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Effect and mechanism of stresses on rock permeability at different scales

Science china Earth Sciences 2006年第7期49卷 714-723页

作者： YIN Shangxian1 & WANG Shangxu2.1. Safety Engineering College, North china institute of Science and {2., Yanjiao, beijing 101601, china 2. Key Laboratory of Geophysics Exploration, china university of Petroleum, beijing 100083, china 1. Safety Engineering College North China Institute of Science and Technology Yanjiao Beijing 101601 China 2. Key Laboratory of Geophysics Exploration China University of Petroleum Beijing 100083 China

The effect of geo-stress fields on macroscopic hydro-geological conditions or micro-cosmic permeability of water-bearing media should follow some laws or principles. Cases study and tests show that: (1) At macro-geologic large scale, deformed and crashed rocks which were induced by geo-stress fields changing provided space for groundwater storage and flow. Groundwater adjusts water-bearing space and dilatants fractures by flowing and press transferring. Coupling of liquid and solid can be implemented for rocks and groundwater. Although tectonic fields witness several times of change and build-up in geological time, stress fields forming regional tectonic framework are coherent with seepage fields, orientation of the maximum horizontal stress demonstrates main seepage direc-tions. (2. At macro-geologic middle scale, zones of stresses changing sharply, quite low stresses, stress or shear concentration can be used to show locations and types of main fractures, zones of geo-stresses changing equably can be acted as normal base media zones of tri-porosity media. (3) At micro-geologic small scale, tri-porosity media include fractured rocks, porous rocks and capillary rocks. Investigations indicate that porosity or permeability is functions of effective stresses, and po-rosity or permeability changing rules of porous rocks with variation of effective stresses can be de-scribed as the index model, the model of power exponent functions is suitable for those of fractured rocks, the model of the second power parabola for capillary rocks. The porosity and permeability loss in fractured rocks, which are greater than that in porous rocks, are shown by calculation of effective compressive coefficient and closing pressure in cracks. The calculations can also explain the mecha-nism why porosity changes are always larger than permeability changes. It is proved by the thick wall cylinder theory that the second power parabola relation between porosity or permeability loss and effective

关键词： geo-stress fields, seepage fields, tri-porosity media, effective stresses, permeability, porosity,scale.

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The precipitation and effect of nano nitrides in HSLC steel

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Science china(Technological Sciences) 2008年第7期51卷 989-998页

作者： FU Jie1, LIU YangChun1,2.& WU HuaJie1,3 1 School of Metallurgical and Ecological Engineering, university of Science and technology {2., {2. 100083, china 2.Shougang technology research institute, Shougang (Group) Corporation, {2. 100041, china 3 Metallurgical Engineering research institute, university of Science and technology {2., {2. 100083, china 1. School of Metallurgical and Ecological Engineering University of Science and Technology Beijing Beijing 100083 China 2. Shougang technology research {2. Shougang (Group) Corporation Beijing 100041 China 3. Metallurgical Engineering research institute University of Science and Technology Beijing Beijing 100083 China

The existing forms of N and Al in HSLC (high strength low carbon) steel produced by TSCR (thin slab casting and rolling process), the precipitation thermodynamics and kinetics of AlN, and its effects on structure and mechanical property are studied. The experimental results show that only a small quantity of nitrogen is com- bined into AlN in HSLC steel produced by TSCR and most of the nitrogen in steel is still free nitrogen. Aluminum-nitride is mainly precipitated during the period of slow air cooling after coiling, but not during rolling and water cooling. The acid-soluble aluminum has no obvious effect on the grain size and mechanical property of HSLC steel produced by TSCR whose acid-soluble aluminum content is 0.005%―0.043%. The precipitation of AlN is not the main cause of grain refinement of HSLC steel produced by TSCR, nor is AlN the dominating precipitate that has precipitation strengthening effect. The nano nitrides are not pure AlN, but have complex compositions.

