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Experimental study on interaction between simulated sandstone and acidic fluid

petroleum Science 2009年第1期6卷 8-16页

作者： Zhang Yongwang Zeng Jianhui Yu Bingsong state key laboratory of petroleum resource and prospecting China University of Petroleum Beijing 102249 China Basin and Reservoir Research Center China University of Petroleum Beijing 102249 China state key laboratory of Geological Processes and Mineral resources China University of Geosciences Beijing 100083 China

In order to investigate the controlling mechanism of temperature, fluid and other factors on water-rock interaction in the diagenetic process, we performed a series of simulated experiments on the interaction between two kinds of fluids with different salinity and a composite mineral system （simulated sandstone）, which contains albite, K-feldspar and other minerals. The experimental results showed that acidity was the most important factor that affected the dissolution of minerals in the composite mineral system. The lower the pH value, the more easily the minerals dissolved. At the same pH value, the dissolution abilities of different acids for various mineral components were also different. Compared to hydrochloric acid （inorganic acid）, oxalic acid （organic acid） was more able to dissolve aluminosilicate minerals. However, the dissolution ability of oxalic acid for carbonate minerals was lower than that of hydrochloric acid. In the process of fluid-rock interaction, dissolution of feldspar was relatively complicated. Increase of temperature would accelerate the dissolution of feldspar. Under acidic conditions, albite had a higher dissolution rate than K-feldspar. K-feldspar could dissolve and convert into montmorillonite and kaolinite, while albite could dissolve and convert into kaolinite both at 40℃ and 80℃. Presence of organic acid, and decrease of pH value and water salinity were all favorable for the dissolution of feldspar, but weakened the ability to form clay minerals.

关键词： Fluid simulated sandstone dissolution static experiment

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Thin bed responses and correction methods for cased hole density logging

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petroleum Science 2008年第4期5卷 322-325页

作者： Wu Wensheng Zhang Yuling state key laboratory of petroleum resource and prospecting China University of Petroleum Beijing 102249 China china National Logging Corporation CNPC Beijing 100101 China

The study of the thin bed responses and correction methods in cased hole density logging can provide a theoretical basis for research to improve data processing methods. By using the Monte Carlo program MCNP, the change of detector count from thin beds with the vertical depth was calculated at different casing thicknesses. The calculation showed that with the low density thin bed moving upward, detector count first increased to a maximum then decreased. The responses of a thin bed with a high density were opposite to those of a thin bed with a low density. The change curve was symmetrical, and the maximums or minimums appeared at the midpoint between the detector and source. Besides, detector count increased with increasing thin bed thickness. At a specific thin bed thickness, further increase of thin bed thickness resulted in a slow increase of detector count then the count rate leveled off. In actual logging, the influence of adjacent formations on density log measurements can be ignored. Finally, based on numerical simulation correction methods for the dual influence of casing and thin beds are discussed.

关键词： Density logging in cased hole thin bed response casing MCNP program correcting

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Multi-level decollement zones and detachment deformation of Longmenshan thrust belt,Sichuan Basin,southwest china

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Science china Earth Sciences 2008年第S2期51卷 32-43页

作者： TANG LiangJie1,2,3,YANG KeMing4,JIN WenZheng1,2,3,L ZhiZhou4 & YU YiXin1,2,3 1 state key laboratory of petroleum resource and prospecting,china university of petroleum,beijing 102.4.,china 2 key laboratory for Hydrocarbon Accumulation Mechanism,china university of petroleum,Ministry of Education,beijing 102.4.,china 3 Basin and Reservoir Research Center,china university of petroleum,beijing 102.4.,china 4 Southwest Division Company,SINOPEC,Chengdu 610081,china 1. state key laboratory of petroleum resource and prospecting China University of Petroleum Beijing 102249 China 2. key laboratory for Hydrocarbon Accumulation Mechanism China University of Petroleum Ministry of Education Beijing 102249 China 3. Basin and Reservoir Research Center China University of Petroleum Beijing 102249 China 4. Southwest Division Company SINOPEC Chengdu 610081 China

