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Indian Ocean-MORB-type isotopic signature of Yushigou ophiolite in North Qilian Mountains and its implications

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Science china Earth Sciences 2006年第6期49卷 561-572页

作者： HOU Qingye1,2. ZHAO Zhidan1,2. ZHANG Hongfei3. ZHANG Benren3.& CHEN Yuelong2.1. State Key Laboratory of Geological Processes and Mineral Resources,{3., Beijing 100083. china 2. School of Earth Science and Mineral Resources,{3., Beijing 100083. china 3. faculty of Earth Sciences,{3., wuhan 43.074, china 1. State Key Laboratory of Geological Processes and Mineral Resources China University of Geosciences Beijing 100083 China 2. School of Earth Science and Mineral Resources China University of Geosciences Beijing 100083 China 3. faculty of Earth Sciences China University of Geosciences Wuhan 430074 China

In order to explore the disputed issue concerning the tectonic affinity ofthe ancient ocean mantle of North Qilian Mountains (NQM), geochemical and Sr, Nd, Pb isotopiccompositions of pillow basalts of the Yushigou Ophiolite (YSGO) suite from NQM have been analyzedsystematically. The pillow basalts exhibit tholeiitic characteristics, with flatchondrite-normalized REE patterns ((La/Yb)_N = 0.98—1.2.). They display no Nb, Ta, Zr, Hf negativeanomalies, and show MORB features in 2.b-Zr/4-Y and Ti/100-Zr-YX3.tectonic discrimination *** results indicate that the Yushigou ophiolite is most likely to be formed in a mid-ocean ridgeor mature back-arc basin. Their isotopic data show a relatively broad and enriched ^(87)Sr/^(86)Sr(0.70509 — 0.70700), restricted ^(143.Nd/^(144)Nd (0.512.55-0.512.78). Pb isotopes are in the rangeof ^(2.6)Pb/^(2.4)Pb (18.054-2..562., ^(2.7)Pb/^(2.4)Pb (15.53.-15.743. and ^(2.8)Pb/^(2.4)Pb(3..068-3..53.). These isotopic data imply that the basalts originated from the depleted mantle(DMM), with the involvement of enriched mantle components (mainly EMII). Geochemical comparisonsbetween the basalts in YSGO and the MORB-type basalts of ophiolite suites occurring in the knownancient Tethyan tectonic domain indicate that the ancient oceanic mantle represented by YSGO suiteforming in early Paleozoic in the North Qilian Moutains is very similar to the Tethyan mantle inboth trace elements and isotopic compositions. The North Qilian Mountains should be a part of theTethyan tectonic domain in early Paleozoic. This further implies that the Tethyan tectonic domaincan be deduced to early Paleozoic in the study area, which will be helpful to discussing thetectonic affinity and evolution of the North Qilian Mountains.

关键词： geochemistry, Indian Ocean-MORB-type isotopic signatures, Tethyan tectonic domain, Yushigou ophiolite, North Qilian Mountains.

Experimental remolding on the caprock's 3. strain field of the Indosinian-Yanshanian epoch in Tongling deposit concentrating area

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Science china Earth Sciences 2005年第7期48卷 863-874页

作者： DENG Jun1,HUANG Dinghua2.WANG Qingfei1,WAN Li1,SUN Zhongshi3.YANG Liqiang1 & GAO Bangfei1 1. State Key Laboratory of Geological Processes and Mineral Resources,china university of {2.,Beijing 100083.china 2. faculty of Earth Sciences,china university of {2.,wuhan 43.074,china 3. Department of Earth Sciences,Jilin university,Changchun 13.061,china State Key Laboratory of Geological Processes and Mineral Resources China University of Geosciences Beijing 100083 China faculty of Earth Sciences China University of Geosciences Wuhan 430074 China Department of Earth Sciences Jilin University Changchun 130061 China