关键词： thin slab casting and rolling high strength low carbon steel AlN nano nitride precipitation strengthening

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Nanostructured Sulfide Composite Coating Prepared by Atmospheric Plasma Spraying

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材料工程 2006年第Z1期34卷 281-284页

作者： GUAN Yao-hui~1,XU Yang~1,ZHENG Zhong-yu~2.TONG Xiao-hui~2.1 Engineering College of china Agricultural university,{2. 100083,china 2.{2. research institute of Mechanical & Electrical technology,{2. 100083,china) Engineering College China Agricultural University Beijing 100083 China beijing research {2. of Mechanical and Electrical technology Beijing 100083 China

Nanostructured FeS-SiC coating was deposited by atmospheric plasma spraying（APS）.The microstructure and phase composition of the coating were characterized with SEM and XRD,*** addition,the size distribution of the reconstituted powders and the porosity of the coating have been *** was found that the reconstitiuted powers with sizes in the range of 2. to 80 μm had excellent flowability and were suitable for plasma spraying *** as-sprayed FeS-SiC composite coating exhibited a bimodal distribution with small grains（30～80nm） and large grains（100～2.0nm）.The coating was mainly composed of FeS and SiC,a small quantity of Fe1-xS and oxide were also *** porosity of the coating was approximately 19%.

关键词： plasma spraying nanostructured FeS-SiC composite coating

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Pattern phenomena in an rf discharge dusty plasma system

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Science china(Physics,Mechanics & Astronomy) 2006年第5期49卷 588-596页

作者： HUANG Feng1,2. YE Maofu2.& WANG Long2.1. College of Science, china Agricultural university, {2. 100083, china 2. institute of Physics, Chinese Academy of Sciences, {2. 100080, china 1. College of Science China Agricultural University Beijing 100083 China 2. institute of Physics Chinese Academy of Sciences Beijing 100080 China

Various dust patterns are observed in an rf discharge dusty plasma system. According to the dust growth process from small to large in size, the formation of different dust patterns can be divided into two stages: the small-particle stage (or dust cloud stage), and the large-particle stage (or dust crystal stage). The evolution relations between different dust patterns with gas pressure changing are investigated. Dust voids, dust acoustic waves and strong turbulence modes are presented at the small-particle stage. The self-organized dust lattices and dust clusters are investigated at the large-particle stage. The static structure of a dust lattice is characterized by means of the pair correlation function. Dust clusters formed by particles with different numbers and the regular evolution of the clusters with gas pressure are also investigated. The packing sequences of dust clusters are verified through two-dimensional confined molecular dynamics simulations.

关键词： dusty plasma dust patterns

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The mathematical model of wetting angle of heterogeneous nucleation

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Science china(Technological Sciences) 2004年第4期47卷 391-397页

作者： HUANG Cheng1, SONG Bo1, MAO Jinghong2.& ZHAO Pei3 1. School of Metallurgical and Ecological Engineering, university of Science and technology {2., {2. 100083, china 2. School of Material Science, university of Science and technology {2., {2. 100083, china 3. Central Iron and Steel research institute, {2. 100081, china 1. School of Metallurgical and Ecological Engineering University of Science and Technology Beijing 100083 Beijing China 2. School of Material Science University of Science and Technology Beijing 100083 Beijing China 3. Central Iron and Steel research institute 100081 Beijing China

The heterogeneous nucleation has been analyzed in terms of the thermodynamic theory, and the mathematical model of wetting angle of heterogeneous nucleation has been developed based on the dynamic requirements of hetero- and homogeneous nucleation. With the wetting angel model, the wetting angles of different catalysts in liquid iron have been calculated. The result shows that the wetting angle of most catalysts is smaller than 40, and the value of f() is far less than 1. The wetting angles of TiN, TiC and RE2.3 are smaller, while the wetting angle of MnO is bigger among the ordinary nucleation catalysts. The wetting angles calculated by this model are in agreement with the results of other research work.