As is well known that many decollement layers were developed in the Longmenshan thrust belt,Si-chuan Basin,china. Through field investigation,explanation of seismic profiles and analysis of the balanced sections,we can divide the decollement zones into 3 categories: (1) the deep level decolle-ment zones,including the crust-mantle decollement layer,intracrustal decollement layer,and presinian basal decollement layer. The main structural styles of their deformation are the crust-mantle decoup-ling detachment deformation,the basal ductile shear deformation,etc.; (2) the middle level decollement zones,including the Cambrian-Ordovician decollement layer,the Silurian decollement layer,etc.,the main structural styles of their deformation are the isopachous fold,the angular fold,the saddle struc-ture,and the combination styles of them; and (3) the shallow level decollement zones,including the Xujiahe Formation decollement layer of Upper Triassic and the Jurassic decollement layers,the main structural styles of their deformation are the thrust-nappe tectonic,the pop-up,the triangle zone ,the duplex,etc. Multi-level decollement zones not only made the Longmenshan thrust belt develop many different deformation styles from deep place to shallow place,but also made some local areas have the superimposition of the tectonic deformation apparently. This study indicates that the multi-level de-collement zones have a very important effect on the shaping and evolution of the Longmenshan thrust belt.

关键词： decollement layer structural styles multi-level decollement zones Longmenshan thrust belt

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The role of the catalysts with highly dispersed and isolated active sites in the selective oxidation of light hydrocarbons

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Progress in Natural Science:Materials International 2005年第12期15卷 1066-1072页

作者： WANG Hongxuan and ZHAO Zhen state key laboratory of Heavy Oil Processing,china university of petroleum,beijing 102.4.,china state key laboratory of Heavy Oil Processing China University of Petroleum Beijing 102249 China

This review summarizes the role of catalysts with highly dispersed and isolated active sites (active sites:supported atoms f≤0.5 %) in the selective oxidation of light hydrocarbons,such as methane,ethane and propane,into oxygenates and the epoxidation of *** plausible structures of the highly dispersed and isolated active species,as well as their effects on the catalytic performances are *** special physico-chemical properties and the functional mechanism of the catalysts with highly dispersed and isolated active sites,as well as the preparation,characterization of the catalysts with highly dispersed and isolated active sites and their applications in other types of reactions of lower hydrocarbons are summarized.

关键词： selective oxidation light hydrocarbons highly dispersed isolated active sites oxygenates catalyst methane ethane propane

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Distribution,formation and evolution of sand ridges on the East china Sea shelf

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Science china(Technological Sciences) 2010年第3期53卷 822-828页

作者： ZHAO RenBao 1,2,SUN HaiTao 3,WU YaSheng 3 &ZHAO ChuanFeng 1,2 1MOE key laboratory of petroleum Engineering,china university of petroleum,beijing 102.4.,china 2 Enhanced Oil Recovering Research Center,china university of petroleum,beijing 102.4.,china 3Faculty of Natural resource&Information Technology,china university of petroleum,beijing 102.4.,china 1. MOE key laboratory of petroleum Engineering China University of Petroleum Beijing 102249 China2. Enhanced Oil Recovering Research Center China University of Petroleum Beijing 102249 China3. Faculty of Natural Resource & Information Technology China University of Petroleum Beijing 102249 China

Influence of CO2 corrosion on reservoir mineralogical composition,pore structure and their mechanical characteristics was studied using XRD,SEM,rock tri-axial machine and core flow experimental *** was found that the corrosion effect was mainly attributed to rock texture and structure,fluid composition and external dynamical conditions in the experimental *** cores with bedding structures,their bedding surfaces were the preferential corrosion regions,because micro-cracks would evolve at these surfaces in the pressure-releasing ***,for cores with massive structures controlled by stable water environment,the CO2 corrosion would result in pore enlargement and secondary pore *** gas velocity from outlet showed sharp increase in the injection process of CO2-H2O *** could be explained by two changes caused by *** was the opening and closure of *** other was particle *** the corrosion time increased,both tensile strength and compressive strength decreased,which confirmed decrease of cementation *** should also be noted that permeability increase and micro-cracks generation would pose damage to the capacity of CO2 geological storage.