Based on field observations and rheology analysis, we perform one analogue experiment and remold the 3. structural frame of Tongling deposit concentrating area firstly. Then we disassemble and dialyze the 3. structures of the model using the methods of "slicing" and "stripping". A series of sliced planes vertical to the fold hinges show similar landscapes of that in the drill hole profiles. Meanwhile, layer stripping analysis indicates that the deformation features of each layer in the model are qualitatively analogical to those obtained from field observations. Through contrasting the 3. structure between the experimental model and the field phenomena, we verify the following 3. deformation features of the caprock in this area: (1) the Tongling area mainly consists of three series of NE S-typed fold groups; (2. in the uniform stress field, the incoherent folds universally develop in different positions, along different axes as well as in different strata; (3. the faults propagate upward which are mostly inter-bedded detachment faults, while the fold amplitudes decrease while going deeper; and (4) the folds and cleavages are highly developed in the Silurian System indicating that the deformation effect of the Indosin-ian-Yanshanian structural layer terminates at this layer, which suggests that the Silurian System is the crucial layer for the inversion between brittle and plastic deformation domains and the underlying strata are subject to the control of another deformation system with distinct properties.

关键词： Tongling deposit concentrating area Indosinian-Yanshanian epoch 3. structural frame of the caprock analogue experiment slicing and stripping analysis structural model.

Geothermal and fluid flowing simulation of ore-forming antimony deposits in Xikuangshan

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Science china Earth Sciences 2006年第8期49卷 862-871页

作者： YANG Ruiyan1,2. MA Dongsheng2. BAO Zhengyu3. PAN Jiayong2. CAO Shuanglin2.& XIA Fei2.1. School of Mathematics and Physics, china university of geosciences, wuhan 43.074,{2. 2. State Key Laboratory for Research of Mineral Deposits, Nanjing university, Nanjing 2.0093.{2. 3. faculty of Earth Sciences, china university of geosciences, wuhan 43.074,{2. 1. School of Mathematics and Physics China University of Geosciences Wuhan 430074 China 2. State Key Laboratory for Research of Mineral Deposits Nanjing University Nanjing 210093 China 3. faculty of Earth Sciences China University of Geosciences Wuhan 430074 China

The Xikuangshan Antimony Deposit located in the Mid-Hunan Basin, china, is the larg- est antimony deposit in the world. Based on the hydrogeological and geochemical data collected from four sections, Xikuangshan-Dajienao (AO), Xikuangshan-Dashengshan (BO), Xikuang- shan-Longshan (CO) and Dafengshan (DO) in the Basin, an advanced metallogenic model related to deep-cyclic meteoric water of Xikuangshan Antimony Deposit is put forward in this paper using a model of heat-gravity-driving fluid flow transportation. The simulation results show that the ore-forming fluid of the deposit mainly comes from the Dashengshan and Longshan areas where BO and CO sections are located if the overall basin keeps a constant atmospheric precipitation and infiltration rate during mineralization, and that the average transportation speed of the ore-forming fluids is about 0.2.0.4 m/a.

关键词： ore-forming fluid, numerical simulation, geothermal field, geofluid transport, Xikuangshan, antimony deposits.

Electron microscopy study of the sakhaite from endogenous borate deposit in Hunan, china

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Science china Earth Sciences 2004年第3期47卷 232-238页

作者： LIU Xiangwen1,2. YANG Guangming2. ZOU Huamin3. QU Jing1 & ZHAO Wenxia4 1. Graduate School, china university of geosciences,{3.,{2. 2. Test Center, china university of geosciences,{3.,{2. 3. Physics and Technology College, wuhan university, wuhan 43.072.{2. 4. Test Center, Zhongshan university, Guangzhou 5102.5,{2. china Univ Geosci Grad Sch Wuhan 430074 Peoples R China china Univ Geosci Test Ctr Wuhan 430074 Peoples R China wuhan Univ Phys & Technol Coll Wuhan 430072 Peoples R China Zhongshan Univ Test Ctr Guangzhou 510275 Peoples R China

