear behavior of metal halide-stabilized linear phosphazene derivatives as lubricants for a steel-on-steel contact

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Science china(Technological sciences) 2005年第3期48卷 282-291页

作者： ZHU Jiamei 1,2., LIU Weimin 2.& LIANG Yongmin 2.1. School of Chemical Engineering and technology, china University of Mining and technology, Xuzhou 2.1008, china 2. State Key Laboratory of Solid Lubrication, Lanzhou institute of Chemical Physics, chinese academy of sciences, Lanzhou 730000, china 1. School of Chemical Engineering and technology China University of Mining and Technology 221008 Xuzhou China 2. State Key Laboratory of Solid Lubrication Lanzhou Institute of Chemical Physics Chinese Academy of Sciences 730000 Lanzhou China

A series of novel metal halide-stabilized linear phosphazene derivatives were synthesized. The friction-reducing and antiwear abilities of the resulting products as the lubricants for a steel-on-steel contact were comparatively investigated on an Optimol SRV oscillating friction and wear tester. The morphology of the worn steel surface was observed on a scanning electron microscope, while the chemical states of some typical elements on the worn steel surface were examined by means of X-ray photoelectron spectroscopy. It was found that both the side branch structures and central metals influenced the friction-reducing and antiwear behaviors of the synthetic derivatives as the lubricants, which was related to the different adsorption activities of the organic compounds composed of different organic ingredients and metallic ions on a nascent metal surface. All the synthetic lubricants except for the iron (III) derivative showed increased antiwear abilities with increasing metallic ionic radius. A protective layer originated from the tribochemical reaction together with the adsorbed boundary lubricating layer containing organic fluorine compounds, nitrogen oxide, and Fe 3 (PO 4 ) 2.plays an important role in improving the friction and wear behavior of the steel-on-steel system.

关键词： metal halide-stabilized linear phosphazene derivatives,lubricant,steel,tribological properties.

Experimental investigation and numerical simulation on the effect of fissure water pressure in vertical sliding surface

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Science china(Technological sciences) 2005年第z1期48卷 53-64页

作者： ZHANG Lei1,2. LI Shihai1, LIAN Zhenzhong1,2.& WANG Yuannian1 1. institute of Mechanics, chinese academy of sciences, Beijing 100080, {2. 2. Graduate School, chinese academy of sciences, Beijing 100060, {2. 1. institute of Mechanics Chinese Academy of Sciences 100080 Beijing China 2. Graduate School Chinese Academy of Sciences 100060 Beijing China

This paper studies the effect of fissure water pressure in different fractures on the critical angle of landslide by laboratory investigation and numerical simulation in order to understand the mechanisms of fissure water pressure on landslide stability. Laboratory observations show that the effect of fissure water pressure on the critical angle of landslide is little when the distance between water-holding fracture and slope toe is three times greater than the depth of fissure water. These experimental results are also simulated by a three-dimensional face-to-face contact discrete element method. This method has included the fissure water pressure and can accurately calculate the critical angle of jointed slope when fissure water pressure in vertical sliding surface exists. Numerical results are in good agreement with experimental observations. It is revealed that the location of water-holding structural surface is important to landslide stability. The ratio of the distance between water-holding fissure and slope toe to the depth of fissure water is a key parameter to justify the effect of fissure water pressure on the critical angle of landslide.

关键词： jointed rock slope, discrete element method, fracture in vertical sliding surface, model experiment,fissure water pressure.

Explicit analytical solutions of the anisotropic Brinkman model for the natural convection in porous media(Ⅱ)

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Science china(Physics,Mechanics & Astronomy) 2005年第4期48卷 422-430页

作者： CAI Ruixian1, GOU Chenhua1, 2.& ZHANG Na1 1. institute of Engineering Thermophysics, chinese academy of sciences, Beijing 100080, {2. 2. Graduate School, chinese academy of sciences, Beijing 100080, {2. 1. institute of Engineering Thermophysics Chinese Academy of Sciences 100080 Beijing China 2. Graduate School Chinese Academy of Sciences 10080 Beijing China

Some algebraically explicit analytical solutions are derived for the anisotropic Brinkman model―an improved Darcy model―describing the natural convection in porous media. Besides their important theoretical meaning (for example, in analyzing the non-Darcy and anisotropic effects on the convection), such analytical solutions can be the benchmark solutions that can promote the development of computational heat and mass transfer. Some solutions considering the anisotropic effect of permeability have been given previously by the authors, and this paper gives solutions including the anisotropic effect of thermal conductivity and the effect of heat sources.

关键词： explicit analytical solution, porous medium, natural convection, Brinkman model, anisotropic.