关键词： carbon dioxide geological storage mineralization enhanced oil recovery corrosion

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A local f-x Cadzow method for noise reduction of seismic data obtained in complex formations

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petroleum Science 2011年第3期8卷 269-277页

作者： Yuan Sanyi Wang Shangxu state key laboratory of petroleum resources and prospecting China University of Petroleum Beijing 102249 China

A noise-reduction method with sliding called the local f-x Cadzow noise-reduction method, windows in the frequency-space （f-x） domain, is presented in this paper. This method is based on the assumption that the signal in each window is linearly predictable in the spatial direction while the random noise is not. For each Toeplitz matrix constructed by constant frequency slice, a singular value decomposition （SVD） is applied to separate signal from noise. To avoid edge artifacts caused by zero percent overlap between windows and to remove more noise, an appropriate overlap is adopted. Besides flat and dipping events, this method can enhance curved and conflicting events. However, it is not suitable for seismic data that contains big spikes or null traces. It is also compared with the SVD, f-x deconvolution, and Cadzow method without windows. The comparison results show that the local Cadzow method performs well in removing random noise and preserving signal. In addition, a real data example proves that it is a potential noise-reduction technique for seismic data obtained in areas of complex formations.

关键词： Cadzow sliding window noise reduction fidelity complex formations Toeplitz matrix,singular value decomposition

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The distribution rule and seepage effect of the fractures in the ultra-low permeability sandstone reservoir in east Gansu Province,Ordos Basin

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Science china Earth Sciences 2008年第S2期51卷 44-52页

作者： ZENG LianBo1,GAO ChunYu2,QI JiaFu1,WANG YongKang2,LI Liang2 & QU XueFeng2 1 state key laboratory of petroleum resource and prospecting,china university of petroleum,beijing 102.4.,china 2 Changqing Oilfield Branch,Petrochina,Xi’an 163517,china china Univ Petr State Key Lab Petr Resource & Prospecting Beijing 102249 Peoples R China Petrochina Changqing Oilfield Branch Xian 163517 Peoples R China

To study the impact of the fractures on development in the ultra-low permeability sandstone reservoir of the Yangchang Formation of the Upper Triassic in the Ordos Basin,data on outcrops,cores,slices,well logging and experiments are utilized to analyze the cause of the formation of the fractures,their distribution rules and the control factors and discuss the seepage flow effect of the fractures. In the studied area developed chiefly high-angle tectonic fractures and horizontal bedding fractures,inter-granular fractures and grain boundary fractures as well. Grain boundary fractures and intragranular fractures serve as vital channels linking intragranular pores and intergranular solution pores in the reservoir matrix,thus providing a good connectivity between the pores in the ultra-low perme-ability sandstone reservoir. The formation of fractures and their distribution are influenced by such external and internal factors as the palaeo-tectonic stress field,the reservoir lithological character,the thickness of the rock layer and the anisotropy of a layer. The present-day stress field influences the preservative state of fractures and their seepage flow effect. Under the tec-tonic effect of both the Yanshan and Himalayan periods,in this region four sets of fractures are distributed,respectively assuming the NE-SW,NW-SE,nearly E-W and nearly S-N orientations,but,due to the effect of the rock anisotropy of the rock formation,in some part of it two groups of nearly orthogonal fractures are chiefly distributed. Under the effect of the present-day stress field,the fractures that assume the NE-SW direction have a good connectivity,big apertures,a high permeability and a minimum starting pressure,all of which are main advantages of the seepage fractures in this region. With the development of oilfields,the permeability of the fractures of dif-ferent directions will have a dynamic change.