关键词： heterogeneous nucleation, mathematical model, wetting angle, undercooling.

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Microstructure and Frictional Behavior of Fe-based Amorphous Metallic Coatings Prepared by Atmospheric Plasma Spraying

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稀有金属材料与工程 2011年第S3期40卷 160-165页

作者： Zhou Zheng1,2. Wang Lu2. He Dingyong1, Liu Yanbo2. Zhang Guanzhen1 1 beijing university of {2., beijing 10012., china 2.beijing institute of {2., beijing 100081, china beijing Univ Technol Beijing 100124 Peoples R China beijing Inst Technol Beijing 100081 Peoples R China

Amorphous metallic coatings with a composition of Fe48Cr15Mo14C15B6Y2.were prepared by means of atmospheric plasma spraying (APS) process under different conditions. The microstructure and frictional behavior were characterized simultaneously in this article. The results show that the as-deposited coatings consist of amorphous matrix and some precipitated nanocrystals, while the amorphous fraction and particle deformation as well as crystallization mechanism are significantly sensitive to the spraying parameters. The amorphous coatings express high microhardness and excellent wear resistance under dry frictional wear condition, which attributes to the inherent characteristic of amorphous phase and the dispersion strengthening of precipitated nanocrystals. The dominant wear mechanism of the amorphous coatings is fatigue wear accompanying with oxidative wear. In addition, the microhardness and wear resistance of the amorphous coatings were improved by optimizing spraying parameters, owing to the effect of both structural character and proper proportional of amorphous and nanocrystals fraction.

关键词： Fe-based amorphous coating APS microstructure friction

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Mineralogy and crystal structure determination of Mg-fillowite

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Science china Earth Sciences 2005年第5期48卷 635-646页

作者： MA Zhesheng 1 , SHI Nicheng 1 & YE Danian 2.1. china university of Geosciences, {2. 100083, china 2. institute of Geology, Chinese Academy of Sciences, {2. 10002., china 1. china university of Geosciences 100083 Beijing China 2. institute of Geology Chinese Academy of Sciences 100029 Beijing China

Accurate crystal structure determination of complex phosphate Mg-fillowite ? Na2.a(Mn4Mg2.e)7[PO4]6 has been finished. Mg-fillowite occurs in muscovite-pegmatite in the Altay area, Xinjiang, china. It is of the trigonal lattice, with space group R-3, unit cell a=1.5143(3) nm, c=4.3191(2. nm, V=8.5736 nm3, Z = 18. The R-factor of the determination accuracy is R (I > 2. ( I )) = 0.0776. The cationic polyhedra consist of two kinds of structural units: compound col- umn and screw column. In three-dimensional space, they are linked with each other through corner sharing or edge sharing to build the entire structure. There are 45 atoms in an asymmetric unit and 72. atoms in a unit cell. In terms of types and connection manners of the coordination polyhedra, the degree of complicity is rarely seen in all mineral crystal structures. Study of such a structure is significant for the classification of phosphate and the building rule of coordination polyhedra in a complex crystal structure.

关键词： Mg-fillowite, complex phosphate, crystal structure, coordination polyhedron.

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The correlation of multi-angle thermal infrared data and the choice of optimal view angles

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Science china Earth Sciences 2004年第6期47卷 570-576页

作者： FAN Wenjie1 & XU Xiru1,2.1.institute of Remote Sensing and gis of Peking {2.,beijing 100871,china 2.Center of Remote Sensing and gis of beijing Normal {2.,beijing 100875,china 1. institute of Remote Sensing and gis of Peking {2. 100871 Beijing China 2. Center of Remote Sensing and gis of beijing Normal {2. 100875 Beijing China

Based on the matrix formula of thermal infrared radiant system, the components temperature can be retrieved by the inversive matrix. Around the stability problem of retrieved result, the research work we did was focused on (i) the correlation of (wk,j) which is the key to affect the retrieval accuracy, (ii) a general method which can help us find the number of retrievable parameters and evaluate the retrieval error before its performance, (iii) the choice of “optimal viewing angle group” based on the formula of absolute error propagation. The row winter wheat field was chosen as an example. The results can provide a theoretical basis for multi-angle thermal infrared remote sensing and components temperature retrieval.

