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Phase transition in the Zr_(60)Al_(15)Ni_(25) bulk metallic glass subjected to rolling at room temperature

science China(Technological sciences) 2006年第6期49卷 655-662页

作者： YAN Zhijie1, 2, LI Jinfu1, ZHOU Yaohe1 & WU Yanqing3.1. State Key Laboratory of Metal Matrix Composites, school of Materials science and Engineering, shanghai Jiao Tong {3., shanghai 20003., China 2. school of Materials science and Engineering, Taiyuan {3. of science and technology, Taiyuan 03.024, China 3. school of Environmental science and Engineering, shanghai Jiao Tong {3., shanghai 20003., China State Key Laboratory of Metal Matrix Composites School of Materials Science Engineering Shanghai Jiao Tong University Shanghai 200030 China school of Materials science Engineering Taiyuan University of Science technology Taiyuan 030024 China school of Environmental science Engineering Shanghai Jiao Tong University Shanghai 200030 China

The microstructure evolution of the Zr60Al15Ni25 metallic glass during rolling at room temperature is investigated by X-ray diffraction (XRD), differential scanning calorimetry (DSC); high-resolution transmission electron microscopy (HREM). The results show that the values of full width at half maximum (FWHM) of the XRD patterns; exothermic enthalpy ΔH of DSC plots do not monotonically change with the variation of deformation degrees . As is not large than 20%, the values of FWHM; ΔH are lower than that of the as-cast state. When reaches 3.%, the values of FWHM; ΔH become larger than that of the as-cast state, while their values begin to decrease again as reaches about 85%. These results indicate that the reversible transitions between ordered; disordered atomic configurations occur during rolling, which is further verified by the HREM images. The reversible phase transition can be explained by the competition between the diffusion controlled reordering; shear-induced disordering during rolling.

关键词： metallic glasses, plastic deformation, phase transformations, shear bands.

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Large-eddy simulations and vortex structures of turbulent jets in crossflow

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science China(Physics,Mechanics & Astronomy) 2007年第1期50卷 118-132页

作者： GUAN Hui1,2 & WU ChuiJie2 1 school of Mechanical and Power Engineering,east China university of {3. and technology,shanghai 20023.,China 2 Research Center for Fluid Dynamics,PLA university of {3. and technology,Nanjing 211101,China 1. school of Mechanical and Power Engineering East China University of Science and Technology Shanghai 200237 China 2. Research Center for Fluid Dynamics PLA University of Science and Technology Nanjing 211101 China

Using the method of large-eddy simulation, the 3.dimensional turbulent jets in crossflow with stream-wise and transverse arrangements of nozzle are simulated, emphasizing on the dynamical process of generation and evolution of vortex structures in these flows. The results show that the basic vortex structures in literatures, such as the counter-rotating vortex pair, leading-edge vortices, lee-side vortices, hanging vortices, kidney vortices and anti-kidney vortices, are not independent physical substances, but local structures of the basic vortex structure of turbulent jets in crossflow-the 3.D stretching vortex rings originating from the orifice of the nozzle, which is discovered in this study. Therefore, the most important large-scale structures of turbulent jets in crossflow are unified to the 3.D vortex rings which stretch and twist in stream-wise and swing in transverse directions. We also found that the shedding frequencies of vortex rings are much lower than the one corresponding to the appearance of leading-edge and lee-side vortices in the turbulent jets.

关键词： turbulent jet in crossflow coherent structure large-eddy simulation

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An improved approach to the efficient construction of and search operations in motion graphs

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science China(Information sciences) 2012年第5期55卷 1042-1051页

作者： GAO Yan 1,CHEN ZhiHua 2,CHEN MinGang 3.& SHEN Yang 3.1 Software Engineering Institute,east China Normal university,shanghai 200062,China 2 Department of Computer {3. and Engineering,east China university of {3. and technology,shanghai 20023.,China 3.Department of Computer {3. and Engineering,shanghai Jiao Tong university,shanghai {13.,China 1. Software Engineering Institute East China Normal University Shanghai 200062 China2. Department of Computer Science and Engineering East China University of Science and Technology Shanghai 200237 China3. Department of Computer Science and Engineering Shanghai Jiao Tong University Shanghai 200240 China

Motion graphs have been widely used as an effective technique in the synthesis of human *** synthesize well-formed motions,motion graphs require smooth transitions and good ***,the time and costs grow quadratically as the graph size *** this paper,we present a method to set up a hierarchical structure,called a structure *** coarse level of this graph models different motion categories and their transitions,and the fine level mainly captures different motion *** interpolation space method is used to improve the graph connectivity at the fine *** structure guides the establishment of a faster and more realistic graphical *** the building process,this structure also helps with searching the motion graph,by performing a traverse search and placing the findings into a direct look-up table or local search ***,when there is no direct link between the different motions,a navigation map is introduced to conduct an appropriate search path via a series of transition motion *** experimental results indicate that our approach could lower the computation time in construction and searching,while simultaneously providing a richer variety of motion styles.