Sakhaite specimens from an endogenous borate deposit in Hunan Province, china have been studied in detail by means of transmission electron microscopy (TEM). The selected area electron diffraction (SAED) patterns obtained with different crystal zone axes show that the crystal system is cubic, with a = 1.463.nm. The convergent beam electron diffraction (CBED) patterns indicate that the point group and space group of sakhaite is m3. and Fd3., respec-tively. The space group of synthetic sakhaite determined by Chichagov (1974) is F413.1} The possible reasons why the space groups of the natural and the synthetic sakhaites are different are discussed.

关键词： sakhaite, space group, convergent beam electron diffraction (CBED).

Petrogenesis and dating of the Kangding complex,Sichuan Province

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Science china Earth Sciences 2005年第5期48卷 622-634页

作者： CHEN Yuelong 1 , LUO Zhaohua 1 , ZHAO Junxiang, LI Zhihong, ZHANG Hongfei & SONG Biao 3.1. faculty of Earth Sciences and Natural Resources, china university of geosciences, Beijing 100083.{2. 2. faculty of Earth Sciences, china university of geosciences, wuhan 43.074,{2. 3. Beijing SHRIMP Center, Institute of Geology, Chinese Academy of Geological Sciences, Beijing 10003.,{2. 1. faculty of Earth Sciences and Natural Resources China University of Geosciences 100083 Beijing China 2. faculty of Earth Sciences China University of Geosciences 430074 Wuhan China 3. Beijing SHRIMP Center Institute of Geology Chinese Academy of Geological Sciences 100037 Beijing China

An analysis of major and trace element geochemistry and SHRIMP U-Pb zircon dating of mafic, intermediate, and felsic rocks from the Mianning metamorphic complex of Si- chuan Province was conducted. One of our conclusions is that a majority of the zircons crystal- lized between 72. and 773.Ma in a magmatic regime. The complexes contain early to late Pa- leo-proterozoic relict zircons from ancient continental crust. The oldest age, 2.68 Ma, may rep- resent the basement of the Yangtze block. Overgrowth zircon rims and palingenetic zircons have been observed and dated, and are believed to have formed after crystallization, during Paleozoic and Mesozoic metamorphic-anatexis. We also conclude that depletion of Nb, Ta, HREE, in a spider-diagram normalized to primitive mantle and calc-alkaline association, implies that they formed in island-arc or under-plating settings.

关键词： Kangding complex, zircons, SHRIMP, tectonic setting.

Experimental study of ore gabbro liquid immiscibility

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Science china Earth Sciences 2005年第4期48卷 496-505页

作者： SANG Zunan1,2. XIA Bin1, ZHOU Yongsheng3.& JIN Zhenmin4 1. Guangzhou Institute of Geochemistry, Chinese Academy of Sciences, Guangzhou 510640, china 2. {3. {2., {3. 43.072. china 3. Institute of Geology, china Seismological Bureau, Beijing 10002., china 4. faculty of Earth Sciences, china university of geosciences,{13., china 1. Guangzhou Institute of Geochemistry Chinese Academy of Sciences 510640 Guangzhou China 2. wuhan university 430072 Wuhan China 3. Institute of Geology China Seismological Bureau 100029 Beijing China 4. faculty of Earth Sciences China University of Geosciences 430074 Wuhan China

In this paper, the authors present the results of a preliminary experimental study on partial melting of fine-grained gabbro, Panzhihua, Sichuan Province, china. Experiments were conducted under (confining) pressure ranging from 450 to 500 MPa and temperature of 900— 12.0℃. The results show that the initial melt is distributed along grain boundaries and triple junctions. Liquid immiscibility phenomena are noted in the melt with two compositional different melt phases, i.e. matrix and sphere phases. The matrix phase is relatively rich in Si, Al and K, and is depleted in Mg, Fe, Ca, Na and Ti, whereas the sphere phase shows opposite trends. The calculation of the melt free energy indicates that the liquid immiscibility is governed by the rule of thermodynamics, as the liquid immiscibility would result in the decrease in free energy of the melt system. The field relationships suggest that the liquid immiscibility may have played an important role in the generation of ore magma of Panzhihua V-Ti magnetite ore deposit. This study thus provides experimental constraints on the mechanism of the formation of V-Ti magnetite deposite.