Structures and physical properties of rigid polyurethane foams with water as the sole blowing agent

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Science china Chemistry 2006年第4期49卷 363-370页

作者： LI Xiaobin1,2. CAO Hongbin1 & ZHANG Yi1 1. institute of Process Engineering, chinese academy of sciences, Beijing 100080, {2. 2. Graduate School of the chinese academy of sciences, Beijing 100039, {2. 1. institute of Process Engineering Chinese Academy of Sciences Beijing 100080 China 2. Graduate School of the chinese academy of sciences Beijing 100039 China

Rigid polyurethane foams blown by varying water level were prepared in this study. The structures and physical properties of rigid polyurethane foams blown by water were measured with FT-IR, universal testing machine (Instron3365), scanning electron microscope (SEM) and differential scanning calorimeter (DSC). The results show that polyurea and polybiuret were the typical charac- teristics, and the cream time and gel time were shorter for the fully water blown rigid foams than that for the fully cyclopentane blown foams. The density of foam samples decreased from 45.0 kg/m3 to 2..4 kg/m3 with the increase of water level from 3 pph to 7 pph. Compressive strength exhibited the similar behavior with density. The average cell size of foam samples ranged from 2.1 μm to 356 μm with the increase of water level from 3 pph to 7 pph, respectively. At the same time, poorer dimen- sional stability was encountered with the increase of average cell size due to fast diffusion rate of CO2.out of the foam. The results of thermal analysis show that the glass transition temperature (Tg) shifted to a higher temperature with the increase of isocyanate level when more water was used as chemical blowing agent.

关键词： polyether polyol, polyurethane rigid foam, compressive strength, dimensional stability, cell size, glass transition temperature.

The GPS-gravimetry boundary value problem

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Science china Earth sciences 2005年第3期48卷 398-405页

作者： YU Jinhai1,2.& ZHANG Chuanding2.1. institute of Geodesy and Geophysics of chinese academy of sciences, Wuhan 430077, {2. 2. Zhengzhou Information Engineering University, Zhengzhou 450052. {2. 1. institute of Geodesy and Geophysics of chinese academy of sciences 430077 Wuhan China 2. Zhengzhou Information Engineering University 450052 Zhengzhou China

How to determine the earth’s external gravity field with the accuracy of O(T2. by making use of GPS data and gravity values measured on the earth’s surface is dealt with in this paper. There are two main steps: to extend these measured values on the earth’s surface onto the reference ellipsoid at first and then to seek for the integral solution of the external Neumann problem outside the ellipsoid. In addition, the corresponding judging criteria of accuracy to solve the GPS-gravity boundary value problem are established. The integral solution given in the paper not only contains all frequency-spectral information of the gravity field with the accuracy of O(T 2., but is also easily computed. In fact, the solution has great significance for both theory and prac- tice.

关键词： Neumann boundary value problem, integral solution, gravity disturbance.

High-temperature phases of pyrophyllite and their evolutionary characteristics

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chinese Science Bulletin 1997年第2期42卷 140-144页

作者： WANG Ling and ZHANG Zhenyu1. Changsha institute of Geotectonics, chinese academy of sciences, Changsha 410013, {2. 2. institute of Geology, chinese academy of sciences, Beijing 10002., {2. Changsha institute of Ceotectonics Chinese Academy of Sciences Changsha China institute of Geology Chinese Academy of Sciences Beijing China

WITH the increase of heating temperature, phase of pyrophyllite will undergo a series of transformations. Former scholars have done some work in this respect; the temperature spans,however, were normally not more than 1150℃ and no relatively comprehensive results have been reported. Thus, the features of the phases from indoor temperature to melting point (1710℃±) for pyrophyllite and the entire evolutionary process of the phases are uncertain.

关键词： pyrophyllite high-temperature phase phase tranformation pyrophyllite anhydrite mullite cristobalite.

Adjoint method for the optimum planning of industrial pollutant sources

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Science china Earth sciences 2005年第8期48卷 1270-1279页

作者： LIU Feng1,2. HU Fei2.& ZHU Jiang2.1. College of Environmental sciences, Peking University, Beijing 100871, china 2. LAPC, {2. of Atmospheric Physics, chinese academy of sciences, Beijing 10002., china 1. College of Environmental sciences Peking University 100871 Beijing China 2. LAPC Institute of Atmospheric Physics Chinese Academy of Sciences 100029 Beijing China

The optimum planning of industrial pollutant sources, which optimizes the economic object without violating environmental constraints, is an important and hard task to be conquered. In this paper, an adjoint method is developed to solve the problem. The penalty function is in-troduced to deal with the environmental inequality constraints, and Lagrange function is con-structed to derive the adjoint equation and the gradient of the object function. In this means, the gradient of the object function can be calculated by solving the adjoint equation, and the infor-mation from the gradient is used to make the object function descend and approach to an optimal solution after some iterations. A two-dimensional, simplified model is used for numerical experi-ments. The theoretical derivations are verified by the results of the experiments. Furthermore, the adjoint method is shown to be of excellent convergence and efficiency, which is adaptive to the fast development of air quality numerical models and super computers.

关键词： optimum planning, industrial pollutant sources, adjoint equation, penalty function, gradient.