关键词： motion graph structure table registration curve motion interpolation

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Chemical Extraction Preparation of Delithiated Cathode Materials of Li-ion Battery

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Journal of Wuhan university of technology(Materials science) 2009年第6期24卷 863-866页

作者：闫时建 school of Materials science and Engineering Taiyuan University of Science and Technology

A method of conventional chemical reaction to prepare delithiated cathode materials of Li-ion battery was introduced. The cathode material of Li-ion battery was mixed with oxidizing agent Na2S2O8 in water solution, and the solution was stirred continuously to make the chemical reaction proceed sufficiently, then the reaction product was filtered and finally the insoluble delithiated cathode material was obtained. A series of tests were conducted to verify the composition, crystal structure and electrochemical property of the delithiated cathode materials were all desirable. This method overcomes the shortcomings of battery charging preparation and chemical extraction preparation employing other oxidizing agents.

关键词： chemical extraction delithiated cathode material Li-ion battery

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Study on rare earth/alkaline earth oxide-doped CeO_2 solid electrolyte

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Rare Metals 2007年第4期26卷 311-316页

作者： YAN Kai ZHEN Qiang Song Xiwen school of Materials science and Engineering Shanghai University Shanghai 200072 China Research Center of Nanoscience and Nanotechnology Shanghai Univeesity Shanghai 200444 China school of Materials science and Engineering Inner Mongolia University of Science and Technology B aotou 014010 China

Five types of rare earth/alkaline earth oxide-doped CeO2 superfine-powders were synthesized by a low-temperature combustion technique. The relevant solid electrolyte materials were also sintered by pressureless sintering at different temperatures. The results of X-ray diffraction and transmission electron microscopy showed that the grain size of the powders was approximately 20-3. nm, and rare earth/alkaline earth oxides were completely dissolved into ceria-based solid solution with fluorite structure. The electrical conductivities of the SmzO3.CeO2 system were measured by the ac impedance technique in air at temperatures ranging from 513.900℃. The results indicated that the ionic conductivities of Srno.2oCe0.8Ol.875 solid electrolyte increase with increasing sintering temperature, and the relationship between the conductivities and measuring temperature obeys the An＇henius equation. Then the SmzO3.CeO2 material was further doped with other rare earth/alkaline earth oxide, and the conductivities improve with the effective index.

关键词： doped ceria rare earth/alkaline earth oxide solid electrolyte conductivity effective index

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Electrochemical Characteristic of Decarburization Reaction

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International Journal of Minerals,Metallurgy and Materials 1999年第1期13卷 27-30页

作者： Xionggang Lu Fushen Li Lifen Li Kouchih Chou (Applied science school, university of science and technology Beijing, Beijing 100083. China)(Material science and Engineering school, shanghai university, shanghai 200072, China) Applied science school University of Science and Technology Beijing Beijing 100083 China Material science and Engineering school Shanghai University Shanghai 200072 China

The electrochemical mechanism of the reaction between Fe-C melts and CaO-SiO2-Al2O3.FeOx slag systems has been carried out. The experimental results suggest that the final content of carbon in melt increases as the partial oxygen pressure of gas decreases no matter whether there is electronic conductor or not. However, the final content of carbon in the system with electronic conductor is much lower than that without electronic conductor. It can be deduced that the transfer ability of oxygen in slag is dominated by electrons. When an electronic conductor exists, an easy pathway for the electrons is provided and the oxygen transfer rate is accelerated.

关键词： melt-slag reaction decarburization electrochemistry electronic conductor

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Dynamic feedback robust stabilization of nonholonomic mobile robots based on visual servoing

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控制理论与应用（英文版） 2010年第2期8卷 139-144页

作者： Chaoli WANG 1 , Zhenying LIANG 2 , 3., Qingwei JIA 4 (1.Department of Control science and Engineering, university of shanghai for science and technology, shanghai 200093. China 2.Business school, university of shanghai for science and technology, shanghai 200093. China 3.school of science, Shandong university of technology, Zibo Shandong 255049, China 4.Research & Development Centre, Hitachi Asia Ltd, Hitachi Tower, Singapore 0493.8) Department of Control science and Engineering University of Shanghai for Science and Technology Shanghai China Business school University of Shanghai for Science and Technology Shanghai China school of science Shandong University of Technology Zibo Shandong China Research & Development Centre Hitachi Asia Ltd Hitachi Tower Singapore

This paper investigates the visual servoing robust stabilization of nonholonomic mobile robots. The calibration of visual parameters is not only complicated, but also needs great consumption of calculated time so that the accurate calibration is impossible in some situations for high requirement of real timing. Hence, it is interesting and important to consider the design of stabilizing controllers for nonholonomic kinematic systems with uncalibrated visual parameters. A novel uncertain model of these nonholonomic kinematic systems is proposed. Based on this model, a stabilizing controller is discussed by using dynamic feedback and two-step techniques. The proposed robust controller makes the mobile robot image pose and the orientation converge to the desired configuration despite the lack of depth information and the lack of precise visual parameters. The stability of the closed loop system is rigorously proved. The simulation is given to show the effectiveness of the presented controllers.