关键词： partial melting, experimental study, gabbro, liquid immiscibility, ore formation mechanism.

Study on the two and three-parameter working stability regions of 3.-TZP suspension

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Science china(Technological Sciences) 2006年第5期49卷 547-568页

作者： CHEN Youqiang1, 2. ZHANG Xinni3. CHEN Sha’ou3.& QI Ping3.1. Department of Chemistry, Qingdao university, Qingdao 2.6071,{3. 2. Department of Chemistry, Tsinghua university, Beijing 100084,{3. 3. Department of Physics, Qingdao university, Qingdao 2.6071,{3. 1. Department of Chemistry Qingdao University Qingdao 266071 China 2. Department of Chemistry Tsinghua University Beijing 100084 China 3. Department of Physics Qingdao University Qingdao 266071 China

We determined the variation tendency of viscosity (η) at various solids load- ing (α) for 3.-TZP suspension as a function of dispersant concentration (Cw) using vis- cosity measurement, measured the diameter of particles as a function of Cw in very dilute suspension using light scattering method, and obtained the surface features of the sedi- ment of suspension with different Cw using SEM. We also discussed the influence of the microstructure of adsorbed polymer layers on particles and their interactions in the dis- persing medium on the stability of suspension. Then two different stable states and two different unstable states for 3.-TZP suspension were given. Accordingly, the (Cw, η), (Cw, α), and (α, η) two-parameter, and (Cw, α, η) three-parameter stability maps were con- structed. Based on the DLVO theory calculations, the dispersant concentration, particle distance (r), and interparticle potential energy (VT) maps with various solids loading for 3.-TZP aqueous suspension were also constructed. In (Cw, r) two-parameter coordinate system, the stable motion region map for particles was established. The Cw, α, and VT,max (the highest potential energy) surface of the potential barrier map was obtained through calculation and simulation on the basis of the surfaces of Cw, r, VT maps introduced above. The (Cw, α) two-parameter stability map was then obtained from the Cw, α, VT,max map. The results showed that this theoretical map can qualitatively prove the experimentally obtained results—the existence of different dispersed states of particles in suspension system and the variation tendency of suspension stability with changing each parame- ter—were reasonable.

关键词： 3.-TZP, suspension, stability, DLVO theory, interparticle potential energy.

复方碘口腔喷雾原位膜的制备及促口腔溃疡修复评价

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中国药科大学学报 2024年

作者：张小军黄山芩郭潇涵季梦菲沈雁陈大全许颖 1.江苏大学药学院 2.中国药科大学药学院 3.烟台大学药学院江苏大学药学院中国药科大学药学院烟台大学药学院

采用原位凝胶技术，制备了新型复方碘口腔喷雾原位膜，用于发挥缓释作用，并促进口腔溃疡创面修复。首先以喷雾状态和成膜时间为指标，对喷雾药液的处方和工艺进行优化。以成膜时间和药膜黏附性为评价指标对药液混合比例进行考察。并对... 详细信息