关键词： components temperature retrieval, correlation, number of retrievable parameters, optimal viewing angle group.

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Numerical simulation of Meiyu front and the diagnosis of moist vorticity vector

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Progress in Natural Science:Materials International 2007年第11期17卷 1341-1347页

作者： Ping Fan1,2.and Luo Zhexian2.1. institute of Atmospheric Physics, Chinese Academy of Sciences, beijing 10002., {2. 2. Nanjing university of Information Sciences & technology, Nanjing 2.0044, {2.) institute of Atmospheric Physics Chinese Academy of Sciences Beijing 100029 China Nanjing university of Information Sciences & technology Nanjing 210044 China

Moist vorticity vector is introduced to study the development and evolution of mesoscale convective vortex (MCV) in the Meiyu front precipitation with the Advanced Regional Predication System (ARPS). In this study, the heavy rainfall is simulated to investigate the genesis, development and dissipation of middle scale convective vortex, which occurred from 0000 UTC 3 July to 12.0 UTC 5 July over the Jianghuai River valley. Moist vorticity vector (MVV) has zonal, radial and vertical components in its 3D spatial distribution. The simulation shows that the vertical component of moist vorticity vector well demonstrates the spatial distribution characteristics of middle scale convective vortex, especially in the process of Meiyu front precipitation. Diagnosis upon zonal, radial averaged and mass-integrated quantities of MVV shows that its vertical component and the surface precipitating ratio are in phase with a correlation coefficient of 0.68, indicating that the vertical component of MVV is closely associated with the Meiyu front precipitation. In addition, the tendency of the vertical component of MVV is mainly determined by the interaction between the vorticity and the zonal and radial gradient of condensational or depositional heating.

关键词： moist vorticity vector mesoscale convective vortex Meiyu front precipitation

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Friction-reducing and antiwear behavior of metal halide-stabilized linear phosphazene derivatives as lubricants for a steel-on-steel contact

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Science china(Technological Sciences) 2005年第3期48卷 282-291页

作者： ZHU Jiamei 1,2., LIU Weimin 2.& LIANG Yongmin 2.1. School of Chemical Engineering and technology, china {2. of mining and technology, Xuzhou 2.1008, china 2. State Key Laboratory of Solid Lubrication, Lanzhou institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, china 1. School of Chemical Engineering and technology China University of Mining and Technology 221008 Xuzhou China 2. State Key Laboratory of Solid Lubrication Lanzhou Institute of Chemical Physics Chinese Academy of Sciences 730000 Lanzhou China

A series of novel metal halide-stabilized linear phosphazene derivatives were synthesized. The friction-reducing and antiwear abilities of the resulting products as the lubricants for a steel-on-steel contact were comparatively investigated on an Optimol SRV oscillating friction and wear tester. The morphology of the worn steel surface was observed on a scanning electron microscope, while the chemical states of some typical elements on the worn steel surface were examined by means of X-ray photoelectron spectroscopy. It was found that both the side branch structures and central metals influenced the friction-reducing and antiwear behaviors of the synthetic derivatives as the lubricants, which was related to the different adsorption activities of the organic compounds composed of different organic ingredients and metallic ions on a nascent metal surface. All the synthetic lubricants except for the iron (III) derivative showed increased antiwear abilities with increasing metallic ionic radius. A protective layer originated from the tribochemical reaction together with the adsorbed boundary lubricating layer containing organic fluorine compounds, nitrogen oxide, and Fe 3 (PO 4 ) 2.plays an important role in improving the friction and wear behavior of the steel-on-steel system.

关键词： metal halide-stabilized linear phosphazene derivatives,lubricant,steel,tribological properties.

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