关键词： Nonholonomic system Uncalibrated visual parameters Stabilization Dynamic feedback

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The characteristics of arc beam shaping in hybrid plasma and laser deposition manufacturing

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science China(Technological sciences) 2006年第2期49卷 238-247页

作者： ZHANG Hai’ou1, QIAN Yingping1,3. WANG Guilan1 & ZHENG Qiguang2 1. school of Material science and technology, Huazhong {3. of science and technology, Wuhan 43.074, China 2. Institute of Laser technology and Engineering, Huazhong {3. of science and technology, Wuhan 43.074, China 3. Mechanical Engineering College, Hubei {3. of technology, Wuhan 43.068, China 1. school of Material science and technology Huazhong University of Science and Technology Wuhan 430074 China 3. Mechanical Engineering College Hubei University of Technology Wuhan 430068 China 2. Institute of Laser technology and Engineering Huazhong University of Science and Technology Wuhan 430074 China

As a new direct metal prototyping technology,the hybrid plasma and laser deposition manufacturing (PLDM) is proposed in this paper. In order to figure out the characteristics of plasma arc beam and mould in the PLDM process of high temperature alloy, the high speed CCD camera is used to obtain the picture around the plasma arc. Afterwards the sketch of picture is clearly obtained. And the effect of laser parameter, such as average power, pulse width, pulse repetition frequency and the angle between laser beam and plasma arc beam on the plasma arc appearance, is studied experimentally. The results show that the modality of plasma arc beam is markedly influenced by laser beam. And the improvements of shape precision and surface state of the layer deposited by PLDM are confirmed.

关键词： plasma hybrid laser, direct deposition, plasma arc beam, molding character, high-temperature alloy.

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Surface Nanocrystallization of Magnesium Alloy AZ91D by High-Energy Shot Peening

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Journal of Wuhan university of technology(Materials science) 2009年第4期24卷 515-519页

作者：张津 school of Materials science & Engineering University of Science and Technology Beijing College of Materials science & Engineering Chongqing University of Technology

High-energy shot peening （HESP）, a method to produce severe plastic deformation by high velocity flying balls, was applied on die cast magnesium alloy AZ91D. Effects of surface nanocrystallization by HESP and heat treatment at different temperatures were investigated. The mi- crostructure evolution was conducted using X-ray diffraction （XRD） and field emission scanning electronic microscopy （FESEM）. The hardness was measured by microhardness tester. The experimental results show that surface nanocrystrallization of AZ91D obtained by HESP would lead to the increase of microhardness. Low temperature heated at 100℃ for 1 h do not change the property obviously. However, both the microstructure and microhardness vary greatly after heat treatment at 400℃ for 1 h.

关键词： AZ91 D surface nanocrystallization HESP microhardnss corrosion resistance

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The mathematical model of wetting angle of heterogeneous nucleation

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science China(Technological sciences) 2004年第4期47卷 391-397页

作者： HUANG Cheng1, SONG Bo1, MAO Jinghong2 & ZHAO Pei3.1. school of Metallurgical and Ecological Engineering, university of science and {3. Beijing, Beijing 100083. China 2. school of Material science, university of science and {3. Beijing, Beijing 100083. China 3. Central Iron and Steel Research Institute, Beijing 100081, China 1. school of Metallurgical and Ecological Engineering University of Science and Technology Beijing 100083 Beijing China 2. school of Material science University of Science and Technology Beijing 100083 Beijing China 3. Central Iron and Steel Research Institute 100081 Beijing China

The heterogeneous nucleation has been analyzed in terms of the thermodynamic theory, and the mathematical model of wetting angle of heterogeneous nucleation has been developed based on the dynamic requirements of hetero- and homogeneous nucleation. With the wetting angel model, the wetting angles of different catalysts in liquid iron have been calculated. The result shows that the wetting angle of most catalysts is smaller than 40, and the value of f() is far less than 1. The wetting angles of TiN, TiC and RE2O3.are smaller, while the wetting angle of MnO is bigger among the ordinary nucleation catalysts. The wetting angles calculated by this model are in agreement with the results of other research work.

关键词： heterogeneous nucleation, mathematical model, wetting angle, undercooling.

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