采用原位凝胶技术，制备了新型复方碘口腔喷雾原位膜，用于发挥缓释作用，并促进口腔溃疡创面修复。首先以喷雾状态和成膜时间为指标，对喷雾药液的处方和工艺进行优化。以成膜时间和药膜黏附性为评价指标对药液混合比例进行考察。并对最优处方制备的复方碘口腔喷雾药液的药物含量、稳定性、pH、喷雾效果，及原位膜的成膜时间、溶解性、吸湿性、保湿性、体外释放等理化性质进行考察；此外，通过细胞实验考察了成膜材料的生物相容性及复方碘口腔喷雾原位膜的促迁移效果；采用兔口腔溃疡模型，对复方碘口腔喷雾在体成膜效果及促修复效果进行评价。实验结果显示，最优处方制备的药液A和药液B的pH分别为6.2. ± 0.02. 6.42.± 0.03.符合正常口腔黏膜pH范围；稳定性好，具有良好的喷雾状态；药液B中碘含量为（1.96 ± 0.01）mg/mL；原位膜体外成膜时间为（118.3.± 3.6）s，口腔内成膜时间为（13..3.± 4.6）s；2. h溶解率为（87.3. ± 1.74）%，吸湿率为（12..17 ± 7.13.%，保湿率为（2..85 ± 2.50）%；复方碘口腔喷雾原位膜中碘含量为（47.42.± 0.3.）mg/g；具有良好的柔韧性和黏附性，并具有一定的缓释效果。细胞实验中，原位膜表现出良好的促成纤维细胞迁移作用。兔口腔溃疡实验表明，复方碘口腔喷雾在体可快速成膜，并可显著促进口腔溃疡修复。本研究所开发的复方碘口腔喷雾原位膜，制备工艺稳定，并可有效促进口腔溃疡创面修复，为口腔黏膜制剂的研究和开发提供了新思路，并具有良好的转化前景。

关键词：口腔喷雾原位膜复方碘口腔溃疡缓释促修复

Carbon isotope composition of the Lower Triassic marine carbonates, Lower Yangtze Region, South china

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Science china Earth Sciences 2006年第3期49卷 225-241页

作者： ZUO Jingxun1,2. TONG Jinnan3. QIU Haiou4 & ZHAO Laishi3.1. Nanjing Institute of Geology and Palaeontology, Chinese Academy of Sciences, Nanjing 2.0008, china 2. Henan Institute of Geological Survey, Zhengzhou 450007, china 3. State Key Laboratory of Geological Processes and Mineral Resources at{2., wuhan 43.074, china 4. faculty of Material Sciences and Chemical Engineering,{2., wuhan 43.074, china 1. Nanjing Institute of Geology and Palaeontology Chinese Academy of Sciences Nanjing 210008 China 2. Henan Institute of Geological Survey Zhengzhou 450007 China 3. State Key Laboratory of Geological Processes and Mineral Resources at china university of geosciences Wuhan 430074 China 4. faculty of Material Sciences and Chemical Engineering China University of Geosciences Wuhan 430074 China

Studies on three Lower Triassic sections located on the shallow water platform, the deep water slope and in the deep water basin in the Lower Yangtze Region, South china, show the similar trend of carbon isotope evolution. Biostratigraphic correlations among the Lower Triassic sections on the basis of standard conodont zones indicate that three negative shifts occurred in the Griesbachian, the Smithian and the late Spathian stages respectively, and one distinctly positive shift occurred in the early Spathian stage. Trend of carbon isotope evolution of the Lower Triassic reflects some significant changes in the global carbon cycle. Moreover, δ 13. background values are intensively controlled by palaeogeographic environment. In general, δ 13. values from deep-water slope carbonates are lighter than those from carbonate platform and heavier than those from deep-water basin carbonates. The positive carbon isotope excursion may be induced by a significant amount of organic carbon burial in marine sediments and increase in primary productivity. The large negative carbon isotope excursions during the Early Triassic in Lower Yangtze Region are interpreted to relate to volcano eruptions based on tuffaceous claystone interlayers observed near the Permian-Triassic boundary, the Induan- Olenekian boundary and the Lower Triassic-Middle Triassic boundary.

关键词： Lower Triassic, carbon isotope compositions, palaeogeography, volcanic eruptions, Lower Yangtze Region.