关键词： fracture genetic type distribution characteristic seepage flow effect ultra-low permeability sandstone reservoir Ordos Basin

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Effect of regularization parameters on geophysical reconstruction

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petroleum Science 2009年第2期6卷 119-126页

作者： Zhou Hui Wang Zhaolei Qiu Dongling Li Guofa Shen Jinsong state key laboratory of petroleum resource and prospecting China University of Petroleum Beijing 102249 China key laboratory of CNPC Geophysical prospecting China University of Petroleum Beijing 102249 China Research Institute Bureau of Geophysical Prospecting Hebei 072751 China china university of petroleum Beijing 102249 China

In this paper we discuss the edge-preserving regularization method in the reconstruction of physical parameters from geophysical data such as seismic and ground-penetrating radar data. In the regularization method a potential function of model parameters and its corresponding functions are introduced. This method is stable and able to preserve boundaries, and protect resolution. The effect of regularization depends to a great extent on the suitable choice of regularization parameters. The influence of the edge-preserving parameters on the reconstruction results is investigated and the relationship between the regularization parameters and the error of data is described.

关键词： Geophysical data inversion error of data regularization regularization parameters

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The multi-factor recombination and processes superimposition model for hydrocarbon accumulation:application to the Silurian in the Tarim Basin

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petroleum Science 2008年第1期5卷 13-19页

作者： Meng Qingyang Pang Xiongqi Gao Jianbo state key laboratory of petroleum resource and prospecting China University of Petroleum Beijing 102249 China Basin and Reservoir Research Center China University of Petroleum Beijing 102249 China Research Center CNOOC Beijing 100027 China

The multi-factor recombination and processes superimposition model for hydrocarbon accumulation is put forward in view of the hydrocarbon geological characteristics of multiple episodes of structural evolution, multiple sets of source-reservoir-seal assemblage, multiple cycles of hydrocarbon accumulation and multiple episodes of readjustment and reconstruction in the complex superimposed basins in china. It is a system including theories and methods that can help to predict favorable exploration regions. According to this model, the basic discipline for hydrocarbon generation, evolution and distribution in the superimposed basins can be summarized in multi-factor recombination, processes superimposition, multiple stages of oil filling and latest stage preservation. With the Silurian of the Tarim basin as an example, based on the reconstruction of the evolution history of the four factors （paleo-anticline, source rock, regional cap rock and kinematic equilibrium belt） controlling hydrocarbon accumulation, this model was adopted to predict favorable hydrocarbon accumulation areas and favorable exploration regions following structural destruction in three stages of oil filling, to provide guidance for further exploration ofoil and gas in the Silurian of the Tarim basin.

关键词： Multi-factor recombination processes superimposition Tarim Basin Silurian favorable exploration region prediction

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Multiphase tectonic movements, cap formations and evolution of the Majiang paleo-reservoir

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petroleum Science 2011年第2期8卷 127-133页

作者： Tang Liangjie Cui Min state key laboratory of petroleum resources and prospecting China University of Petroleum Beijing 102249 China CNOOC Research Institute Beijing 100027 China

The Majiang paleo-reservoir is a typical destroyed hydrocarbon reservoir, buried in carbonate strata of china＇s southern marine-facies. Field geological explorations, interpretations of seismic profiles and balanced cross-section restorations around this paleo-reservoir reveal that its formation and evolution have been restricted by multiphase tectonic movements of different intensities. A regional tectonic mechanism and model have been suggested for the formation and evolution of the Majiang paleo- reservoir. Geological field exploration has been carried out along three typical Silurian cross-sections and rock samples were tested in combination with water-rock interaction. Based on the result of cap tests, the planar distribution, the residual thickness, the erosion thickness and the preservation conditions, the Silurian mudstone cap is discussed around the Majiang paleo-reservoir. Combining the hydrodynamic conditions of its formation and evolution and its tectonic movements, we determined the fact that the thicker the cap is, the more resistant it is to hydrodynamic destruction. The multi-phase formation and destructive geological model of the paleo-reservoir is established through an overall analysis of multi- phase tectonic evolutions, cap developments, hydrodynamic conditions and solid mineral metallogenic ages measured by Rb-Sr, Pb and Sm-Nd isotope techniques.

关键词： Multiphase tectonic evolution key tectonic changes cap evolution hydrocarbonpreservation Majiang paleo-reservoir

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